ChemicalBook > CAS DataBase List > 4-AMINO-3-BROMO-5-NITROPYRIDINE

4-AMINO-3-BROMO-5-NITROPYRIDINE

Product Name: 4-AMINO-3-BROMO-5-NITROPYRIDINE
CAS No.: 89284-05-9
Chemical Name: 4-AMINO-3-BROMO-5-NITROPYRIDINE
Synonyms: 4-AMino-3-broMo-5-nitropy...;3-bromo-5-nitro-4-pyridinamine;4-AMino-3-nitro-5-broMopyridine;4-AMINO-3-BROMO-5-NITROPYRIDINE;3-Bromo-4-amino-5-nitropyridine;4-Pyridinamine, 3-bromo-5-nitro-;4-Amino-3-bromo-5-nitropyridine 97%;4-AMINO-3-BROMO-5-NITROPYRIDINE ISO 9001：2015 REACH
CBNumber: CB31076135
Molecular Formula: C5H4BrN3O2
Formula Weight: 218.01
MOL File: 89284-05-9.mol

Less

4-AMINO-3-BROMO-5-NITROPYRIDINE Property

Melting point:: 174-175℃
Boiling point:: 346.5±37.0 °C(Predicted)
Density: 1.929
refractive index: 1.682
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
form: claggy powder
pka: 2.87±0.24(Predicted)
color: Amber/gold
InChI: InChI=1S/C5H4BrN3O2/c6-3-1-8-2-4(5(3)7)9(10)11/h1-2H,(H2,7,8)
InChIKey: UXDLBXRMNSJEPB-UHFFFAOYSA-N
SMILES: C1=NC=C([N+]([O-])=O)C(N)=C1Br

Less

Safety

HS Code: 2933399990

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

Less

N-Bromosuccinimide Price

TRC

Product number: A602458
Product name: 4-Amino-3-bromo-5-nitropyridine
Packaging: 1g
Price: $75
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H55-9-02
Product name: 4-Amino-3-bromo-5-nitropyridine
Packaging: 1g
Price: $75
Updated: 2021/12/16

AK Scientific

Product number: W9221
Product name: 3-Bromo-5-nitropyridin-4-amine
Packaging: 5g
Price: $78
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB139502
Product name: 3-Bromo-5-nitropyridin-4-amine
Packaging: 5G
Price: $110
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0037552
Product name: 4-AMINO-3-BROMO-5-NITROPYRIDINE
Purity: 95.00%
Packaging: 50MG
Price: $117.6
Updated: 2021/12/16

Less

4-AMINO-3-BROMO-5-NITROPYRIDINE Chemical Properties,Usage,Production

Synthesis

1681-37-4

89284-05-9

The general procedure for the synthesis of 4-amino-3-bromo-5-nitropyridine from 4-amino-3-nitropyridine was as follows: 3-nitropyridin-4-amine (LXVIII) (10 g, 71.88 mmol) was mixed with acetic acid (100 ml) in a sealed tube, followed by the addition of sodium acetate (NaOAc) (29.50 g, 359 mmol), and the slow dropwise addition of bromine ( 4.43 ml, 86.3 mmol). The sealed tube was heated at 100 °C for overnight reaction under stirring conditions. Upon completion of the reaction, the mixture was concentrated under vacuum and the resulting solid was dissolved in water, alkalized with saturated aqueous sodium bicarbonate (NaHCO3) and extracted with dichloromethane (DCM). The organic phases were combined, dried and concentrated to give 3-bromo-5-nitropyridin-4-amine (LXIX) as a yellow solid (13.7 g, 62.8 mmol, 87% yield). The product was identified by 1H NMR (DMSO-d6, 500 MHz): δ 8.58 (s, 1H), 9.19 (s, 1H); ESIMS analysis showed the molecular ion peak m/z 218.1 (M + H), corresponding to the molecular formula C5H4BrN3O2.

References

[1] Patent: US2013/296302, 2013, A1. Location in patent: Paragraph 0563
[2] Patent: WO2011/84486, 2011, A1. Location in patent: Page/Page column 119-120
[3] Patent: US2013/267495, 2013, A1. Location in patent: Paragraph 0460-0461
[4] Patent: EP2464232, 2015, B1. Location in patent: Paragraph 0087; 0088
[5] Patent: US2016/68548, 2016, A1. Location in patent: Paragraph 0852

4-AMINO-3-BROMO-5-NITROPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

Less

4-AMINO-3-BROMO-5-NITROPYRIDINE Suppliers

China 112 Germany 1 India 1 United Kingdom 2 United States 9 Global 125

Alichem(Changzhou) Co., Ltd.

