ChemicalBook > CAS DataBase List > 1,2:5,6-Bis-O-(1-methylethylidene)-D-mannitol

1,2:5,6-Bis-O-(1-methylethylidene)-D-mannitol

Product Name
1,2:5,6-Bis-O-(1-methylethylidene)-D-mannitol
CAS No.
1707-77-3
Chemical Name
1,2:5,6-Bis-O-(1-methylethylidene)-D-mannitol
Synonyms
(1S,2S)-1,2-bis((R)-2,2-dimethyl-1,3-dioxolan-4-yl)ethane-1,2-diol;D-MANNITOL DIACETONIDE;1,2:5,6-DI-O-ISOPROPYLIDENE-D-MANNITOL;1,2-bis(2,2-dimethyl-1,3-dioxolan-4-yl)-1,2-ethanediol;NSC 47987;NSC 67545;NSC 89874;DIACETONE-D-MAN;idene-D-mannitoL;D-Mannitol diaceton
CBNumber
CB2741824
Molecular Formula
C12H22O6
Formula Weight
262.3
MOL File
1707-77-3.mol
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1,2:5,6-Bis-O-(1-methylethylidene)-D-mannitol Property

Melting point:
120-122 °C(lit.)
alpha 
6 º (c=5, Chloroform)
Boiling point:
382.0±32.0 °C(Predicted)
Density 
1.175±0.06 g/cm3(Predicted)
refractive index 
6.5 ° (C=8, CHCl3)
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
solubility 
methanol: 100 mg/mL, clear, colorless
form 
Crystalline Powder
pka
12.98±0.20(Predicted)
color 
White
optical activity
[α]/D +6.0±1.0°, c = 5 in chloroform
BRN 
83765
InChIKey
ODYBCPSCYHAGHA-ZYUZMQFOSA-N
CAS DataBase Reference
1707-77-3(CAS DataBase Reference)
NIST Chemistry Reference
D-Mannitol, 1,2:5,6-bis-o-(1-methylethylidene)-(1707-77-3)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
22-24/25-36/37-26
WGK Germany 
3
F 
10-21
HS Code 
29329990
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
296406
Product name
1,2:5,6-Di-O-isopropylidene-D-mannitol
Purity
98%
Packaging
5g
Price
$72.4
Updated
2023/06/20
Sigma-Aldrich
Product number
296406
Product name
1,2:5,6-Di-O-isopropylidene-D-mannitol
Purity
98%
Packaging
25g
Price
$182
Updated
2023/06/20
TCI Chemical
Product number
D2024
Product name
1,2:5,6-Di-O-isopropylidene-D-mannitol
Purity
>97.0%(GC)
Packaging
5g
Price
$24
Updated
2024/03/01
TCI Chemical
Product number
D2024
Product name
1,2:5,6-Di-O-isopropylidene-D-mannitol
Purity
>97.0%(GC)
Packaging
25g
Price
$65
Updated
2024/03/01
Alfa Aesar
Product number
L12127
Product name
1,2:5,6-Di-O-isopropylidene-D-mannitol
Packaging
5g
Price
$41.65
Updated
2024/03/01
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1,2:5,6-Bis-O-(1-methylethylidene)-D-mannitol Chemical Properties,Usage,Production

Chemical Properties

White Solid

Uses

Nebivolol intermediate.

Purification Methods

Although quite soluble in H2O, it gives a purer product when crystallised from this solvent, forming needles [Baer J Am Chem Soc 67 338 1945, NMR: Curtis et al. J Chem Soc, Perkin Trans 1 1756 1977]. [Beilstein 19/11 V 589.]

1,2:5,6-Bis-O-(1-methylethylidene)-D-mannitol Preparation Products And Raw materials

Raw materials

Preparation Products

(R)-(-)-2,2-Dimethyl-1,3-dioxolane-4-methanol
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1,2:5,6-Bis-O-(1-methylethylidene)-D-mannitol Suppliers

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View Lastest Price from 1,2:5,6-Bis-O-(1-methylethylidene)-D-mannitol manufacturers

Hebei Weibang Biotechnology Co., Ltd
Product
1,2:5,6-Bis-O-(1-methylethylidene)-D-mannitol 1707-77-3
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2024-11-01
Hebei Chuanghai Biotechnology Co,.LTD
Product
Diisopropylidene Mannitol 1707-77-3
Price
US $5.00-2.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10000kg
Release date
2024-08-23
Hebei Mojin Biotechnology Co., Ltd
Product
1,2:5,6-Bis-O-(1-methylethylidene)-D-mannitol 1707-77-3
Price
US $0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
50000KG/month
Release date
2023-09-06

1707-77-3, 1,2:5,6-Bis-O-(1-methylethylidene)-D-mannitolRelated Search:

