ChemicalBook > CAS DataBase List > tert-Butyl 3S-amino-2,3,4,5-tetrahydro-1H-[1]benaepin-2-one-1-acetate tartrate

tert-Butyl 3S-amino-2,3,4,5-tetrahydro-1H-[1]benaepin-2-one-1-acetate tartrate

Product Name
tert-Butyl 3S-amino-2,3,4,5-tetrahydro-1H-[1]benaepin-2-one-1-acetate tartrate
CAS No.
117770-66-8
Chemical Name
tert-Butyl 3S-amino-2,3,4,5-tetrahydro-1H-[1]benaepin-2-one-1-acetate tartrate
Synonyms
tert-Butyl 3S-amino-2,3,4,5-tetrahydro-1H-[1]benaepin-2-one-...;T-BUTYL 3S-AMINO-2,3,4,5-TETRAHYDRO-1H-1BENAEPIN-2-ONE-1-ACETATE-TARTRATE;tert-Butyl 3S-amino-2,3,4,5-tetrahydro-1H-[1]benaepin-2-one-1-acetate tartrate;tert-butyl 2-(3-amino-2-oxo-4,5-dihydro-3H-1-benzazepin-1-yl)acetate,2,3-dihydroxybutanedioic acid;(S)-tert-Butyl 2-(3-aMino-2-oxo-2,3,4,5-tetrahydro-1H-benzo[b]azepin-1-yl)acetate (2R,3R)-2,3-dihydroxysuccinate;1H-1-Benzazepine-1-acetic acid, 3-aMino-2,3,4,5-tetrahydro-2-oxo-, 1,1-diMethylethyl ester, (3S)-, (2R,3R)-2,3-dihydroxybutanedioate (1:1) (9CI)
CBNumber
CB2855071
Molecular Formula
C16H22N2O3.C4H6O6
Formula Weight
440.446
MOL File
117770-66-8.mol
More
Less

tert-Butyl 3S-amino-2,3,4,5-tetrahydro-1H-[1]benaepin-2-one-1-acetate tartrate Property

Melting point:
190°C (dec.)
More
Less

Hazard and Precautionary Statements (GHS)

More
Less

N-Bromosuccinimide Price

American Custom Chemicals Corporation
Product number
CHM0077493
Product name
(3-AMINO-2-OXO-2,3,4,5-TETRAHYDRO-BENZO[B]AZEPIN-1-YL)-ACETIC ACID TERT-BUTYL ESTER
Purity
95.00%
Packaging
5G
Price
$1370.41
Updated
2021/12/16
Crysdot
Product number
CD11340245
Product name
(S)-tert-Butyl2-(3-amino-2-oxo-2,3,4,5-tetrahydro-1H-benzo[b]azepin-1-yl)acetate(2R,3R)-2,3-dihydroxysuccinate
Purity
95+%
Packaging
1000g
Price
$513
Updated
2021/12/16
More
Less

tert-Butyl 3S-amino-2,3,4,5-tetrahydro-1H-[1]benaepin-2-one-1-acetate tartrate Chemical Properties,Usage,Production

Preparation

The preparation of the tert-Butyl 3S-amino-2,3,4,5-tetrahydro-1H-benaepin-2-one-1-acetate tartrate is as follows:Chiral Resolution Of Highly Pure (+1-T-BUTYLOX CARBONYLMETHYL-3-AMINO- 2, 3, 4N5-TETRAHYDRO-LH-[L] BENZAZEPIN-2-ONE USING Tartaric Acid Part A: Preparation of Highly Pure (S)-L-T-BUTYLOXYCARBONYLMETHYL-3-AMINO- 2,3, 4, 5-Tetrahydro-lh- [l] Benzazepin-2-One Tartrate Salt of Formula V Highly pure 1-t-butyloxycarbonylmethyl-3-amino-2, 3, 4, 5-TETRAHYDRO-LH- BENZAZEPIN-2-ONE of Formula II (5.0 g, 17.24 mmol) was heated in ethanol (12.5 ml) at 50-55°C for 25 minutes. The temperature was further raised to 60-65°C and to this was added a solution of L- (+)-tartaric acid (1.8g, 11.9mmol) in ethanol (7.5ml). The reaction mixture was stirred for 24 hours at 60-65°C, allowed to cool to 35-37°C and filtered at the same temperature to afford the crude product (2.75g, 72%). This was suspended in alcohol (11ml) and stirred at 62-65°C for 3 hours, allowed to cool to 45-47°C and filtered to afford the title compound. Yield: 2.55 g, 93% Purity: 99.87%

