METHYL PHENYL CARBONATE
- Product Name
- METHYL PHENYL CARBONATE
- CAS No.
- 13509-27-8
- Chemical Name
- METHYL PHENYL CARBONATE
- Synonyms
- Benzoyl carbonate;PHENYLMETHYL CARBONATE;METHYL PHENYL CARBONATE;Carbonic acid methyl phenyl;Carbonic acid=methyl=phenyl ester;Carbonic acid O-phenyl O-methyl ester
- CBNumber
- CB2712514
- Molecular Formula
- C8H8O3
- Formula Weight
- 152.15
- MOL File
- 13509-27-8.mol
METHYL PHENYL CARBONATE Property
- Melting point:
- 147-151 °C
- Boiling point:
- 210-213℃
- Density
- 1.5214g/ml
- refractive index
- 1.4985
- storage temp.
- Inert atmosphere,Room Temperature
- Appearance
- Colorless to light yellow Liquid
- Stability:
- Stable. Incompatible with strong oxidizing agents.
Safety
- Safety Statements
- 22-24/25
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- 9802CA
- Product name
- Methylphenylcarbonate
- Packaging
- 1g
- Price
- $77
- Updated
- 2021/12/16
- Product number
- 9802CA
- Product name
- Methylphenylcarbonate
- Packaging
- 10g
- Price
- $157
- Updated
- 2021/12/16
- Product number
- A189967
- Product name
- Methylphenylcarbonate
- Purity
- 98%
- Packaging
- 1g
- Price
- $10
- Updated
- 2021/12/16
- Product number
- A189967
- Product name
- Methylphenylcarbonate
- Purity
- 98%
- Packaging
- 5g
- Price
- $37
- Updated
- 2021/12/16
- Product number
- A189967
- Product name
- Methylphenylcarbonate
- Purity
- 98%
- Packaging
- 25g
- Price
- $116
- Updated
- 2021/12/16
METHYL PHENYL CARBONATE Chemical Properties,Usage,Production
Chemical Properties
colourless liquid
Synthesis
67-56-1
1202680-24-7
13509-27-8
GENERAL METHODS: To a solution of methanol (0.7 mmol) and AlCl3 (0.7 mmol) in toluene (10 mL) was added compound 3 (CAS:1202680-24-7, 0.7 mmol). The progress of the reaction was monitored by thin layer chromatography (TLC) and the mixture was stirred at room temperature until the compound 3 was completely consumed. Upon completion of the reaction, 10% NaOH aqueous solution (50 mL) and dichloromethane (30 mL) were added to the reaction mixture under stirring for extraction. The organic layer was separated and washed with distilled water (50 mL) and subsequently dried over anhydrous magnesium sulfate. The solvent was removed by evaporation under reduced pressure to give the crude product. The crude product was purified by passing through an open silica gel column (2.5 x 4 cm) using hexane/ethyl acetate (3:1, v/v) as eluent. Compounds 5 and 6 were eluted first, followed by ethyl acetate. Finally, 4,5-dichloropyridazin-3(2H)-one (1) was eluted. The column chromatography fractions containing the pure compounds were combined and the solvents were evaporated under reduced pressure to afford the target product, methyl phenyl carbonate.4,5-Dichloropyridazin-3(2H)-one was obtained in quantitative yield and was reusable.
References
[1] Bulletin of the Korean Chemical Society, 2014, vol. 35, # 9, p. 2758 - 2764
[2] Synlett, 2016, vol. 27, # 10, p. 1577 - 1581
METHYL PHENYL CARBONATE Preparation Products And Raw materials
Raw materials
Preparation Products
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