ChemicalBook > CAS DataBase List > Carbamic acid, (3-pyrrolidinylmethyl)-, 1,1-dimethylethyl ester, (S)- (9CI)

Carbamic acid, (3-pyrrolidinylmethyl)-, 1,1-dimethylethyl ester, (S)- (9CI)

Product Name
Carbamic acid, (3-pyrrolidinylmethyl)-, 1,1-dimethylethyl ester, (S)- (9CI)
CAS No.
173340-26-6
Chemical Name
Carbamic acid, (3-pyrrolidinylmethyl)-, 1,1-dimethylethyl ester, (S)- (9CI)
Synonyms
(S)-3-(Boc-aminomethyl)py...;(S)-tert-butyl pyrrolidin-3-ylmethylcarbamate;tert-butyl ((S)-pyrrolidin-3-yl)MethylcarbaMate;tert-butyl N-[(3S)-pyrrolidin-3-ylmethyl]carbamate;(S)-3-N-Boc-aminomethyl pyrrolidine, CAS 173340-26-6;Carbamic acid, (3-pyrrolidinylmethyl)-, 1,1-dimethylethyl es...;(S)-(3-Pyrrolidinylmethyl)-carbamic acid 1,1-dimethylethyl ester;Carbamic acid, N-[(3S)-3-pyrrolidinylmethyl]-, 1,1-dimethylethyl ester;Carbamic acid, (3-pyrrolidinylmethyl)-, 1,1-dimethylethyl ester, (S)- (9CI)
CBNumber
CB31051644
Molecular Formula
C10H20N2O2
Formula Weight
200.28
MOL File
173340-26-6.mol
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Carbamic acid, (3-pyrrolidinylmethyl)-, 1,1-dimethylethyl ester, (S)- (9CI) Property

Boiling point:
303.9±15.0 °C(Predicted)
Density 
0.997
storage temp. 
2-8°C(protect from light)
pka
12.71±0.46(Predicted)
Appearance
Colorless to light yellow Liquid
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Safety

HS Code 
2933998090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC
Product number
B124263
Product name
(S)-tert-butylpyrrolidin-3-ylmethylcarbamate
Packaging
500mg
Price
$265
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB144351
Product name
(S)-tert-Butyl (pyrrolidin-3-ylmethyl)carbamate
Packaging
500mg
Price
$80
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB144351
Product name
(S)-tert-Butyl (pyrrolidin-3-ylmethyl)carbamate
Packaging
1g
Price
$140
Updated
2021/12/16
Activate Scientific
Product number
AS51128
Product name
(S)-3-(N-Boc-aminomethyl)pyrrolidine
Purity
95+% ee
Packaging
1g
Price
$214
Updated
2021/12/16
Matrix Scientific
Product number
070421
Product name
(S)-Pyrrolidin-3-ylmethyl-carbamic acid tert-butyl ester
Purity
97%
Packaging
1g
Price
$225
Updated
2021/12/16
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Carbamic acid, (3-pyrrolidinylmethyl)-, 1,1-dimethylethyl ester, (S)- (9CI) Chemical Properties,Usage,Production

Synthesis

173340-24-4

173340-26-6

General procedure for the synthesis of (S)-3-N-Boc-aminomethylpyrrolidine from (3R)-1-[(1S)-1-phenylethyl]-3-pyrrolidinylmethyl]carbamic acid,1,1-dimethylethyl ester (9CI): tert-butyl [1-(1-phenylethyl)-pyrrolidin-3-ylmethyl]-carbamate (3.50 g, 11.5 mmol) was dissolved in methanol in methanol, 20% Pd/C catalyst was added and the hydrogenation reaction was carried out under hydrogen pressure of 50 psi.After 24 h, the reaction mixture was filtered and concentrated to afford 1.75 g (S)-3-N-Boc-aminomethylpyrrolidine (yield: 76%). Mass spectrometry analysis (APCI+): m/z 201 ([M+H]+).

References

[1] Patent: WO2005/49602, 2005, A1. Location in patent: Page/Page column 88; 89; 124
[2] Patent: WO2005/49605, 2005, A1. Location in patent: Page/Page column 116; 117; 152

Carbamic acid, (3-pyrrolidinylmethyl)-, 1,1-dimethylethyl ester, (S)- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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Carbamic acid, (3-pyrrolidinylmethyl)-, 1,1-dimethylethyl ester, (S)- (9CI) Suppliers

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View Lastest Price from Carbamic acid, (3-pyrrolidinylmethyl)-, 1,1-dimethylethyl ester, (S)- (9CI) manufacturers

Career Henan Chemical Co
Product
(S)-tert-Butyl (pyrrolidin-3-ylmethyl)carbamate 173340-26-6
Price
US $1.00/g
Min. Order
1g
Purity
99%
Supply Ability
10000KGS
Release date
2020-01-09

173340-26-6, Carbamic acid, (3-pyrrolidinylmethyl)-, 1,1-dimethylethyl ester, (S)- (9CI)Related Search:

Tert-butyl 2,6-diazaspiro[3.4]octane-2-carboxylate (R)-1-BENZYL-3-N-BOC-AMINOMETHYL PYRROLIDINE (cis)-5-Boc-Hexahydro-pyrrolo[3,4-b]pyrrole R-1-CBZ-3-(BOC-AMINOMETHYL)-PYRROLIDINE Carbamic acid, (3-pyrrolidinylmethyl)-, 1,1-dimethylethyl ester, (S)- (9CI) cis-2-Boc-hexahydropyrrolo[3,4-c]pyrrole TERT-BUTYL 2,6-DIAZABICYCLO[2.2.1]HEPTANE-2-CARBOXYLATE TERT-BUTYL ([(3S,4R)-4-PHENYLPYRROLIDIN-3-YL]METHYL)CARBAMATE CIS-5-BENZYL-2-BOC-HEXAHYDROPYRROLO[3,4-C]PYRROLE

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