ChemicalBook > CAS DataBase List > 3-Iodophenol

3-Iodophenol

Product Name
3-Iodophenol
CAS No.
626-02-8
Chemical Name
3-Iodophenol
Synonyms
3-Jodphenol;m-iodo-pheno;3-iodo-pheno;3-IODOPHENOL;M-IODOPHENOL;3-lodophenol;META-IODOPHENOL;Phenol, m-iodo-;PHENOL, 3-IODO-;3- iodinephenol
CBNumber
CB2461111
Molecular Formula
C6H5IO
Formula Weight
220.01
MOL File
626-02-8.mol
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3-Iodophenol Property

Melting point:
42-44 °C (lit.)
Boiling point:
190 °C / 100mmHg
Density 
1.8665 (estimate)
Flash point:
>230 °F
storage temp. 
2-8°C
solubility 
Chloroform, Ethyl Acetate
form 
Crystalline Powder, Crystals and/or Chunks
pka
9.03(at 25℃)
color 
Yellow-beige to gray
Water Solubility 
slightly soluble
Sensitive 
Light Sensitive
BRN 
2039304
InChIKey
FXTKWBZFNQHAAO-UHFFFAOYSA-N
CAS DataBase Reference
626-02-8(CAS DataBase Reference)
NIST Chemistry Reference
Phenol, 3-iodo-(626-02-8)
EPA Substance Registry System
m-Iodophenol (626-02-8)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-37/39-24/25
RIDADR 
UN 3335
WGK Germany 
2
RTECS 
SL5490000
TSCA 
T
HazardClass 
IRRITANT
HS Code 
29081900
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
I10007
Product name
3-Iodophenol
Purity
98%
Packaging
5g
Price
$41.6
Updated
2024/03/01
Sigma-Aldrich
Product number
I10007
Product name
3-Iodophenol
Purity
98%
Packaging
25g
Price
$111
Updated
2024/03/01
TCI Chemical
Product number
I0495
Product name
3-Iodophenol
Purity
>98.0%(GC)
Packaging
10g
Price
$91
Updated
2024/03/01
TCI Chemical
Product number
I0495
Product name
3-Iodophenol
Purity
>98.0%(GC)
Packaging
25g
Price
$178
Updated
2024/03/01
Alfa Aesar
Product number
A11155
Product name
3-Iodophenol, 98%
Packaging
10g
Price
$42.65
Updated
2024/03/01
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3-Iodophenol Chemical Properties,Usage,Production

Chemical Properties

yellow-beige to grey crystalline powder, crystals

Uses

3-Iodophenol is used in esterification, electrophilic aromatic substitution, alkylation, nucleophilic aromatic substitution, Mitsunobu, transition metal-catalyzed cross-coupling, acylation, and oxidation reactions.

Definition

ChEBI: 3-iodophenol is an iodophenol.

Application

3-Iodophenol is used in the synthesis of centrally acting H2 receptor histamine antagonists. Also used in the preparation of various cell-permeable probes for biological assays.

Synthesis

3-Iodophenol Synthesis:
1￡?Add potassium tert-butoxide (67.3 mg, 0.60 mmol, 2.0 eq.), oxime (74.5 mg, 0.60 mmol, 2.0 eq.), and 4??-bromoacetophenone (59.7 mg, 0.30 mmol, 1.0 eq.) to an oven-dry screw-cap 8mL reaction vial.
2￡?Add anhydrous DMSO (1.5 mL) to the solids a magnetic stir bar.
3￡?Close the vial and sparge the reaction mixture with N2 for 15 minutes, seal with parafilm.
4￡?Stir the reaction mixture and heat at 100??C in a metal heating block for 16 h.
5￡?Dilute the mixture with CH2Cl2 or EtOAc (20 mL), pour into a mixture of water (10mL) and brine (5 mL), acidify with 10% aq HCl (~1 mL).
6￡?Collect the organic phase and extract the aqueous phase with CH2Cl2 or EtOAc (3?á20mL).
7￡?Combine the organics, dry (MgSO4) and concentrate under reduced pressure.
8￡?Purify the crude product to give 3-Iodophenol by column chromatography (30% EtOAc in hexane).

3-Iodophenol Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Iodophenol Suppliers

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View Lastest Price from 3-Iodophenol manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
3-Iodophenol 626-02-8
Price
US $750.00-730.00/kg
Min. Order
1kg
Purity
98% GC
Supply Ability
10T
Release date
2022-09-21
Hebei Chuanghai Biotechnology Co,.LTD
Product
3-Iodophenol 626-02-8
Price
US $30.00-10.00/kg
Min. Order
10kg
Purity
99%
Supply Ability
100000kg
Release date
2024-08-20
Hebei Weibang Biotechnology Co., Ltd
Product
3-Iodophenol 626-02-8
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20 mt
Release date
2023-03-01

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