p-Anisohydrazide

Product Name: p-Anisohydrazide
CAS No.: 3290-99-1
Chemical Name: p-Anisohydrazide
Synonyms: AKOS 92185;anisichydrazide;p-anisohydrazide;anisoylhydrazine;AKOS BBS-00004504;P-ANISOYLHYDRAZINE;P-ANISIC HYDRAZIDE;anisicacidhydrazide;LABOTEST-BB LT00025103;4-METHOXYBENZHYDRAZIDE
CBNumber: CB3128224
Molecular Formula: C8H10N2O2
Formula Weight: 166.18
MOL File: 3290-99-1.mol

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p-Anisohydrazide Property

Melting point:: 136-140 °C(lit.)
Boiling point:: 294.38°C (rough estimate)
Density: 1.2265 (rough estimate)
refractive index: 1.6180 (estimate)
storage temp.: Sealed in dry,Room Temperature
form: powder to crystal
pka: 12.65±0.10(Predicted)
color: White to Orange to Green
Water Solubility: Slightly soluble in water.
BRN: 389017
InChIKey: REKQLYUAUXYJSZ-UHFFFAOYSA-N
CAS DataBase Reference: 3290-99-1(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-37/39
WGK Germany: 3
RTECS: BZ4800000
HazardClass: IRRITANT
HS Code: 2928009090
Toxicity: LD50 ivn-mus: 178 mg/kg CSLNX* NX#00894

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 558346
Product name: 4-Methoxybenzhydrazide
Purity: 97%
Packaging: 5g
Price: $21.85
Updated: 2025/07/31

Sigma-Aldrich

Product number: 558346
Product name: 4-Methoxybenzhydrazide
Purity: 97%
Packaging: 25g
Price: $78.1
Updated: 2025/07/31

TCI Chemical

Product number: M1770
Product name: 4-Methoxybenzohydrazide
Purity: >98.0%(GC)(T)
Packaging: 5g
Price: $91
Updated: 2025/07/31

TCI Chemical

Product number: M1770
Product name: 4-Methoxybenzohydrazide
Purity: >98.0%(GC)(T)
Packaging: 25g
Price: $235
Updated: 2025/07/31

TRC

Product number: M292953
Product name: 4-Methoxybenzhydrazide
Packaging: 5g
Price: $75
Updated: 2021/12/16

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p-Anisohydrazide Chemical Properties,Usage,Production

Uses

4-Methoxybenzhydrazide is used as pharmaceutical intermediates and it is also involved in a variety of organic synthesis.

Uses

4-Methoxybenzhydrazide may be used to synthesize:

N′-[(E)-5-bromo-2-hydroxy-3-methoxybenzylidene]-4-methoxybenzohydrazide monohydrate
2,5-bis(4-methoxyphenyl)-1,3,4-oxadiazole
hydrazone ligands, which readily forms ruthenium(II) hydrazone complexes via reaction with [RuHCl(CO)(PPh₃)₃]

Synthesis Reference(s)

Journal of Medicinal Chemistry, 27, p. 1565, 1984 DOI: 10.1021/jm00378a007

Safety Profile

Poison by intravenous route. Questionable carcinogen with experimental neoplastigenic data. When heated to decomposition it emits toxic fumes of Nox.

Synthesis

121-98-2

3290-99-1

4-Methoxybenzoic acid hydrazide was synthesized according to literature [22]. A mixture of methyl 4-methoxybenzoate (1.66 g, 10 mmol) with 80% hydrazine hydrate (3.6 mL, 60 mmol) in anhydrous ethanol (20 mL) was heated and refluxed for 6 hours. After completion of the reaction, the solvent was removed by distillation under reduced pressure to give a white precipitate. The crude product was recrystallized from anhydrous ethanol to give 4-methoxybenzohydrazide as colorless needle-like crystals. Yield 96%, melting point 138-139°C (literature values in accordance).

References

[1] Journal of the American Chemical Society, 2013, vol. 135, # 15, p. 5656 - 5668
[2] Journal of the Chilean Chemical Society, 2012, vol. 57, # 4, p. 1492 - 1496
[3] Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2017, vol. 174, p. 272 - 278
[4] European Journal of Medicinal Chemistry, 1985, vol. 20, # 3, p. 257 - 266
[5] Bioorganic and Medicinal Chemistry, 2005, vol. 13, # 16, p. 4842 - 4850

p-Anisohydrazide Preparation Products And Raw materials

Raw materials

Preparation Products

5-(4-METHOXYPHENYL)-1 3 4-OXADIAZOLE-2-&

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p-Anisohydrazide Suppliers

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View Lastest Price from p-Anisohydrazide manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: p-Anisohydrazide 3290-99-1
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20T
Release date: 2024-07-11

Career Henan Chemical Co

Product: p-Anisohydrazide 3290-99-1
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: Customized
Release date: 2019-07-02

3290-99-1, p-AnisohydrazideRelated Search:

4-Methoxybenzoyl chloride p-Anisidine-3-sulfonic acid p-Anisidine p-Anisaldehyde p-Anisohydrazide 3,4-METHYLENEDIOXYBENZHYDRAZIDE 1-(4-METHOXYBENZOYL)-2-(1-NAPHTHOYL)-HYDRAZINE 3,4-DIMETHOXYBENZHYDRAZIDE 3,4,5-TRIMETHOXYBENZHYDRAZIDE 4-ETHOXYBENZHYDRAZIDE o-anisohydrazide Formylhydrazine Benzoyl hydrazine 3,5-DIIODO-4-METHOXYBENZHYDRAZIDE 4-PHENOXYBENZHYDRAZIDE 3,5-DICHLORO-4-METHOXYBENZENECARBOHYDRAZIDE 2,3-DICHLORO-4-[2-(4-METHOXYBENZOYL)HYDRAZONO]BUT-2-ENOIC ACID 4-(4-METHOXYPHENYL)-1-(3,4,5-TRIMETHOXYBENZOYL)THIOSEMICARBAZIDE

p-anisohydrazide

P-ANISIC HYDRAZIDE

P-ANISOYLHYDRAZINE

P-METHOXY BENZHYDRAZIDE

4-METHOXYBENZENE-1-CARBOHYDRAZIDE

4-METHOXYBENZOHYDRAZIDE

4-METHOXYBENZHYDRAZIDE

4-METHOXY-BENZOIC ACID HYDRAZIDE

4-METHOXYBENZOYLHYDRAZINE

LABOTEST-BB LT00025103

(p-methoxybenzoyl)hydrazine

4-methoxybenzoylhydrazide

4-methoxybenzoyl-hydrazin

anisicacidhydrazide

anisichydrazide

anisoylhydrazine

p-anisicacid,hydrazide

p-methoxybenzoicacidhydrazide

p-methoxy-benzoicacihydrazide

p-methoxybenzoichydrazide

AKOS 92185

AKOS BBS-00004504

4-Methoxybenzhydrazide, 98+%

1-(4-Methoxybenzoyl)hydrazine

4-Methoxybenzhydrazide 97%

4-Methoxybenzoylhydrazine p-Anisic Hydrazide p-Anisoylhydrazine

4-Methoxybenzohydrazide&gt

Benzoic acid, 4-methoxy-, hydrazide

4-Methoxybenzoic hydrazide

3290-99-1

H3COC6H4CONHNH2

Organic Building Blocks

Hydrazides

Building Blocks

Carbonyl Compounds

Building Blocks

Carbonyl Compounds

Chemical Synthesis

Organic Building Blocks

Carbonyl Compounds

Hydrazides

Organic Building Blocks

Aromatic Hydrazides, Hydrazines, Hydrazones and Oximes