Tel: 19941333411
Fax: QQ:749741756
Email: sales@alichem.cn
Country: China
ProdList: 523
Advantage: 58

ShangHai DEMO Chemical Co.,Ltd

Tel: 400-021-7337 2355568890
Fax: 0086-21-50182339
Email: sales@demochem.com
Country: China
ProdList: 2572
Advantage: 57

Capot Chemical Co., Ltd

Tel: +86 (0) 571 85 58 67 18
Fax: 0086-571-85864795
Country: China
ProdList: 18207
Advantage: 66

JinYan Chemicals(ShangHai) Co.,Ltd.

Tel: 13817811078
Fax: 86-021-50426522,50426273
Email: sales@jingyan-chemical.com
Country: China
ProdList: 9976
Advantage: 60

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
Email: info@hanhongsci.com
Country: China
ProdList: 42934
Advantage: 64

Nan Jing Dirise Chemcial Co.,LTD

Tel: 025-52161033 15312098939
Fax: 025-83254025
Email: sales@njdrschem.com
Country: China
ProdList: 579
Advantage: 64

Jinan Trio PharmaTech Co., Ltd.

Tel: 0531-88811783
Fax: +86 (531) 55696010 QQ 1762738062
Email: sales@trio-pharmatech.com
Country: China
ProdList: 1856
Advantage: 62

PSN Pharmaceutical Technology Co., Ltd.

Tel: 86-25-57062118
Fax: 86-25-57065896
Email: sales@jspsn.com
Country: China
ProdList: 496
Advantage: 57

China Langchem Inc.

Tel: 0086-21-58956006
Fax: 0086-21-58956100
Country: China
ProdList: 7811
Advantage: 57

Wuhan Arike Technology Co., Ltd.

Tel: 027- 51832457 94518350
Fax: E-Mail Inquiry
Country: China
ProdList: 746
Advantage: 62

Shanghai Sphchem Co., Ltd.

Tel: 021-56491756 13512199871
Fax: 021-5649-1756
Email: 2819742715@qq.com
Country: China
ProdList: 4000
Advantage: 55

Shanghai Topbiochem Technology Co., Ltd

Tel: +86-21-60341587
Fax: +86-21-61294319
Email: sales@topbiochem.com
Country: China
ProdList: 6175
Advantage: 58

Shanghai T&W Pharmaceutical Co., Ltd.

Tel: +86 21 61551611
Fax: +86 21 50676805
Country: China
ProdList: 9891
Advantage: 58

Nanjing Norris-Pharm Technology Co., Ltd

Tel: 18652989687
Fax: +86-25-52131256
Email: sales@norris-pharm.com
Country: China
ProdList: 8878
Advantage: 55

Shanghai Synmedia Chemical Co., Ltd.

Tel: 021-38681880 13817889927
Fax: 0213390-8196
Email: sales@synmedia-chem.com
Country: China
ProdList: 249
Advantage: 58

REBO Biochemical Technology Limited

Tel: +86-15861285899
Fax: +86-518-86661625
Email: sales@rebobiochem.com
Country: China
ProdList: 100
Advantage: 55

CEG Chemical Science&Technology Co., Ltd.

Tel: Mobile:13665161512
Fax: +86-510-68873513
Country: China
ProdList: 1785
Advantage: 58

Bide Pharmatech Ltd.

Tel: 400-164-7117 13681763483
Fax: +86-21-61629029
Email: product02@bidepharm.com
Country: China
ProdList: 39966
Advantage: 60

ShangHai Yuchuan Pharmaceutical Technology Co., Ltd.

Tel: 02161555100
Fax: -
Country: China
ProdList: 820
Advantage: 58

Shanghai HuanChuan Industry Co.,Ltd.

Tel: 021-61478794
Fax: 021-61478794
Email: sales@hcshhai.com
Country: China
ProdList: 9793
Advantage: 50

Shanghai Yongye Biotechnology Co., Ltd.

