Methyl 2-bromo-6-chlorobenzoate

Product Name: Methyl 2-bromo-6-chlorobenzoate
CAS No.: 685892-23-3
Chemical Name: Methyl 2-bromo-6-chlorobenzoate
Synonyms: EOS-61701;Methyl 2-acetyl-6-chlorobenzoate;Benzoic acid, 2-bromo-6-chloro-, methyl ester;Methyl 2-bromo-6-chlorobenzoate ISO 9001：2015 REACH
CBNumber: CB31117582
Molecular Formula: C8H6BrClO2
Formula Weight: 249.49
MOL File: 685892-23-3.mol

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Methyl 2-bromo-6-chlorobenzoate Property

Melting point:: 54-56°
Boiling point:: 274.5±20.0 °C(Predicted)
Density: 1.604±0.06 g/cm3(Predicted)
Flash point:: 110°
storage temp.: Sealed in dry,Room Temperature
Appearance: White to yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M295995
Product name: Methyl2-bromo-6-chlorobenzoate
Packaging: 100mg
Price: $45
Updated: 2021/12/16

TRC

Product number: M295995
Product name: Methyl2-bromo-6-chlorobenzoate
Packaging: 500mg
Price: $65
Updated: 2021/12/16

TRC

Product number: M295995
Product name: Methyl2-bromo-6-chlorobenzoate
Packaging: 1g
Price: $75
Updated: 2021/12/16

AK Scientific

Product number: J96513
Product name: Methyl2-bromo-6-chlorobenzoate
Packaging: 250mg
Price: $22
Updated: 2021/12/16

AK Scientific

Product number: J96513
Product name: Methyl2-bromo-6-chlorobenzoate
Packaging: 1g
Price: $53
Updated: 2021/12/16

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Methyl 2-bromo-6-chlorobenzoate Chemical Properties,Usage,Production

Uses

Methyl 2-bromo-6-chlorobenzoate

Synthesis

93224-85-2

74-88-4

685892-23-3

GENERAL STEPS: 2-bromo-6-chlorobenzoic acid (9.5 g, 0.041 mol) and potassium carbonate (8.6 g, 0.061 mol) were sequentially added to 50 mL of N,N-dimethylformamide and stirred until completely dissolved. Subsequently, iodomethane (11.2 g, 0.081 mol) was slowly added dropwise over 10 minutes. After the dropwise addition, the reaction mixture was continued to be stirred at room temperature for 3.5 hours. Upon completion of the reaction, the reaction mixture was diluted with 500 mL of water and back-extracted with ethyl acetate (3 x 300 mL). The organic phases were combined, washed with 1 M aqueous hydrochloric acid (100 mL), dried over anhydrous sodium sulfate, filtered, and concentrated under reduced pressure to afford methyl 2-bromo-6-chlorobenzoate (10.0 g, 99.4% yield). The product was characterized by 1H NMR (400 MHz, CDCl3): δ 7.413 (d, J = 8 Hz, 1H), 7.29 (d, J = 8 Hz, 1H), 7.137 (t, J = 8 Hz, 1H), 3.9 (s, 3H).

References

[1] Patent: US2014/256734, 2014, A1. Location in patent: Paragraph 0238-0240
[2] Journal of the American Chemical Society, 2015, vol. 137, # 13, p. 4445 - 4452
[3] Organic Process Research and Development, 2005, vol. 9, # 6, p. 764 - 767

Methyl 2-bromo-6-chlorobenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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Methyl 2-bromo-6-chlorobenzoate Suppliers

China 91 Germany 1 India 1 United States 7 Global 100

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View Lastest Price from Methyl 2-bromo-6-chlorobenzoate manufacturers

Shanghai Rlavie Technology Co ltd

Product: Methyl 2-bromo-6-chlorobenzoate 685892-23-3
Price: US $0.00-0.00/KG
Min. Order: 1g
Purity: 98%min
Supply Ability: 200kgs/month
Release date: 2021-11-20

Career Henan Chemical Co

Product: Methyl 2-bromo-6-chlorobenzoate 685892-23-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2019-07-12

685892-23-3, Methyl 2-bromo-6-chlorobenzoateRelated Search:

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Methyl 2-acetyl-6-chlorobenzoate

EOS-61701

Benzoic acid, 2-bromo-6-chloro-, methyl ester

Methyl 2-bromo-6-chlorobenzoate ISO 9001：2015 REACH

685892-23-3

685829-23-3