N-Boc-9-azabicyclo[3.3.1]nonan-3-one
- Product Name
- N-Boc-9-azabicyclo[3.3.1]nonan-3-one
- CAS No.
- 512822-27-4
- Chemical Name
- N-Boc-9-azabicyclo[3.3.1]nonan-3-one
- Synonyms
- N-Boc-9-azabicycL;o[3.3.1]nonan-3-one;9-Boc-3-oxo-9-azabicyclo[...;N-Boc-9-azabicyclo[3.3.1]nonan-3-one;9-Boc-9-aza-bicyclo[3.3.1]nonan-3-one;9-Boc-3-oxo-9-azabicyclo[3.3.1]nonane;9-Azabicyclo[3.3.1]nonan-3-one, N-BOC protected;tert-butyl 3-oxo-9-azabicyclo[3.3.1]nane-9-carboxylate;tert-butyl 3-oxo-9-azabicyclo[3.3.1]nonane-9-carboxylate;3-Oxo-9-aza-bicyclo3.3.1none-9-carboxylic acid tert-butyl ester
- CBNumber
- CB31459666
- Molecular Formula
- C13H21NO3
- Formula Weight
- 239.31
- MOL File
- 512822-27-4.mol
N-Boc-9-azabicyclo[3.3.1]nonan-3-one Property
- Boiling point:
- 342.9±35.0 °C(Predicted)
- Density
- 1?+-.0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- pka
- -1.65±0.20(Predicted)
- form
- solid
- color
- white
- InChI
- InChI=1S/C13H21NO3/c1-13(2,3)17-12(16)14-9-5-4-6-10(14)8-11(15)7-9/h9-10H,4-8H2,1-3H3
- InChIKey
- YEKYAQUJESJBFI-UHFFFAOYSA-N
- SMILES
- C12N(C(OC(C)(C)C)=O)C(CCC1)CC(=O)C2
Safety
- HS Code
- 2933998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H301Toxic if swalloed
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
N-Bromosuccinimide Price
- Product number
- B416608
- Product name
- N-Boc-9-Azabicyclo[3.3.1]nonan-3-one
- Packaging
- 1g
- Price
- $90
- Updated
- 2021/12/16
- Product number
- 263821
- Product name
- N-Boc-9-Azabicyclo[3.3.1]nonan-3-one
- Packaging
- 500mg
- Price
- $389
- Updated
- 2021/12/16
- Product number
- J50928
- Product name
- N-Boc-9-Azabicyclo[3.3.1]nonan-3-one
- Packaging
- 1g
- Price
- $15
- Updated
- 2021/12/16
- Product number
- FB32840
- Product name
- N-Boc-9-Azabicyclo[3.3.1]nonan-3-one
- Packaging
- 500mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 4H56-1-AA
- Product name
- N-Boc-9-azabicyclo[3.3.1]nonan-3-one
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
N-Boc-9-azabicyclo[3.3.1]nonan-3-one Chemical Properties,Usage,Production
Synthesis
24424-99-5
72761-60-5
512822-27-4
General procedure for the synthesis of N-Boc-9-azabicyclo[3.3.1]nonan-3-one hydrochloride from di-tert-butyl dicarbonate and 9-azabicyclo[3.3.1]nonan-3-one hydrochloride: 9-azabicyclo[3.3.1]nonan-3-one hydrochloride (12.0 g, 68.3 mmol) was suspended in tetrahydrofuran (THF, 200 mL) followed by addition of methylamine (27.6 g, 273 mmol). Di-tert-butyl dicarbonate (15.6 g, 71.7 mmol) dissolved in THF (50 mL) was added slowly and dropwise over 15 min at 15 °C. The reaction mixture was stirred at room temperature for 1 hour. Upon completion of the reaction, water was added and extracted with diethyl ether (200 mL). The organic phase was washed with water (2 x 100 mL) and subsequently purified by filtration through a short silica gel column. The final product N-Boc-9-azabicyclo[3.3.1]nonan-3-one was obtained in a yield of 15.24 g (93% yield).
References
[1] Patent: WO2009/98209, 2009, A1. Location in patent: Page/Page column 16
N-Boc-9-azabicyclo[3.3.1]nonan-3-one Preparation Products And Raw materials
Raw materials
Preparation Products
N-Boc-9-azabicyclo[3.3.1]nonan-3-one Suppliers
- Tel
- --
- Fax
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- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
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View Lastest Price from N-Boc-9-azabicyclo[3.3.1]nonan-3-one manufacturers
- Product
- N-Boc-9-azabicyclo[3.3.1]nonan-3-one 512822-27-4
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 1000KGS
- Release date
- 2019-12-20