ChemicalBook > CAS DataBase List > 5-METHOXY-2-NITROBENZONITRILE

5-METHOXY-2-NITROBENZONITRILE

Product Name: 5-METHOXY-2-NITROBENZONITRILE
CAS No.: 38469-84-0
Chemical Name: 5-METHOXY-2-NITROBENZONITRILE
Synonyms: 3-Cyano-4-nitroanisole;5-METHOXY-2-NITROBENZONITRILE;Benzonitrile, 5-methoxy-2-nitro-;3-Cyano-4-nitroanisole, 2-Cyano-4-methoxynitrobenzene
CBNumber: CB32449204
Molecular Formula: C8H6N2O3
Formula Weight: 178.14
MOL File: 38469-84-0.mol

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5-METHOXY-2-NITROBENZONITRILE Property

Melting point:: 96 °C
Boiling point:: 352.2±32.0 °C(Predicted)
Density: 1.32±0.1 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
Appearance: Light brown to yellow Solid

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Safety

HS Code: 2926907090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: M326988
Product name: 5-Methoxy-2-nitrobenzonitrile
Packaging: 100mg
Price: $45
Updated: 2021/12/16

TRC

Product number: M326988
Product name: 5-Methoxy-2-nitrobenzonitrile
Packaging: 500mg
Price: $65
Updated: 2021/12/16

AK Scientific

Product number: W5921
Product name: 5-Methoxy-2-nitrobenzonitrile
Packaging: 1g
Price: $84
Updated: 2021/12/16

Matrix Scientific

Product number: 073350
Product name: 5-Methoxy-2-nitrobenzonitrile
Purity: 95+%
Packaging: 1g
Price: $231
Updated: 2021/12/16

Matrix Scientific

Product number: 073350
Product name: 5-Methoxy-2-nitrobenzonitrile
Purity: 95+%
Packaging: 5g
Price: $639
Updated: 2021/12/16

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5-METHOXY-2-NITROBENZONITRILE Chemical Properties,Usage,Production

Synthesis

41994-92-7

38469-84-0

Step 2: Synthesis of 5-methoxy-2-nitrobenzonitrile To a 100 mL round bottom flask was added 5-methoxy-2-nitrobenzamide (2.1 g, 0.01 mol), trifluoroacetic anhydride (2.2 mL), triethylamine (2.9 mL) and dichloromethane (30 mL). The reaction mixture was stirred at room temperature for 1 hour. After completion of the reaction, the reaction mixture was washed with distilled water (30 mL × 2). The organic layer was separated and dried over anhydrous sodium sulfate and subsequently concentrated under reduced pressure to give 1.75 g (92% yield) of white solid product. Mass spectrometry (MS) showed m/z: 179 ([M + H]+).

References

[1] Patent: US2010/120741, 2010, A1. Location in patent: Page/Page column 59

5-METHOXY-2-NITROBENZONITRILE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-METHOXY-2-NITROBENZONITRILE manufacturers

Career Henan Chemical Co

Product: 5-METHOXY-2-NITROBENZONITRILE 38469-84-0
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 1000KGS
Release date: 2019-12-24

38469-84-0, 5-METHOXY-2-NITROBENZONITRILERelated Search:

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5-METHOXY-2-NITROBENZONITRILE

3-Cyano-4-nitroanisole, 2-Cyano-4-methoxynitrobenzene

3-Cyano-4-nitroanisole

Benzonitrile, 5-methoxy-2-nitro-

38469-84-0