5-METHYL-2-NITROBENZALDEHYDE

Product Name: 5-METHYL-2-NITROBENZALDEHYDE
CAS No.: 5858-28-6
Chemical Name: 5-METHYL-2-NITROBENZALDEHYDE
Synonyms: 2-Nitro-5-methylbenzaldehyde;5-METHYL-2-NITROBENZALDEHYDE;Benzaldehyde, 5-methyl-2-nitro-
CBNumber: CB2839578
Molecular Formula: C8H7NO3
Formula Weight: 165.15
MOL File: 5858-28-6.mol

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5-METHYL-2-NITROBENZALDEHYDE Property

Melting point:: 64 °C
Boiling point:: 314.0±30.0 °C(Predicted)
Density: 1.278±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: Light yellow to green yellow Solid

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Safety

HS Code: 2913000090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B498268
Product name: 5-methyl-2-nitrobenzaldehyde
Packaging: 50mg
Price: $65
Updated: 2021/12/16

TRC

Product number: B498268
Product name: 5-methyl-2-nitrobenzaldehyde
Packaging: 500mg
Price: $350
Updated: 2021/12/16

Oakwood

Product number: 047928
Product name: 5-Methyl-2-nitrobenzaldehyde
Packaging: 250mg
Price: $90
Updated: 2021/12/16

AK Scientific

Product number: 8690AB
Product name: 5-Methyl-2-nitrobenzaldehyde
Packaging: 250mg
Price: $126
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4754-1-15
Product name: 5-Methyl-2-nitrobenzaldehyde
Purity: 98.0%
Packaging: 250mg
Price: $142
Updated: 2021/12/16

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5-METHYL-2-NITROBENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

66424-92-8

5858-28-6

General procedure for the synthesis of 5-methyl-2-nitrobenzaldehyde from 5-methyl-2-nitrobenzyl alcohol: a) 5-methyl-2-nitrobenzyl alcohol (10 g, 59.88 mmol) was dissolved in dichloromethane (210 mL). Subsequently 3A molecular sieves (54 g) and pyridinium dichromate (22.53 g, 59.88 mmol) were added. The reaction mixture was stirred at room temperature for 6 hours. After completion of the reaction, the crude product was filtered through a short silica gel column and concentrated under reduced pressure. The residue was purified by fast column chromatography (silica gel, 10-20% ethyl acetate/hexane as eluent) to afford 7.84 g (79% yield) of the target compound 5-methyl-2-nitrobenzaldehyde as a colorless oil.1H NMR (CDCl3) δ 10.41 (m, 1H), 8.02 (m, 1H), 7.69 (s, 1H), 7.53 (d, 1H). 1H), 2.51 (s, 3H).

References

[1] Patent: US2004/10004, 2004, A1. Location in patent: Page 22
[2] Journal of Organic Chemistry, 1980, vol. 45, # 7, p. 1334 - 1336
[3] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001, vol. 40, # 5, p. 436 - 437
[4] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001, vol. 40, # 4, p. 329 - 330
[5] Bulletin of the Korean Chemical Society, 2011, vol. 32, # 12, p. 4309 - 4315

5-METHYL-2-NITROBENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-METHYL-2-NITROBENZALDEHYDE Suppliers

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View Lastest Price from 5-METHYL-2-NITROBENZALDEHYDE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 5-Methyl-2-nitro-benzaldehyde 5858-28-6
Price: US $0.00-0.00/KG
Min. Order: 10mg
Purity: 99%HPLC
Supply Ability: 2000tons
Release date: 2020-01-15

Zhuozhou Wenxi import and Export Co., Ltd

Product: 5-METHYL-2-NITROBENZALDEHYDE 5858-28-6
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-10

Zhuozhou Wenxi import and Export Co., Ltd

Product: 5-METHYL-2-NITROBENZALDEHYDE 5858-28-6
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-09

5858-28-6, 5-METHYL-2-NITROBENZALDEHYDERelated Search:

4-NITROISOPHTHALIC ACID 5-Methyl-2-nitrobenzoic acid 2-Nitrobenzaldehyde 4,6-DINITRO-1,3-BENZENEDICARBONYL CHLORIDE 4-(ACETYLAMINO)-6-NITRO-1,3-BENZENEDICARBOXYLIC ACID Methyl 3-formyl-4-nitrobenzoate 2-NITRO-5-METHOXYCARBONYL BENZOIC ACID Methyl 5-Methyl-2-Nitrobenzoate 2,4,5-TRIFLUORO-3-METHYL-6-NITROBENZOIC ACID 4,5-DINITROPHTHALIC ACID 4,6-DINITRO-1,3-BENZENEDICARBOXYLIC ACID 3-NITRO-2-NAPHTHOIC ACID, MAGNESIUM SALT-BIS(HEXACHLOROCYCLOPENTADIENE) ADDUCT, TECH. 5-METHYL-2-NITROBENZAMIDE AKOS 243-15 4-(IMIDAZOLYLMETHYL)-1-NITRO-9H-9-XANTHENONE RARECHEM AQ BD 0019 ETHYL 5-METHYL-2-NITROBENZOATE 4-CHLORO-6-NITROISOPHTHALIC ACID

Benzaldehyde, 5-methyl-2-nitro-

5-METHYL-2-NITROBENZALDEHYDE

2-Nitro-5-methylbenzaldehyde

5858-28-6