ChemicalBook > CAS DataBase List > 1,3-Dibromoadamantane

1,3-Dibromoadamantane

Product Name: 1,3-Dibromoadamantane
CAS No.: 876-53-9
Chemical Name: 1,3-Dibromoadamantane
Synonyms: NSC 102289;1,3-Dibromoadamantan;Carazolol Impurity 5;1,3-DIBROMOADAMANTANE;Dibromoadamantane,97%;Memantine Impurity 44;Memantine Impurity 46;1,3-DIBROMO- ADAMANTINE;Adamantane, 1,3-dibromo-;1,3-Dibromoadamantane>
CBNumber: CB2770189
Molecular Formula: C10H14Br2
Formula Weight: 294.03
MOL File: 876-53-9.mol

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1,3-Dibromoadamantane Property

Melting point:: 108-110 °C (lit.)
Boiling point:: 287.6±13.0 °C(Predicted)
Density: 1.864±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
solubility: Chloroform (Slightly), Ethyl Acetate (Slightly)
form: Solid
color: White to Pale Gray
InChI: InChI=1S/C10H14Br2/c11-9-2-7-1-8(4-9)5-10(12,3-7)6-9/h7-8H,1-6H2
InChIKey: HLWZKLMEOVIWRK-UHFFFAOYSA-N
SMILES: C12(Br)CC3CC(CC(Br)(C3)C1)C2
CAS DataBase Reference: 876-53-9(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36
WGK Germany: 3
HazardClass: IRRITANT
HS Code: 2902190000

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 403083
Product name: 1,3-Dibromoadamantane
Purity: 99%
Packaging: 1g
Price: $47.5
Updated: 2025/07/31

TCI Chemical

Product number: D5654
Product name: 1,3-Dibromoadamantane (purified by sublimation)
Purity: min. 99.0 %
Packaging: 5G
Price: $258
Updated: 2025/07/31

TCI Chemical

Product number: D2480
Product name: 1,3-Dibromoadamantane
Purity: >97.0%(GC)
Packaging: 5g
Price: $46
Updated: 2025/07/31

TCI Chemical

Product number: D2480
Product name: 1,3-Dibromoadamantane
Purity: >97.0%(GC)
Packaging: 25g
Price: $108
Updated: 2025/07/31

TCI Chemical

Product number: D5654
Product name: 1,3-Dibromoadamantane (purified by sublimation)
Packaging: 1G
Price: $77
Updated: 2025/07/31

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1,3-Dibromoadamantane Chemical Properties,Usage,Production

Chemical Properties

White Solid

Uses

1,3-Dibromoadamantane may be used in the preparation of 1,3-bis(phenyldimethylsilyl)adamantine.

General Description

1,3-Dibromoadamantane is reported to react with diphenylphosphide ions (Ph₂P^-) under photostimulation by the S_RN1 mechanism. The viscosity-dependent retarding effect of 1,3-dibromoadamantane in highly viscous polymeric chlorotrifluoroethene has been studied by 13C NMR relaxation measurements. Preparation of 1,3-dibromoadamantane via dibromination of adamantine has been reported.

Synthesis

281-23-2

768-90-1

876-53-9

Reactions were carried out in 20 mL glass ampoules or 17 mL stainless steel pressure microreactors with consistent results from parallel experiments. Under argon protection, 0.3 mmol of tris(acetylacetonato)iron(III) [Fe(acac)3], 10 mmol of adamantane, 10 mmol of carbon tetrabromide (CBr4), and 150 mmol of dibromomethane (CH2Br2) were added to the microreactor (or ampoule). The reactor (or ampoule) was sealed and heated under stirring conditions. After completion of the reaction, the reactor (or ampoule) was cooled to room temperature, opened and the solvent was removed by distillation and the residue was purified by crystallization with hexane or ethanol. The conversion of adamantane and the yield of its derivatives were determined by gas chromatography (GLC) using decene as an internal standard with correction factors of 1.09 and 1.53 for adamantane and bromoadamantane, respectively.The structures of the resulting compounds were confirmed by comparison with known samples and literature data.

References

[1] Russian Journal of Organic Chemistry, 2015, vol. 51, # 2, p. 184 - 187
[2] Zh. Org. Khim., 2015, vol. 51, # 2, p. 196 - 199
[3] Tetrahedron Letters, 1986, vol. 27, # 12, p. 1399 - 1402
[4] Journal of Organic Chemistry USSR (English Translation), 1984, vol. 20, p. 2041
[5] Zhurnal Organicheskoi Khimii, 1984, vol. 20, # 10, p. 2239 - 2240

1,3-Dibromoadamantane Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1,3-Dibromoadamantane manufacturers

Wuhan JiyunZen Tech Co., Ltd.

Product: 1,3-Dibromoadamantane 876-53-9
Price: US $5.00-0.50/KG
Min. Order: 1KG
Purity: 99% hplc
Supply Ability: 500TONS
Release date: 2025-05-30

Hebei Chuanghai Biotechnology Co., Ltd

Product: 1,3-Dibromoadamantane 876-53-9
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 5tons
Release date: 2024-12-02

Henan Aochuang Chemical Co.,Ltd.

Product: 1,3-Dibromoadamantane 876-53-9
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1ton
Release date: 2022-10-12

876-53-9, 1,3-DibromoadamantaneRelated Search:

Amantadine Altrenogest 1,5-Dibromopentane Adamantane 1,5-DIBROMO-3-METHYLPENTANE 1,3-DIBROMO-3-METHYLBUTANE 2-BROMO-6-METHYLHEPTANE 2-Bromoheptane 2,4-DIBROMOPENTANE 2-CYCLOHEXYLETHYL BROMIDE 1-BROMO-5-METHYLHEXANE 1,7-DIBROMOHEPTANE 3-BROMOOCTANE 1,3-Dibromobutane 1-BROMO-3-METHYLCYCLOHEXANE CYCLOOCTYL BROMIDE 1,4-DIBROMOADAMANTANE 98% Bromocyclohexane

1,3-DIBROMOADAMANTANE

1,3-DIBROMOTRICYCLO[3.3.1.1(3,7)]DECANE

1,3-DIBROMO- ADAMANTINE

Dibromoadamantane,97%

tricyclo[3.3.1.1~3,7~]decane, 1,3-dibromo-

1,3-Dibromoadamantan

Adamantane, 1,3-dibromo-

NSC 102289

1,3-Dibromoadamantane in stock Factory

1,3-Dibromoadamantane&gt

1,3-Dibromoadamantane (purified by sublimation)

1,3-Dibromoadamantane ISO 9001：2015 REACH

Memantine Impurity 44

Memantine Impurity 46

Carazolol Impurity 5

1,3-Dibromoadamantane,99%

876-53-9

C10H14Br2

Alkyl

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Adamantanes

Halogenated Hydrocarbons

Organic Building Blocks

Alkyl

Halogenated Hydrocarbons

Organic Building Blocks

Adamantane derivatives

Miscellaneous Reagents

Adamantanes