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5-METHYL-2-NITROBENZALDEHYDE

Product Name
5-METHYL-2-NITROBENZALDEHYDE
CAS No.
5858-28-6
Chemical Name
5-METHYL-2-NITROBENZALDEHYDE
Synonyms
2-Nitro-5-methylbenzaldehyde;5-METHYL-2-NITROBENZALDEHYDE;Benzaldehyde, 5-methyl-2-nitro-
CBNumber
CB2839578
Molecular Formula
C8H7NO3
Formula Weight
165.15
MOL File
5858-28-6.mol
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5-METHYL-2-NITROBENZALDEHYDE Property

Melting point:
64 °C
Boiling point:
314.0±30.0 °C(Predicted)
Density 
1.278±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
Appearance
Light yellow to green yellow Solid
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Safety

HS Code 
2913000090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B498268
Product name
5-methyl-2-nitrobenzaldehyde
Packaging
50mg
Price
$65
Updated
2021/12/16
TRC
Product number
B498268
Product name
5-methyl-2-nitrobenzaldehyde
Packaging
500mg
Price
$350
Updated
2021/12/16
SynQuest Laboratories
Product number
4754-1-15
Product name
5-Methyl-2-nitrobenzaldehyde
Purity
98.0%
Packaging
1g
Price
$454
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0151091
Product name
5-METHYL-2-NITRO-BENZALDEHYDE
Purity
95.00%
Packaging
5MG
Price
$495.95
Updated
2021/12/16
Oakwood
Product number
047928
Product name
5-Methyl-2-nitrobenzaldehyde
Packaging
250mg
Price
$90
Updated
2021/12/16
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5-METHYL-2-NITROBENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

66424-92-8

5858-28-6

General procedure for the synthesis of 5-methyl-2-nitrobenzaldehyde from 5-methyl-2-nitrobenzyl alcohol: a) 5-methyl-2-nitrobenzyl alcohol (10 g, 59.88 mmol) was dissolved in dichloromethane (210 mL). Subsequently 3A molecular sieves (54 g) and pyridinium dichromate (22.53 g, 59.88 mmol) were added. The reaction mixture was stirred at room temperature for 6 hours. After completion of the reaction, the crude product was filtered through a short silica gel column and concentrated under reduced pressure. The residue was purified by fast column chromatography (silica gel, 10-20% ethyl acetate/hexane as eluent) to afford 7.84 g (79% yield) of the target compound 5-methyl-2-nitrobenzaldehyde as a colorless oil.1H NMR (CDCl3) δ 10.41 (m, 1H), 8.02 (m, 1H), 7.69 (s, 1H), 7.53 (d, 1H). 1H), 2.51 (s, 3H).

References

[1] Patent: US2004/10004, 2004, A1. Location in patent: Page 22
[2] Journal of Organic Chemistry, 1980, vol. 45, # 7, p. 1334 - 1336
[3] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001, vol. 40, # 5, p. 436 - 437
[4] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001, vol. 40, # 4, p. 329 - 330
[5] Bulletin of the Korean Chemical Society, 2011, vol. 32, # 12, p. 4309 - 4315

5-METHYL-2-NITROBENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-METHYL-2-NITROBENZALDEHYDE Suppliers

China 48 India 1 United States 7 Global 56
A.J Chemicals
Tel
--
Fax
--
Email
sales@ajchem.in
Country
India
ProdList
6100
Advantage
58
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View Lastest Price from 5-METHYL-2-NITROBENZALDEHYDE manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
5-Methyl-2-nitro-benzaldehyde 5858-28-6
Price
US $0.00-0.00/KG
Min. Order
10mg
Purity
99%HPLC
Supply Ability
2000tons
Release date
2020-01-15
Zhuozhou Wenxi import and Export Co., Ltd
Product
5-METHYL-2-NITROBENZALDEHYDE 5858-28-6
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-10
Zhuozhou Wenxi import and Export Co., Ltd
Product
5-METHYL-2-NITROBENZALDEHYDE 5858-28-6
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-09

5858-28-6, 5-METHYL-2-NITROBENZALDEHYDERelated Search:

4-NITROISOPHTHALIC ACID 5-Methyl-2-nitrobenzoic acid 2-Nitrobenzaldehyde 4,6-DINITRO-1,3-BENZENEDICARBONYL CHLORIDE 4-(ACETYLAMINO)-6-NITRO-1,3-BENZENEDICARBOXYLIC ACID Methyl 3-formyl-4-nitrobenzoate 2-NITRO-5-METHOXYCARBONYL BENZOIC ACID Methyl 5-Methyl-2-Nitrobenzoate 2,4,5-TRIFLUORO-3-METHYL-6-NITROBENZOIC ACID 4,5-DINITROPHTHALIC ACID 4,6-DINITRO-1,3-BENZENEDICARBOXYLIC ACID 3-NITRO-2-NAPHTHOIC ACID, MAGNESIUM SALT-BIS(HEXACHLOROCYCLOPENTADIENE) ADDUCT, TECH. 5-METHYL-2-NITROBENZAMIDE AKOS 243-15 4-(IMIDAZOLYLMETHYL)-1-NITRO-9H-9-XANTHENONE RARECHEM AQ BD 0019 ETHYL 5-METHYL-2-NITROBENZOATE 4-CHLORO-6-NITROISOPHTHALIC ACID

  • Benzaldehyde, 5-methyl-2-nitro-
  • 5-METHYL-2-NITROBENZALDEHYDE
  • 2-Nitro-5-methylbenzaldehyde
  • 5858-28-6