ChemicalBook > CAS DataBase List > 3,3',5-TRIIODOTHYROACETIC ACID

3,3',5-TRIIODOTHYROACETIC ACID

Product Name
3,3',5-TRIIODOTHYROACETIC ACID
CAS No.
51-24-1
Chemical Name
3,3',5-TRIIODOTHYROACETIC ACID
Synonyms
TIRATRICOL;TRIAC;Levothyroxine EP Impurity C;T3A;Nidolin;Triacana;Tilaquke;TRIIODOTHYROACETICACID;Levothyroxine Impurity C;Liothyronine EP Impurity C
CBNumber
CB8275848
Molecular Formula
C14H9I3O4
Formula Weight
621.93
MOL File
51-24-1.mol
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3,3',5-TRIIODOTHYROACETIC ACID Property

Melting point:
65°; mp 180-183°
Boiling point:
531.6±50.0 °C(Predicted)
Density 
2.466±0.06 g/cm3(Predicted)
storage temp. 
-20°C
solubility 
DMSO (Slightly, Heated), Methanol (Slightly, Heated, Sonicated)
form 
Solid
pka
4.02±0.10(Predicted)
color 
White to Pale Beige
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Safety

Hazard Codes 
Xn
Risk Statements 
20/21/22
Safety Statements 
36
WGK Germany 
3
HS Code 
2916.39.7900
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
T7650
Product name
3,3′,5-Triiodothyroacetic acid
Purity
≥90%
Packaging
100mg
Price
$135
Updated
2024/03/01
Sigma-Aldrich
Product number
T7650
Product name
3,3′,5-Triiodothyroacetic acid
Purity
≥90%
Packaging
1g
Price
$620
Updated
2024/03/01
TCI Chemical
Product number
T3878
Product name
3,3',5-Triiodothyroacetic Acid
Packaging
200MG
Price
$176
Updated
2024/03/01
TCI Chemical
Product number
T3878
Product name
3,3',5-Triiodothyroacetic Acid
Packaging
1G
Price
$337
Updated
2021/12/16
Cayman Chemical
Product number
28729
Product name
Tiratricol
Packaging
100mg
Price
$61
Updated
2024/03/01
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3,3',5-TRIIODOTHYROACETIC ACID Chemical Properties,Usage,Production

Chemical Properties

White to Off-White Solid

Originator

Triacana,Ana,Italy,1972

Uses

thyroid agent

Uses

3,3'',5-Triiodo Thyroacetic Acid (T3-Acetic Acid (USP)) is a thyroid hormone analogue. A potent Thyroxine impurity. Levothyroxine EP Impurity C.

Manufacturing Process

Preparation of 3:5-diiodo-4-(4'-hydroxyphenoxy)phenylacetic acid (diacid): A solution of ethyl 3:5-diiodo-4-(4'-methoxyphenoxy)phenyl acetate (9.5 g) in acetic acid (60 ml) was heated under reflux with hydroiodic acid (SG 1.7, 50 ml) and red phosphorus (0.5 g) for 1 hour. The hot solution was filtered and the filtrate concentrated at 50°C and 15 mm of mercury to above 20 ml. The residue was treated with water (70 ml) containing a little sodium thiosulfate to decolorize the product. The solid was collected by filtration and purified by the method of Harington and Pitt-Rivers [Biochem. J. (1952), Vol. 50, page 438]. Yield 8.36 g (95%). After crystallization from 70% (v/v) acetic acid it melted at 219°C.
A solution of 438 mg of diac in methanol (20 ml) and ammonia solution (SG 0.88; 20 ml) was iodinated at 0°C with 1.8 ml 1 N iodine solution. The product was isolated in almost theoretical yield in a manner similar to that described for tetrac. After crystallization from 50% (v/v) methanol, triac was obtained as colorless needles which melted over the range 65°C to 90°C according to the rate of heating. The molten form resolidified at about 110°C and finally melted at 180°C to 181°C without decomposition. The compound, dried at 25°C/3 mm over silica gel, contains methanol of crystallization.

Therapeutic Function

Thyroid hormone

3,3',5-TRIIODOTHYROACETIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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3,3',5-TRIIODOTHYROACETIC ACID Suppliers

Shifang ShengYuan Technology Co., Ltd.
Tel
0838-6510595 13402890778 18881099744
Email
1120021438@qq.com
Country
China
ProdList
131
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56
Shanghai Mokai Pharmaceutical Technology Co., Ltd.
Tel
021-60951261 18601606476
Email
nancy@mkpharma.cn
Country
China
ProdList
453
Advantage
58
J & K SCIENTIFIC LTD.
Tel
010-82848833 400-666-7788
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
Advantage
76
INTATRADE GmbH
Tel
+49 3493/605464
Fax
+49 3493/605470
Email
sales@intatrade.de
Country
Germany
ProdList
3572
Advantage
66
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44689
Advantage
61
Chemsky(shanghai)International Co.,Ltd.
Tel
021-50135380
Email
shchemsky@sina.com
Country
China
ProdList
32321
Advantage
50
Spectrum Chemical Manufacturing Corp.
Tel
021-021-021-67601398-809-809-809 15221380277
Fax
021-57711696
Email
marketing_china@spectrumchemical.com
Country
China
ProdList
9658
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BOC Sciences
Tel
1-631-485-4226; 16314854226
Email
info@bocsci.com
Country
United States
ProdList
14055
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65
Dalian Meilun Biotech Co., Ltd.
Tel
0411-62910999 13889544652
Email
meilunui@163.com
Country
China
ProdList
4727
Advantage
58
S.Z. PhyStandard Bio-Tech. Co., Ltd.
Tel
0755-4000505016 13380397412
Fax
0755 28094224
Email
3001272453@qq.com
Country
China
ProdList
5050
Advantage
50
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View Lastest Price from 3,3',5-TRIIODOTHYROACETIC ACID manufacturers

