3-Methoxypyradiazine
- Product Name
- 3-Methoxypyradiazine
- CAS No.
- 19064-65-4
- Chemical Name
- 3-Methoxypyradiazine
- Synonyms
- 3-METHOXYPYRIDAZINE;3-Methoxypyradiazine;3-MethoxypyridaziIne;3-Methoxy-1,2-diazine;3-Methoxypyridazine>Pyridazine, 3-methoxy-;Methoxypyridazine Methoxypyridazine;3-METHOXYPYRIDAZINE3-METHOXYPYRIDAZINE;3-METHOXYPYRIDAZINE ISO 9001：2015 REACH
- CBNumber
- CB3279841
- Molecular Formula
- C5H6N2O
- Formula Weight
- 110.11
- MOL File
- 19064-65-4.mol
3-Methoxypyradiazine Property
- Boiling point:
- 244℃
- Density
- 1.102
- refractive index
- 1.5140 to 1.5180
- Flash point:
- 89℃
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- clear liquid
- pka
- 3.21±0.10(Predicted)
- color
- Colorless to Red to Green
- λmax
- 265nm(H2O)(lit.)
Safety
- HS Code
- 2933998090
N-Bromosuccinimide Price
- Product number
- M2078
- Product name
- 3-Methoxypyridazine
- Purity
- >97.0%(GC)(T)
- Packaging
- 1g
- Price
- $79
- Updated
- 2024/03/01
- Product number
- M2078
- Product name
- 3-Methoxypyridazine
- Purity
- >97.0%(GC)(T)
- Packaging
- 5g
- Price
- $245
- Updated
- 2025/07/31
- Product number
- M332968
- Product name
- 3-Methoxypyridazine
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- X0231
- Product name
- 3-Methoxypyridazine
- Packaging
- 1g
- Price
- $49
- Updated
- 2021/12/16
- Product number
- OR304308
- Product name
- 3-Methoxypyridazine
- Purity
- 97%
- Packaging
- 5g
- Price
- $112
- Updated
- 2021/12/16
3-Methoxypyradiazine Chemical Properties,Usage,Production
Synthesis
1722-10-7
19064-65-4
General procedure for the synthesis of 3-methoxypyridazine from 6-methoxy-3-chloropyridazine: 3-chloro-6-methoxypyridazine (3.60 g, 24.90 mmol), 10% Pd/C (1.590 g, 1.49 mmol), and ammonium formate (3.14 g, 49.81 mmol) were dissolved in methanol (20 mL) at room temperature and the reaction was stirred for 30 minutes. Upon completion of the reaction, the mixture was filtered through diatomaceous earth to remove the Pd/C catalyst. Subsequently, the filtrate was concentrated to dryness under reduced pressure. The resulting residue was dissolved in dichloromethane, washed once with water, dried over anhydrous magnesium sulfate, filtered and concentrated again under reduced pressure to give the title compound 3-methoxypyridazine in brown liquid form (2.41 g, 88% yield, 95% purity). The crude product could be directly used in the subsequent reaction without further purification. The product was confirmed by 1H NMR (300 MHz, chloroform-d): δ 8.83 (dd, J = 4.4, 1.3 Hz, 1H), 7.35 (dd, J = 8.9, 4.4 Hz, 1H), 6.97 (dd, J = 8.9, 1.3 Hz, 1H), 4.14 (s, 3H). Mass spectra (APCI) showed m/z = 152 (M + ACN + H). HPLC analysis showed a retention time of 0.43 min.
References
[1] Patent: US2008/318943, 2008, A1. Location in patent: Page/Page column 74
[2] Patent: US2006/148801, 2006, A1. Location in patent: Page/Page column 13
[3] Patent: WO2012/69202, 2012, A1. Location in patent: Page/Page column 50-51
[4] Patent: EP2463289, 2012, A1. Location in patent: Page/Page column 20
[5] Patent: EP1762568, 2007, A1. Location in patent: Page/Page column 51-52
3-Methoxypyradiazine Preparation Products And Raw materials
Raw materials
Preparation Products
3-Methoxypyradiazine Suppliers
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- China
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View Lastest Price from 3-Methoxypyradiazine manufacturers
- Product
- 3-Methoxypyridazine 19064-65-4
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.0% min
- Supply Ability
- 100 tons min
- Release date
- 2021-05-12
- Product
- 3-Methoxypyridazine 19064-65-4
- Price
- US $200.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%, 99.5% Sublimated
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-30
- Product
- 3-Methoxypyradiazine 19064-65-4
- Price
- US $0.00-0.00/kg
- Min. Order
- 0.001kg
- Purity
- 98%minGC
- Supply Ability
- 100kgs/month
- Release date
- 2022-07-04