5-METHYL-2-NITROBENZALDEHYDE
- Product Name
- 5-METHYL-2-NITROBENZALDEHYDE
- CAS No.
- 5858-28-6
- Chemical Name
- 5-METHYL-2-NITROBENZALDEHYDE
- Synonyms
- 2-Nitro-5-methylbenzaldehyde;5-METHYL-2-NITROBENZALDEHYDE;Benzaldehyde, 5-methyl-2-nitro-
- CBNumber
- CB2839578
- Molecular Formula
- C8H7NO3
- Formula Weight
- 165.15
- MOL File
- 5858-28-6.mol
5-METHYL-2-NITROBENZALDEHYDE Property
- Melting point:
- 64 °C
- Boiling point:
- 314.0±30.0 °C(Predicted)
- Density
- 1.278±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- Light yellow to green yellow Solid
Safety
- HS Code
- 2913000090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B498268
- Product name
- 5-methyl-2-nitrobenzaldehyde
- Packaging
- 50mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- B498268
- Product name
- 5-methyl-2-nitrobenzaldehyde
- Packaging
- 500mg
- Price
- $350
- Updated
- 2021/12/16
- Product number
- 4754-1-15
- Product name
- 5-Methyl-2-nitrobenzaldehyde
- Purity
- 98.0%
- Packaging
- 1g
- Price
- $454
- Updated
- 2021/12/16
- Product number
- CHM0151091
- Product name
- 5-METHYL-2-NITRO-BENZALDEHYDE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $495.95
- Updated
- 2021/12/16
- Product number
- 047928
- Product name
- 5-Methyl-2-nitrobenzaldehyde
- Packaging
- 250mg
- Price
- $90
- Updated
- 2021/12/16
5-METHYL-2-NITROBENZALDEHYDE Chemical Properties,Usage,Production
Synthesis
66424-92-8
5858-28-6
General procedure for the synthesis of 5-methyl-2-nitrobenzaldehyde from 5-methyl-2-nitrobenzyl alcohol: a) 5-methyl-2-nitrobenzyl alcohol (10 g, 59.88 mmol) was dissolved in dichloromethane (210 mL). Subsequently 3A molecular sieves (54 g) and pyridinium dichromate (22.53 g, 59.88 mmol) were added. The reaction mixture was stirred at room temperature for 6 hours. After completion of the reaction, the crude product was filtered through a short silica gel column and concentrated under reduced pressure. The residue was purified by fast column chromatography (silica gel, 10-20% ethyl acetate/hexane as eluent) to afford 7.84 g (79% yield) of the target compound 5-methyl-2-nitrobenzaldehyde as a colorless oil.1H NMR (CDCl3) δ 10.41 (m, 1H), 8.02 (m, 1H), 7.69 (s, 1H), 7.53 (d, 1H). 1H), 2.51 (s, 3H).
References
[1] Patent: US2004/10004, 2004, A1. Location in patent: Page 22
[2] Journal of Organic Chemistry, 1980, vol. 45, # 7, p. 1334 - 1336
[3] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001, vol. 40, # 5, p. 436 - 437
[4] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001, vol. 40, # 4, p. 329 - 330
[5] Bulletin of the Korean Chemical Society, 2011, vol. 32, # 12, p. 4309 - 4315
5-METHYL-2-NITROBENZALDEHYDE Preparation Products And Raw materials
Raw materials
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View Lastest Price from 5-METHYL-2-NITROBENZALDEHYDE manufacturers
- Product
- 5-Methyl-2-nitro-benzaldehyde 5858-28-6
- Price
- US $0.00-0.00/KG
- Min. Order
- 10mg
- Purity
- 99%HPLC
- Supply Ability
- 2000tons
- Release date
- 2020-01-15
- Product
- 5-METHYL-2-NITROBENZALDEHYDE 5858-28-6
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-10
- Product
- 5-METHYL-2-NITROBENZALDEHYDE 5858-28-6
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-09