3-METHYLAZETIDINE HYDROCHLORIDE

Product Name: 3-METHYLAZETIDINE HYDROCHLORIDE
CAS No.: 935669-28-6
Chemical Name: 3-METHYLAZETIDINE HYDROCHLORIDE
Synonyms: EOS-60406;3-Methylazetidine;3-Methylazetidine HCl;3-Methylazetidine hydroch...;METHYLAZETIDINE HYDROCHLORIDE;3-METHYLAZETIDINE HYDROCHLORIDE;3-Methylazetidine hydrochlorate;3-methylazetidinium hydrochloride;3-METHYLAZETIDINE BENZENESULFONATE;Azetidine, 3-methyl-, hydrochloride
CBNumber: CB32449875
Molecular Formula: C4H10ClN
Formula Weight: 107.58
MOL File: 935669-28-6.mol

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3-METHYLAZETIDINE HYDROCHLORIDE Property

storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: Colorless to light yellow <150 °C Solid,>151 °C Liquid

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

TRC

Product number: M286718
Product name: 3-MethylazetidineBenzenesulfonicAcidSalt
Packaging: 1g
Price: $200
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0382588
Product name: 3-METHYLAZETIDINE HYDROCHLORIDE
Purity: 95.00%
Packaging: 5MG
Price: $503.75
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H31-5-32
Product name: 3-Methylazetidinehydrochloride
Packaging: 5G
Price: $620
Updated: 2021/12/16

AK Scientific

Product number: W9623
Product name: 3-Methylazetidinehydrochloride
Packaging: 250mg
Price: $82
Updated: 2021/12/16

Matrix Scientific

Product number: 069355
Product name: 3-Methylazetidine hydrochloride
Purity: >95%
Packaging: 1g
Price: $109
Updated: 2021/12/16

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3-METHYLAZETIDINE HYDROCHLORIDE Chemical Properties,Usage,Production

Synthesis

934664-23-0

935669-28-6

General procedure for the synthesis of 3-methylazetidine hydrochloride from benzyl 3-methylene azetidine-1-carboxylate: the product of step (iii) (14.1 g) was dissolved in ethanol (100 mL), 10% Pd/C (JM type 87L) (1.48 g) was added and treated under hydrogen atmosphere. The reaction mixture was stirred for 40 h at 20 °C under hydrogen pressure of 4.50 bar to remove the Cbz protecting groups. Subsequently, the mixture was transferred to ethanol (100 mL) containing palladium hydroxide (2 g) and continued to be hydrogenated at 4.50 bar hydrogen pressure for 24 hours. Upon completion of the reaction, the mixture was filtered through a pad of diatomaceous earth and the filtrate was cooled to 0°C in an ice bath. To the cooled filtrate was added dropwise a dioxane solution (26.0 mL) of 4 M HCl, followed by evaporation of the solution to dryness to give the title product 3-methylazetidine hydrochloride (7.46 g) as a light brown oil. The product was characterized by 1H NMR (400 MHz, CDCl3): δ 9.24 (s, 2H), 3.95 (ddd, J = 7.4, 9.8, 11.4 Hz, 2H), 3.55-3.45 (m, 2H), 2.85 (dt, J = 6.7, 14.2 Hz, 1H), 1.16 (d, 3H).

References

[1] Patent: EP2740458, 2016, B1. Location in patent: Paragraph 0052

3-METHYLAZETIDINE HYDROCHLORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-METHYLAZETIDINE HYDROCHLORIDE Suppliers

China 75 India 2 United Kingdom 2 United States 10 Global 89

Accela ChemBio Inc.

Tel: +1-858-6993322
Fax: (+1)-858-876-1948
Email: info@accelachem.com
Country: United States
ProdList: 21193
Advantage: 58

Alchem Pharmtech,Inc.