WUHAN FORTUNA CHEMICAL CO., LTD
Product
Tiratricol 51-24-1
Price
US $0.00/g
Min. Order
1g
Purity
95%101% HPLC
Supply Ability
1000G
Release date
2021-08-13
WUHAN CIRCLE POWDER TECHNOLOGY CO.,LTD
Product
Tiratricol 51-24-1
Price
US $0.00/KG
Min. Order
100g
Purity
98%+
Supply Ability
100kg
Release date
2020-10-14
Career Henan Chemical Co
Product
2-[4-(4-hydroxy-3-iodophenoxy)-3,5-diiodophenyl]acetic acid 51-24-1
Price
US $1.00/KG
Min. Order
1KG
Purity
98% HPLC
Supply Ability
10 tons
Release date
2020-02-14

51-24-1, 3,3',5-TRIIODOTHYROACETIC ACIDRelated Search:


  • TIRATRICOL
  • TRIAC
  • 3,3',5-TRIIODOTHYROACETIC ACID
  • 4-[4-HYDROXY-3-IODOPHENOXY]-3,5-DIIODOPHENYLACETIC ACID
  • 4'-HYDROXY-3,5,3'-TRIIODOPHENOXY-4-PHENYLACETIC ACID
  • 2-[4-(4-hydroxy-3-iodo-phenoxy)-3,5-diiodo-phenyl]acetic acid
  • 3,3,5-triiodothyroacetic acid,*free acid
  • TRIIODOTHYROACETICACID
  • 2-[4-(4-hydroxy-3-iodophenoxy)-3,5-diiodophenyl]acetic acid
  • 2-[4-(4-hydroxy-3-iodo-phenoxy)-3,5-diiodo-phenyl]ethanoic acid
  • [(4-Hydroxy-3-iodo-4-phenoxy)-3,5-diiodophenyl]acetic Acid
  • 4-(4-Hydroxy-3-iodophenoxy)-3,5-diiodobenzeneacetic Acid
  • Nidolin
  • T3A
  • Triacana
  • Tiratricol/ 3,3',5-triiodothyroacetic acid
  • 3,3',5-TRIIODOTHYROACETIC ACID (TIRATRICOL)
  • Benzeneacetic acid,4-(4-hydroxy-3-iodophenoxy)-3,5-diiodo-
  • Tiratricol SynonyMs 3,3,5-Triiodothyroacetic acid
  • Levothyroxine Impurity C
  • 3,3',5-Triiodothyroacetic acid >=90%
  • Levothyroxine EP Impurity C
  • Tiratricol,4-(4-hydroxy-3-iodophenoxy)-3,5-diiodo-Benzeneacetic acid
  • Liothyronine EP Impurity C
  • Levothyroxine Impurity 3(Levothyroxine EP Impurity C)
  • [4-(4-Hydroxy-3-iodophenoxy)-3,5-di
  • Liothyronine EP Impurity C (Levothyroxine EP Impurity C)
  • Tiratricol (Triiodothyroacetic Acid)
  • Liothyronine EP Impurity C (Triiodothyroacetic Acid/ Levothyroxine EP Impurity C/ Levothyroxine T3-Acetic Acid)
  • Levothyroxine EP Impurity C/ Levothyroxine T3-Acetic Acid (Liothyronine EP Impurity C/ Triiodothyroacetic Acid)
  • 4'-HYDROXY-3,5,3'-TRIIODOPHENOXY-4-PChemicalbookHENYLACETICACID
  • 51-24-1 C14H9I3O4 3,3',5-TRIIODOTHYROACETIC ACID
  • Liothyronine Sodium Impurity C
  • 2-[4-(4-hydroxy-3-iodophenoxy)-3,5-diiodophenyl]aceticaci
  • Tilaquke
  • Liothyronine Sodium EP Impurity C
  • Levothyroxine Sodium EP Impurity C
  • Levothyroxine EP Impurity-C (T3 acetic acid)
  • 3,3',5-TRIIODOTHYROACETIC ACID
  • LEVOTHYROXINE EP IMPURITY C | T3-ACETIC ACID (USP)
  • 51-24-1
  • C14H9I3O4
  • C13 to C42+
  • Carboxylic Acids
  • Carbonyl Compounds
  • Building Blocks
  • Organic Building Blocks
  • API
  • Bioactive Small Molecules
  • Building Blocks
  • C13 to C42+
  • Carbonyl Compounds
  • Carboxylic Acids
  • Cell Biology
  • Chemical Synthesis
  • Organic Building Blocks
  • T
  • Aromatics, Drug Analogues, Impurities, Pharmaceuticals, Intermediates & Fine Chemicals