ChemicalBook > CAS DataBase List > 3-(4-BROMO-PHENYL)-PROPIONALDEHYDE

3-(4-BROMO-PHENYL)-PROPIONALDEHYDE

Product Name
3-(4-BROMO-PHENYL)-PROPIONALDEHYDE
CAS No.
80793-25-5
Chemical Name
3-(4-BROMO-PHENYL)-PROPIONALDEHYDE
Synonyms
4-Bromophenylpropanal;4-(4-broMophenyl)butanal;Benzenepropanal, 4-broMo-;3-(4-BROMO-PHENYL)-PROPIOLDEHYDE;3-(4-BROMO-PHENYL)-PROPIONALDEHYDE
CBNumber
CB2779182
Molecular Formula
C9H9BrO
Formula Weight
213.07
MOL File
80793-25-5.mol
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3-(4-BROMO-PHENYL)-PROPIONALDEHYDE Property

Boiling point:
267.8±15.0 °C(Predicted)
Density 
1.399±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
Appearance
Colorless to light yellow Liquid
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Safety

HazardClass 
IRRITANT
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H227Combustible liquid

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Biosynth Carbosynth
Product number
FB151387
Product name
3-(4-Bromo-phenyl)-propionaldehyde
Packaging
25mg
Price
$60
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB151387
Product name
3-(4-Bromo-phenyl)-propionaldehyde
Packaging
50mg
Price
$100
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB151387
Product name
3-(4-Bromo-phenyl)-propionaldehyde
Packaging
100mg
Price
$150
Updated
2021/12/16
AK Scientific
Product number
2565AC
Product name
3-(4-Bromophenyl)propionaldehyde
Packaging
1g
Price
$177
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB151387
Product name
3-(4-Bromo-phenyl)-propionaldehyde
Packaging
250mg
Price
$250
Updated
2021/12/16
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3-(4-BROMO-PHENYL)-PROPIONALDEHYDE Chemical Properties,Usage,Production

Synthesis

25574-11-2

80793-25-5

GENERAL STEPS: Example A.4: Synthesis of 3-(4-bromophenyl)propanal (10×) 4-Bromophenylpropanol (4.71 g, 21.8 mmol) was dissolved in dichloromethane (DCM), Dess-Martin periodinane (9.71 g, 20.9 mmol) was added, and the reaction was carried out for 2 hours at room temperature. Upon completion of the reaction, the reaction was quenched with 2 M NaOH solution and the organic and aqueous phases were separated and the aqueous phase was extracted with DCM. The organic phases were combined, dried with anhydrous magnesium sulfate (MgSO4), filtered and concentrated under reduced pressure. The crude product was purified by rapid chromatography on silica gel, the eluent being a gradient solution of DCM in cyclohexane (cHex) to afford the target product 3-(4-bromophenyl)propionaldehyde (10×) (4.46 g, 96% yield) as a colorless liquid. 1H NMR (400 MHz, CDCl3) δ 9.81 (s, 1H), 7.41 (d, J = 8.4 Hz, 2H), 7.07 (d, J = 8.4 Hz, 2H), 2.91 (t, J = 7.6 Hz, 2H), 2.79-2.74 (m, 2H). MS (ES) C9H9BrO calculated value: 211/213, ([M-H]-) not detected, 100% purity.

References

[1] Patent: WO2015/181272, 2015, A1. Location in patent: Page/Page column 30
[2] Patent: EP3239143, 2017, A2. Location in patent: Paragraph 0120
[3] Patent: WO2015/66413, 2015, A1. Location in patent: Page/Page column 176; 177
[4] Patent: US2017/253554, 2017, A1. Location in patent: Paragraph 0425; 0426
[5] Chemical Communications, 2011, vol. 47, # 27, p. 7875 - 7877

3-(4-BROMO-PHENYL)-PROPIONALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-(4-BROMO-PHENYL)-PROPIONALDEHYDE manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
3-(4-Bromophenyl)propanal 80793-25-5
Price
US $0.00-0.00/KG
Min. Order
10mg
Purity
99%HPLC
Supply Ability
2000tons
Release date
2020-01-15

80793-25-5, 3-(4-BROMO-PHENYL)-PROPIONALDEHYDERelated Search:

(S)-N-Fmoc-3-Bromophenylalanine (S)-N-BOC-4-Bromophenylalanine 3-(4-BROMO-PHENYL)-3-OXO-PROPIONIC ACID ETHYL ESTER 4-BROMO-DL-PHENYLALANINE (R)-N-Fmoc-4-Bromophenylalanine 4-Bromo-1,8-naphthalic anhydride AC-P-BROMO-DL-PHE-OH (RS)-beta-Amino-beta-(4-bromophenyl)propionic acid 2-(4-BROMO-BENZYL)-MALONIC ACID DIETHYL ESTER N-ACETYL-2-(4-BROMOPHENYL)-DL-BETA-ALANINE 3-[(AMINOCARBONYL)AMINO]-3-(4-BROMOPHENYL)PROPANOIC ACID 2-(4-BROMOBENZYLIDENE)-1-BENZOSUBERONE EPOXIDE METHYL 2-AMINO-4-(4-BROMOPHENYL)-7,7-DIMETHYL-5-OXO-4,6,7,8-TETRAHYDRO2H-CHROMENE-3-CARBOXYLATE 2-(4-BENZYLIDENE)-1-INDANONEEPOXIDE 2-(4-BROMOBENZYLIDENE)-1-TETRALONE EPOXIDE [2-(BENZYLOXY)PHENYL][3-(4-BROMOPHENYL)OXIRAN-2-YL]METHANONE 1-[2-(BENZYLOXY)PHENYL]-2,3-DIBROMO-3-(4-BROMOPHENYL)PROPAN-1-ONE ethyl 3-amino-3-(4-bromophenyl)propanoate

  • 3-(4-BROMO-PHENYL)-PROPIONALDEHYDE
  • 3-(4-BROMO-PHENYL)-PROPIOLDEHYDE
  • 4-(4-broMophenyl)butanal
  • Benzenepropanal, 4-broMo-
  • 4-Bromophenylpropanal
  • 80793-25-5