Tel: 8485655694
Email: sales@alchempharmtech.com
Country: United States
ProdList: 63687
Advantage: 58

Protheragen-ING

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Email: info@protheragen-ing.com
Country: United States
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Advantage: 58

Aladdin Scientific

Tel
Email: tp@aladdinsci.com
Country: United States
ProdList: 52923
Advantage: 58

Synthonix Inc

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Email: info@synthonix.com
Country: United States
ProdList: 6872
Advantage: 58

NE Scientific

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Country: United States
ProdList: 5030
Advantage: 55

Combi-Blocks Inc.

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Email: sales@combi-blocks.com
Country: United States
ProdList: 6618
Advantage: 69

SynQuest Laboratories, Inc.

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Email: info@synquestlabs.com
Country: United States
ProdList: 6871
Advantage: 62

Matrix Scientific

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Email: sales@matrixscientific.com
Country: United States
ProdList: 6632
Advantage: 80

Rintech, Inc.

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Email: info@rintechinc.com
Country: United States
ProdList: 3416
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View Lastest Price from 3-METHYLAZETIDINE HYDROCHLORIDE manufacturers

Career Henan Chemical Co

Product: 3-METHYLAZETIDINE HYDROCHLORIDE 935669-28-6
Price: US $6.60/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg -1000kg
Release date: 2020-01-02

935669-28-6, 3-METHYLAZETIDINE HYDROCHLORIDERelated Search:

Zetidoline 3-AZETIDINECARBOXYLIC ACID, METHYL ESTER, HYDROCHLORIDE 1-(2-CHLOROPYRIDIN-3-YL)-3,3-DIMETHYLAZETIDIN-2-ONE 3-(4-methoxybenzyl)azetidine 4-methylbenzenesulfonate 3-(4-fluorobenzyl)azetidine 4-methylbenzenesulfonate 3-(4-(trifluoromethyl)benzyl)azetidine 4-methylbenzenesulfonate TERT-BUTYL 3-(TOSYLOXYMETHYL)AZETIDINE-1-CARBOXYLATE 3-METHYLAZETIDINE HYDROCHLORIDE 3-(3-fluorobenzyl)azetidine 4-methylbenzenesulfonate 3-benzylazetidine 4-methylbenzenesulfonate 3-(2-fluorobenzyl)azetidine 4-methylbenzenesulfonate 1-(2-BENZOYL-4-CHLOROPHENYL)-3,3-DIMETHYL-2-AZETANONE 3-([(2-CHLORO-4-FLUOROBENZYL)OXY]IMINO)-2-[4-(3,3-DIMETHYL-2-OXO-1-AZETANYL)PHENYL]PROPANENITRILE 1-(4-[3-(4-CHLOROPHENYL)PYRAZOLO[1,5-A]PYRIMIDIN-7-YL]PHENYL)-3,3-DIMETHYL-2-AZETANONE 1-[[3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL](METHYL)AMINO]-3,3-DIMETHYL-2-AZETANONE 1-(3-([3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL]OXY)PHENYL)-3,3-DIMETHYL-2-AZETANONE 1-(4-[1-(4-CHLOROPHENYL)-1H-PYRAZOL-5-YL]PHENYL)-3,3-DIMETHYL-2-AZETANONE 1-(5-CHLORO-2-PYRIDINYL)-3,3-DIMETHYL-2-AZETANONE

3-METHYLAZETIDINE HYDROCHLORIDE

3-METHYLAZETIDINE BENZENESULFONATE

3-METHYLAZETIDINE BENZENESULFONIC ACID SALT

3-Methylazetidine hydroch...

3-Methylazetidine

METHYLAZETIDINE HYDROCHLORIDE

3-Methylazetidine HCl

Azetidine, 3-methyl-, hydrochloride

EOS-60406

Azetidine, 3-methyl-, hydrochloride (1:1)

3-Methylazetidine hydrochloride 95%

3-methylazetidinium hydrochloride

3-Methylazetidine hydrochlorate

3-Methylazetidine hydrochloride - [M1321]

935669-28-6