Dimethyl sulfate Dimethyl sulfoxide N,N-Dimethylformamide Dacthal Hydroxyacetone Mannitol Dimethyl sulfide Dimethyl ether D-Mannitol Dimethyl fumarate Dimethyl carbonate Diacetone acrylamide Diacetone Alcohol ETHANE Diacetone-D-glucose 4-METHYL-1,3-DIOXOLANE 1,2,6-Hexanetriol 3-Methoxy-1-butanol

  • DIACETONE-D-MAN
  • DIACETONE-D-MANNITOL
  • D-MANNITOL DIACETONIDE
  • 1,2:5,6-ISOPROPYLIDENE-D-MANNITOL
  • 1,2,5,6-DI-O-ISOPROPYLIDENE-D-MANNITOL
  • 1,2:5,6-DI-O-ISOPROPYLIDENE-D-MANNITOL
  • 1,2:5,6-bis-o-(1-methylethylidene)-d-mannitol
  • 1,2:5,6-BIS-O-(1-METHYLETHYLIDENE)-D-MARNITOL
  • 1,2-bis(2,2-dimethyl-1,3-dioxolan-4-yl)-1,2-ethanediol
  • 1,2:5,6-Bis-O-(1-met
  • 1,2,5,6-Di-O-isopropylidene-D-mannitol ,98%
  • 1,2:5,6-Di-O-isopropylidene-D-maitol
  • 1,2,5,6-Diacetone-D-Mannitol (Mannitol diacetonide)
  • D-(+)-1,2:5,6-Di-O-isopropylideneMannitol
  • D-Mannitol 1,2:5,6-Bis-acetonide
  • NSC 47987
  • NSC 67545
  • NSC 89874
  • (1R,2R)-1,2-bis[(4S)-2,2-diMethyl-1,3-dioxolan-4-yl]ethane-1,2-diol
  • D-Mannitol diaceton
  • 1,2:5,6-Di-O-isopropylidene-D-Mannitol, 96%, 96%
  • 1,2:5,6-Bis-O-(1-methylethylide
  • (1S,2S)-1,2-bis[(4R)-2,2-dimethyl-1,3-dioxolan-4-yl]ethane-1,2-diol
  • 5,6-Bis-O-(1-methylethylidene)-D-mannitol
  • 1,2,5,6-DI-O-ISOPROPYLLIDINE-D-MANITOL
  • Diacetone-D-mannitol, ≥98%,GC
  • N'-(6-chloro-2-methoxy-9-acridinyl)ethane-1,2-diamine
  • 1,2:5,6-Bis-o-(1-methylidene)-D-mannitol
  • (1S,2S)-1,2-bis((R)-2,2-dimethyl-1,3-dioxolan-4-yl)ethane-1,2-diol
  • 1,2,5,6-Diisopropylidene-D-mannitol
  • 1,2-5,6-Diacetone D-mannitol
  • Diisopropylidene mannitol
  • Mannitol, 1,2:5,6-di-O-isopropylidene-, D
  • 1,2,5,6-DI-Isopopylidene-D-Mannitol
  • Isopropylidene-D-Mannitol
  • (2,2,2',2'-TETRAMETHYL-[4,4']BI[[1,3]DIOXOLANYL]-5-YL)-METHANOL
  • 1 2:5 6-DI-O-ISOPROPYLIDENE-D-MANNITOL 98%
  • 1,2:5,6-DI-O-ISOPROPYLIDINE-D-MANNITOL
  • D-Mannitol, 1,2:5,6-bis-O-(1-methylethylidene)-
  • (1S,2S)-1,2-Bis[(4R)-2,2-dimethyl-1,3-dioxolane-4-yl]-1,2-ethanediol
  • (1S,2S)-1,2-Bis[(4R)-2,2-dimethyl-1,3-dioxolane-4-yl]ethylene glycol
  • (1S,2S)-1,2-Bis[(4R)-2,2-dimethyl-1,3-dioxolane-4β-yl]ethylene glycol
  • 1-O,2-O:5-O,6-O-Bis(1-methylethylidene)-D-mannitol
  • Mannitol diacetonide
  • 1,2:5,6-Di-O-isopropylidene-D-mannitol&gt
  • 1,2:5,6-Di-O-isopropyL
  • idene-D-mannitoL
  • 1,2:5,6-Bis-O-(1-methylethylidene)-D-mannitol USP/EP/BP
  • (+)-1,2:5,6-di-O-isopropylidene-D-mannitol
  • 1,2:5,6- Di-o- Isopropyide- D- Manitol
  • 1707-77-3
  • C12H22O6
  • Specialty Synthesis
  • Monosaccharides
  • O-Substituted Sugars
  • Sugar Alcohols
  • Dioxanes & Dioxolanes
  • Sugars