tert-Butyl 3S-amino-2,3,4,5-tetrahydro-1H-[1]benaepin-2-one-1-acetate tartrate Preparation Products And Raw materials

Raw materials

Preparation Products

More
Less

tert-Butyl 3S-amino-2,3,4,5-tetrahydro-1H-[1]benaepin-2-one-1-acetate tartrate Suppliers

Austria 1 China 52 Germany 1 United Kingdom 1 United States 4 Global 59
Zhejiang Karry Pharmachem Co., Ltd.
Tel
19157666807
Email
info@karrypharma.com
Country
China
ProdList
37
Advantage
58
XiaoGan ShenYuan ChemPharm co,ltd
Tel
15527768850
Email
1791901229@qq.com
Country
China
ProdList
8849
Advantage
52
Tianjin heowns Biochemical Technology Co., Ltd.
Tel
400 638 7771
Email
sales@heowns.com
Country
China
ProdList
14443
Advantage
57
Cantotech Chemicals, Ltd.
Tel
86-0755-86635001
Fax
86-0755-22642228
Email
cantotech@126.com
Country
China
ProdList
4576
Advantage
55
Wuhan Dahua Pharmaceutical Co., Ltd.
Tel
027-59262863 13277907145 3091977954
Fax
027-59420980
Country
China
ProdList
4951
Advantage
58
Shanghai YuLue Chemical Co., Ltd.
Tel
021-60345187 13671753212
Fax
021-34702061
Email
lzz841106@aliyun.com
Country
China
ProdList
10287
Advantage
55
Shanghai QianJin Chemical Technology Co., Ltd
Tel
021-20900665 17321230821
Fax
021-20900665
Email
2986274987@qq.com
Country
China
ProdList
982
Advantage
55
Shanghai Uchem Inc.
Tel
15618758386 15618758386
Fax
QQ:3004479444
Email
sales3@myuchem.com
Country
China
ProdList
2018
Advantage
55
Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
Email
sales@amadischem.com
Country
China
ProdList
131981
Advantage
58
Shandong Ono Chemical Co., Ltd.
Tel
0539-6362799 20）
Fax
0539-6362799（To 20）
Country
China
ProdList
9998
Advantage
58
Capot Chemical Co.,Ltd.
Tel
571-85586718 +8613336195806
Fax
+86-571-85864795
Email
sales@capotchem.com
Country
China
ProdList
29797
Advantage
60
Wuhan FengyaoTonghui Chemical Products Co., Ltd.
Tel
027-87466105 15377573527
Email
2678564200@qq.com
Country
China
ProdList
17997
Advantage
58
Tianjin heowns Biochemical Technology Co., Ltd.
Tel
400-6387771-6038 18902104717
Email
sales@heowns.com
Country
China
ProdList
20532
Advantage
60
Hubei Xinyuanshun Pharmaceutical Chemical Co., Ltd.
Tel
027-51831887 15337167856
Fax
027-51837635 QQ1165326703
Email
hubeixinyuanshun@163.com
Country
China
ProdList
10305
Advantage
58
Hefei TNJ Chemical Industry Co.,Ltd.
Tel
0551-65418684 +8618949823763
Fax
0086-551-65418684
Email
sales@tnjchem.com
Country
China
ProdList
25363
Advantage
58
Dayang Chem (Hangzhou) Co.,Ltd.
Tel
571-88938639 +8617705817739
Fax
+86-571-88938652，+86-571- 88492614
Email
info@dycnchem.com
Country
CHINA
ProdList
52867
Advantage
58
AFINE CHEMICALS LIMITED
Tel
0571-85134551 18958018566;
Fax
008657185134895
Email
info@afinechem.com
Country
China
ProdList
15377
Advantage
58
Hubei Jusheng Technology Co.,Ltd.
Tel
18871490254
Fax
027-59599243
Email
linda@hubeijusheng.com
Country
CHINA
ProdList
28180
Advantage
58
Wuhan xinyangruihe Chemical Technology Co., Ltd.
Tel
027-83855313 15307155313
Fax
QQ：2274366233
Email
2274366233@qq.com
Country
China
ProdList
5661
Advantage
58
Shanghai Yanze Chemical Co., Ltd.
Tel
021-13773155751 19901447308
Email
260924549@qq.com
Country
China
ProdList
8709
Advantage
58
Chongqing Chemdad Co., Ltd
Tel
+86-023-61398051 +8613650506873
Email
sales@chemdad.com
Country
China
ProdList
39916
