ChemicalBook > CAS DataBase List > N-Boc-9-azabicyclo[3.3.1]nonan-3-one

N-Boc-9-azabicyclo[3.3.1]nonan-3-one

Product Name: N-Boc-9-azabicyclo[3.3.1]nonan-3-one
CAS No.: 512822-27-4
Chemical Name: N-Boc-9-azabicyclo[3.3.1]nonan-3-one
Synonyms: N-Boc-9-azabicycL;o[3.3.1]nonan-3-one;9-Boc-3-oxo-9-azabicyclo[...;N-Boc-9-azabicyclo[3.3.1]nonan-3-one;9-Boc-9-aza-bicyclo[3.3.1]nonan-3-one;9-Boc-3-oxo-9-azabicyclo[3.3.1]nonane;9-Azabicyclo[3.3.1]nonan-3-one, N-BOC protected;tert-butyl 3-oxo-9-azabicyclo[3.3.1]nane-9-carboxylate;tert-butyl 3-oxo-9-azabicyclo[3.3.1]nonane-9-carboxylate;3-Oxo-9-aza-bicyclo3.3.1none-9-carboxylic acid tert-butyl ester
CBNumber: CB31459666
Molecular Formula: C13H21NO3
Formula Weight: 239.31
MOL File: 512822-27-4.mol

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N-Boc-9-azabicyclo[3.3.1]nonan-3-one Property

Boiling point:: 342.9±35.0 °C(Predicted)
Density: 1?+-.0.06 g/cm3(Predicted)
storage temp.: 2-8°C
pka: -1.65±0.20(Predicted)
form: solid
color: white
InChI: InChI=1S/C13H21NO3/c1-13(2,3)17-12(16)14-9-5-4-6-10(14)8-11(15)7-9/h9-10H,4-8H2,1-3H3
InChIKey: YEKYAQUJESJBFI-UHFFFAOYSA-N
SMILES: C12N(C(OC(C)(C)C)=O)C(CCC1)CC(=O)C2

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H301Toxic if swalloed

H314Causes severe skin burns and eye damage

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC

Product number: B416608
Product name: N-Boc-9-Azabicyclo[3.3.1]nonan-3-one
Packaging: 1g
Price: $90
Updated: 2021/12/16

Usbiological

Product number: 263821
Product name: N-Boc-9-Azabicyclo[3.3.1]nonan-3-one
Packaging: 500mg
Price: $389
Updated: 2021/12/16

AK Scientific

Product number: J50928
Product name: N-Boc-9-Azabicyclo[3.3.1]nonan-3-one
Packaging: 1g
Price: $15
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB32840
Product name: N-Boc-9-Azabicyclo[3.3.1]nonan-3-one
Packaging: 500mg
Price: $75
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H56-1-AA
Product name: N-Boc-9-azabicyclo[3.3.1]nonan-3-one
Packaging: 1g
Price: $75
Updated: 2021/12/16

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N-Boc-9-azabicyclo[3.3.1]nonan-3-one Chemical Properties,Usage,Production

Synthesis

24424-99-5

72761-60-5

512822-27-4

General procedure for the synthesis of N-Boc-9-azabicyclo[3.3.1]nonan-3-one hydrochloride from di-tert-butyl dicarbonate and 9-azabicyclo[3.3.1]nonan-3-one hydrochloride: 9-azabicyclo[3.3.1]nonan-3-one hydrochloride (12.0 g, 68.3 mmol) was suspended in tetrahydrofuran (THF, 200 mL) followed by addition of methylamine (27.6 g, 273 mmol). Di-tert-butyl dicarbonate (15.6 g, 71.7 mmol) dissolved in THF (50 mL) was added slowly and dropwise over 15 min at 15 °C. The reaction mixture was stirred at room temperature for 1 hour. Upon completion of the reaction, water was added and extracted with diethyl ether (200 mL). The organic phase was washed with water (2 x 100 mL) and subsequently purified by filtration through a short silica gel column. The final product N-Boc-9-azabicyclo[3.3.1]nonan-3-one was obtained in a yield of 15.24 g (93% yield).

References

[1] Patent: WO2009/98209, 2009, A1. Location in patent: Page/Page column 16

N-Boc-9-azabicyclo[3.3.1]nonan-3-one Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from N-Boc-9-azabicyclo[3.3.1]nonan-3-one manufacturers

Career Henan Chemical Co

Product: N-Boc-9-azabicyclo[3.3.1]nonan-3-one 512822-27-4
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 1000KGS
Release date: 2019-12-20

512822-27-4, N-Boc-9-azabicyclo[3.3.1]nonan-3-oneRelated Search:

2-Chloro-2-methylpropane 1,1'-Carbonyldiimidazole NICKEL CARBONYL PSEUDO-PELLETIERINE Carbonyl iron powder 1-BOC-2-ETHYL-PIPERIDIN-4-ONE 1-Piperidinecarboxylicacid,2-methyl-4-oxo-,1,1-dimethylethylester,(2R)-(9CI) 1-Piperidinecarboxylicacid,2-methyl-4-oxo-,1,1-dimethylethylester,(2S)-(9CI) 9-azabicyclo[3.3.1]nonan-3-one N-Boc-9-azabicyclo[3.3.1]nonan-3-one

N-Boc-9-azabicyclo[3.3.1]nonan-3-one

3-Oxo-9-aza-bicyclo[3.3.1]nonane-9-carboxylic acid tert-butyl ester

tert-butyl 3-oxo-9-azabicyclo[3.3.1]nonane-9-carboxylate

9-Boc-3-oxo-9-azabicyclo[...

9-Boc-3-oxo-9-azabicyclo[3.3.1]nonane

9-Boc-9-aza-bicyclo[3.3.1]nonan-3-one

3-Oxo-9-aza-bicyclo3.3.1none-9-carboxylic acid tert-butyl ester

tert-butyl 3-oxo-9-azabicyclo[3.3.1]nane-9-carboxylate

N-Boc-9-azabicycL

o[3.3.1]nonan-3-one

9-Azabicyclo[3.3.1]nonane-9-carboxylic acid, 3-oxo-, 1,1-dimethylethyl ester

9-Azabicyclo[3.3.1]nonan-3-one, N-BOC protected

512822-27-4

Amines and Anilines

Carbonyl Compounds