3-Phenoxypyridine
- Product Name
- 3-Phenoxypyridine
- CAS No.
- 2176-45-6
- Chemical Name
- 3-Phenoxypyridine
- Synonyms
- 3-PHENOXYPYRIDINE;Pyridine, 3-phenoxy-;3-PHENOXYPYRIDINE AND MONOSULFATE
- CBNumber
- CB2512248
- Molecular Formula
- C11H9NO
- Formula Weight
- 171.2
- MOL File
- 2176-45-6.mol
3-Phenoxypyridine Property
- Boiling point:
- 147-149 °C
- Density
- 1.117±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 4.35±0.10(Predicted)
- form
- solid
- Appearance
- Colorless to light yellow Liquid
Safety
- Toxicity
- mouse,LD50,oral,400mg/kg (400mg/kg),United States Patent Document. Vol. #4859663,
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- CDS020813
- Product name
- 3-Phenoxypyridine
- Packaging
- 25 mg
- Price
- $73.1
- Updated
- 2025/07/31
- Product number
- P318890
- Product name
- 3-Phenoxypyridine
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- CS-0060564
- Product name
- 3-Phenoxypyridine
- Purity
- ≥98.0%
- Packaging
- 100mg
- Price
- $67
- Updated
- 2021/12/16
- Product number
- CS-0060564
- Product name
- 3-Phenoxypyridine
- Purity
- ≥98.0%
- Packaging
- 250mg
- Price
- $112
- Updated
- 2021/12/16
- Product number
- 4H56-1-3BW
- Product name
- 3-Phenoxypyridine
- Purity
- 98%
- Packaging
- 1g
- Price
- $160
- Updated
- 2021/12/16
3-Phenoxypyridine Chemical Properties,Usage,Production
Synthesis
1692-25-7
144930-50-7
2176-45-6
GENERAL METHODS: Pyridine-3-boronic acid (1.0 mmol), homotrimethylphenyl (phenyl) iodonium trifluoromethanesulfonate (1.2 mmol), eosin Y (34.5 mg, 0.02 mmol) and sodium tert-butoxide (1.1 mmol, 25 mg) were dissolved in N,N-dimethylformamide (2.0 mL) in a borosilicate flask. The reaction was stirred for 1-2 hours at room temperature under continuous irradiation with 18 Watt LED visible light. Upon completion of the reaction (monitored by thin layer chromatography), the reaction mixture was poured into water (50 mL) and stirring was continued for 2 hours. The aqueous phase was extracted with dichloromethane (2 x 20 mL), the organic phases were combined and dried over anhydrous sodium sulfate. After concentration under reduced pressure, the residue was purified by silica gel column chromatography [eluent: ethyl acetate/petroleum ether (60-90 °C) = 1:10 to 1:4] to afford the target product, 3-phenoxypyridine (3h), as a yellowish oil.1H NMR (CDCl3, 400 MHz) δ 8.21-8.20 (m, 1H), 7.70-7.66 (m, 1H), and 7.42-7.38 (m, 2H), 7.16-7.14 (m, 2H), 7.01-6.97 (m, 1H), 6.91-6.89 (m, 1H); 13C NMR (CDCl3, 125 MHz) δ 163.8, 154.2, 147.8, 139.4, 129.7, 124.6, 121.2. 118.4, 111.5.
References
[1] Journal of Chemical Research, 2016, vol. 40, # 5, p. 261 - 264
3-Phenoxypyridine Preparation Products And Raw materials
Raw materials
Preparation Products
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