Advantage
58
Zhejiang zetian fine chemical co. LTD
Tel
0571-87322520 18957127338
Email
June@zetchem.com
Country
China
ProdList
398
Advantage
58
CONIER CHEM AND PHARMA LIMITED
Tel
+8618523575427
Email
sales@conier.com
Country
China
ProdList
49391
Advantage
58
Shanghai Haohong Pharmaceutical Co., Ltd.
Tel
4008210725 4008210725
Email
malulu@leyan.com
Country
China
ProdList
55023
Advantage
58
Zhongxin Chenshi (Wuhan) Technology Co., Ltd
Tel
18942922096
Fax
QQ 2662561040
Email
2662561040@qq.com
Country
China
ProdList
1002
Advantage
58
Suzhou QIHANG Biotechnology Co., Ltd
Tel
18662190603
Email
437347250@qq.com
Country
China
ProdList
4677
Advantage
58
Mainchem Co., Ltd.
Tel
--
Fax
--
Email
sarah@mainchem.com
Country
China
ProdList
6572
Advantage
58
Shanghai UCHEM Inc.
Tel
18939844854 18939844854
Fax
QQ3004479448
Email
sales6@myuchem.com
Country
China
ProdList
3125
Advantage
58
Wuhan haorong Biotechnology Co., Ltd
Tel
13217229939
Email
773651767@qq.com
Country
China
ProdList
4732
Advantage
58
Shaanxi DIDU pharmaceutical and Chemical Co., Ltd
Tel
17691182729 18161915376
Email
1046@dideu.com
Country
China
ProdList
10010
Advantage
58
WEITIXIHAUGONG
Tel
0371-53370800 18037197114
Email
2853031799@qq.com
Country
China
ProdList
10006
Advantage
58
Wuhan Fengyao Tonghui Chemical Products Co. LTD
Tel
027-87466205 15377579727
Email
1228964013@qq.com
Country
China
ProdList
8561
Advantage
58
Tiantai Yisheng Biochemical Technology Co., Ltd
Tel
18958639818
Email
156697457@qq.com
Country
China
ProdList
118
Advantage
58
Henan Tianfu Chemical Co.,Ltd.
Tel
+86-0371-55170693 +86-19937530512
Fax
0371-55170693
Email
info@tianfuchem.com
Country
China
ProdList
21689
Advantage
55
Shanghai Daken Advanced Materials Co.,Ltd
Tel
+86-371-66670886
Email
forrest.lee@dakenchem.com
Country
China
ProdList
15956
Advantage
58
Zhejiang ZETian Fine Chemicals Co. LTD
Tel
18957127338
Email
stella@zetchem.com
Country
China
ProdList
2141
Advantage
58
Hangzhou FandaChem Co.,Ltd.
Tel
008657128800458; +8615858145714
Fax
+86-571-56059825
Email
fandachem@gmail.com
Country
China
ProdList
9341
Advantage
55
career henan chemical co
Tel
+86-0371-86658258
Email
sales@coreychem.com
Country
China
ProdList
29914
Advantage
58
Changzhou AniKare Pharmatech Co., Ltd.
Tel
+86-0519-8359-8696 +8618018249389
Email
sales@anikare.com
Country
China
ProdList
8469
Advantage
58
Zhejiang Karry Pharmachem Co., Ltd.
Tel
+8613567161161
Email
info@karrypharma.com
Country
China
ProdList
34
Advantage
58
GIHI CHEMICALS CO.,LIMITED
Tel
+8618058761490
Email
info@gihichemicals.com
Country
China
ProdList
50000
Advantage
58
ZHEJIANG JIUZHOU CHEM CO., LTD
Tel
+86-0576225566889 +86-13454675544
Email
admin@jiuzhou-chem.com；jamie@jiuzhou-chem.com；alice@jiuzhou-chem.com
Country
China
ProdList
19949
Advantage
58
PT CHEM GROUP LIMITED
Tel
+86-85511178 +86-85511178
Email
peter68@ptchemgroup.com
Country
China
ProdList
35453
Advantage
58
Shanghai Yubai Biotechnology Co., Ltd.
Tel
--
Fax
--
Email
rongbai_sh021@163.com
Country
CHINA
ProdList
6723
Advantage
58
Zhejiang Xinsanhe Pharmaceutical Chemical Co., Ltd.
Tel
--
Fax
--
Email
sales@sanhechem.com
Country
CHINA
ProdList
16
Advantage
58
Shanghai Titanchem Co., Ltd.
Tel
--
Fax
--
Email
hua.zhang@titanchem.com
Country
China
ProdList
1456
Advantage
30
More
Less