Tel: 86-021-61559134 15921386130
Fax: 021-55068248
Email: 3423497944@qq.com
Country: China
ProdList: 8144
Advantage: 55

Nanjing Duolong Bio-tech Co.,Ltd.

Tel: 18905173768
Fax: 025-83263139
Email: 52513593@qq.com
Country: China
ProdList: 2331
Advantage: 50

Shanghai Jovan Biochemical Technology Co. Ltd.

Tel: +86-021-61654350
Fax: +86-021-61654350
Email: 1245958370@qq.com
Country: China
ProdList: 2982
Advantage: 50

Nanjing Chalf-Pharm Technology Co., Ltd.

Tel: 025-57018978 18251899859
Fax: 025-57018008
Email: sales@chalf-pharm.com
Country: China
ProdList: 5674
Advantage: 50

Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.

Tel: 025-66028182 18626450290
Email: yftan@aikonchem.com
Country: China
ProdList: 16679
Advantage: 50

Cool Pharm, Ltd

Tel: 021-60455363 18019463053
Fax: 50966098
Email: sales@coolpharm.com
Country: China
ProdList: 12346
Advantage: 58

Jiangsu Mingchem Corporation

Tel: 0519-85170101
Fax: 0519-85170505
Email: sales@mingchem.com
Country: China
ProdList: 608
Advantage: 55

Nanjing Huang Tai Pharmaceutical Technology Co. Ltd.

Tel: 025-58803135 18551845925
Fax: 025-58803650
Email: 3569572487@qq.com
Country: China
ProdList: 337
Advantage: 58

Shanghai Carlow Chemicals Co., Ltd.

Tel: 21-33526724 18930996265
Fax: +86 21 37023730
Email: info@carlowchem.com
Country: China
ProdList: 1969
Advantage: 50

Hubei Chuangliankangcheng Pharmaceutical Co., Ltd.

Tel: 027-65388397 18164111589
Fax: 027-65388397
Email: 3321478047@qq.com
Country: China
ProdList: 2007
Advantage: 55

Shanghai Brain Biotechnology Co., Ltd.

Tel: 13564638271
Fax: 021-68948280
Email: shhjiang1977@163.com
Country: China
ProdList: 2987
Advantage: 55

Shanghai YuanYe Biotechnology Co., Ltd.

Tel: 021-61312847; 18021002903
Fax: QQ:3008007432
Email: 3008007409@qq.com
Country: China
ProdList: 71826
Advantage: 60

ChengDu TongChuangYuan Pharmaceutical Co.Ltd

Tel: 028-83379370 13880556291
Fax: 028-87747383
Email: tcy@tcypharm.com
Country: China
ProdList: 7218
Advantage: 58

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Shanghai CR Corporation Limited

Tel: 13062833949; 4006653949 4006653949
Fax: QQ: 2136646215
Email: fred.wen@crcorporation.cn
Country: China
ProdList: 9756
Advantage: 58

Nanijing m&m biotechnology Co. ,Ltd.

Tel: 025-87782433 18021532344
Fax: 025-87782433
Email: 1345332203@qq.com
Country: China
ProdList: 4134
Advantage: 58

Hangzhou Molcore Biopharmatech Co.,Ltd

Tel: 400-711-5280 86-571-81025280
Fax: 86-571-85806285
Email: sales@molcore.com
Country: China
ProdList: 9967
Advantage: 58

Changzhou Ditong chemical Co.,Ltd.

Tel: 0519-88298848 18118010980
Fax: 0519-85130733
Email: info@edengenechem.com
Country: China
ProdList: 736
Advantage: 58

Shanghai Zhen Li Biological Technology Co., Ltd

Tel: 021-16621358918; 18516310516
Fax: 13045646768
Email: zhenlipharma888@163.com
Country: China
ProdList: 19035
Advantage: 58

Capot Chemical Co.,Ltd.

Tel: +86-（0）57185586718; +8613336195806
Fax: +86-571-85864795
Email: sales@capot.com
Country: China
ProdList: 29735
Advantage: 60

Wuhan FengyaoTonghui Chemical Products Co., Ltd.

Tel: 027-87466105 15377573527
Email: 2678564200@qq.com
Country: China
ProdList: 17987
Advantage: 58

Shanghai Haohong Pharmaceutical Co., Ltd.

Tel: 400-8210725 400821072
Fax: 021-58955996
Email: malulu@leyan.com
Country: China
ProdList: 25000
Advantage: 58

Suzhou Devi Pharma Technology Co., Ltd.

Tel: 0512-66565816 18651107528
Fax: 0512-66565816
Country: China
ProdList: 1040
Advantage: 58

Shanghai SPAR pharmaceutical technology co., LTD

Tel: 021-000000 13917643586;
Email: admin@jingshipharmatech.com
Country: China
ProdList: 9855
Advantage: 58

Shanghai Jizhi Biochemical Technology Co. Ltd.

Tel: 4009004166/18616739031 18616739031
Email: 3007523370@qq.com
Country: China
ProdList: 52687
Advantage: 58

Shanghai Moss Medicine Technology Co., Ltd.

Tel: +86-188369842 +86-15618151133
Fax: QQ188369842
Email: 188369842@qq.com
Country: China
ProdList: 1959
Advantage: 58

Fuxin Crest Biotechnology Co. Ltd.

Tel: 13062833949
Fax: QQ: 2073772974
Email: fred.wen@crcorporation.cn
Country: China
ProdList: 853
Advantage: 58

Nanjing Asfam Pharmaceutical Technology Co., Ltd.

Tel: 025-58867862 18751812725
Fax: 02558867862
Email: sales@ace-pharm.com
Country: China
ProdList: 1985
Advantage: 58

CR Corporation Limited

Tel: +8613062833949
Email: fred.wen@crcorporation.cn
Country: China
ProdList: 8645
Advantage: 58

ANHUI WITOP BIOTECH CO., LTD

Tel: +8615255079626
Email: eric@witopchemical.com
Country: China
ProdList: 23541
Advantage: 58

Less

View Lastest Price from 4-AMINO-3-BROMO-5-NITROPYRIDINE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 4-Amino-3-bromo-5-nitropyridine 89284-05-9
Price: US $1.00-1.00/Kg/Drum
Min. Order: 1g
Purity: 98%
Supply Ability: 50tons
Release date: 2020-05-12

Dideu Industries Group Limited

Product: 4-AMINO-3-BROMO-5-NITROPYRIDINE 89284-05-9
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons min
Release date: 2021-09-08

Career Henan Chemical Co

Product: 4-AMINO-3-BROMO-5-NITROPYRIDINE 89284-05-9
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 1000KGS
Release date: 2019-12-20

89284-05-9, 4-AMINO-3-BROMO-5-NITROPYRIDINERelated Search:

4-Amino-3-methylbenzonitrile 4-AMINO-5-IODO-3-PICOLINE 2-AMINO-5-BROMO-3-NITROPYRIDINE 2-AMINO-3-BROMO-5-NITROPYRIDINE,2-Amino-3-bromo-5-nitropyridine 98% 3-AMINO-5-BROMO-2-NITROPYRIDINE 3-BROMO-5-NITROPYRIDINE 4-AMINO-3-BROMO-5-NITROPYRIDINE 4-AMINO-2-BROMO-3-NITROPYRIDINE 3-bromo-N-ethyl-5-nitropyridin-4-amine 2-Amino-6-bromo-3-nitropyridine 6-AMINO-5-BROMO-3-NITROPYRIDINE-2-CARBOXAMIDE N-benzyl-3-bromo-5-nitropyridin-4-amine 3-bromo-5-nitro-N-(2-pyrrolidin-1-ylethyl)pyridin-4-amine 3-bromo-N-methyl-5-nitropyridin-4-amine 3-bromo-5-nitro-N-(pyridin-2-ylmethyl)pyridin-4-amine 3-bromo-N-(1-methylethyl)-5-nitropyridin-4-amine 3-bromo-N-cyclopropyl-5-nitropyridin-4-amine N'-(3-bromo-5-nitropyridin-4-yl)-N,N-dimethylethane-1,2-diamine

4-AMINO-3-BROMO-5-NITROPYRIDINE

4-AMino-3-nitro-5-broMopyridine

4-AMino-3-broMo-5-nitropy...

4-Amino-3-bromo-5-nitropyridine 97%

3-bromo-5-nitro-4-pyridinamine

3-Bromo-4-amino-5-nitropyridine

4-Pyridinamine, 3-bromo-5-nitro-

4-AMINO-3-BROMO-5-NITROPYRIDINE ISO 9001：2015 REACH

89284-05-9

Pyridine