View Lastest Price from tert-Butyl 3S-amino-2,3,4,5-tetrahydro-1H-[1]benaepin-2-one-1-acetate tartrate manufacturers

Career Henan Chemical Co
Product
tert-Butyl 3S-amino-2,3,4,5-tetrahydro-1H-[1]benaepin-2-one-1-acetate tartrate 117770-66-8
Price
US $7.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
100kg
Release date
2018-12-25

117770-66-8, tert-Butyl 3S-amino-2,3,4,5-tetrahydro-1H-[1]benaepin-2-one-1-acetate tartrateRelated Search:

Isobutyl acetate Vinyl acetate Butyl acetate tert-Butanol Glycine Sodium acetate Iminodiacetic acid tert-Butyl bromoacetate Glatiramer acetate tert-Butyl acetate Ethyl acetate Tocopheryl acetate Nitrilotriacetic acid DL-sec-Butyl acetate tert-Butyl chloroacetate tert-Butyl peroxyacetate Dimethylaminoethanol bitartrate ACETATE

  • tert-butyl 2-(3-amino-2-oxo-4,5-dihydro-3H-1-benzazepin-1-yl)acetate,2,3-dihydroxybutanedioic acid
  • 1H-1-Benzazepine-1-acetic acid, 3-aMino-2,3,4,5-tetrahydro-2-oxo-, 1,1-diMethylethyl ester, (3S)-, (2R,3R)-2,3-dihydroxybutanedioate (1:1) (9CI)
  • (S)-tert-Butyl 2-(3-aMino-2-oxo-2,3,4,5-tetrahydro-1H-benzo[b]azepin-1-yl)acetate (2R,3R)-2,3-dihydroxysuccinate
  • tert-Butyl 3S-amino-2,3,4,5-tetrahydro-1H-[1]benaepin-2-one-1-acetate tartrate
  • T-BUTYL 3S-AMINO-2,3,4,5-TETRAHYDRO-1H-1BENAEPIN-2-ONE-1-ACETATE-TARTRATE
  • tert-Butyl 3S-amino-2,3,4,5-tetrahydro-1H-[1]benaepin-2-one-...
  • 117770-66-8
  • C16H22N2O3C4H6O6