General description Application Product Introduction
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2-Bromothiophene

General description Application Product Introduction
Product Name
2-Bromothiophene
CAS No.
1003-09-4
Chemical Name
2-Bromothiophene
Synonyms
S0502;DKIIR;NSC 4456;INDIP-020;forTipepidine;2-Bromthiophen;Thienyl bromide;2-bromo-thiophen;2-BROMOTHIOPHENE;2-Bromothiaphene
CBNumber
CB3335815
Molecular Formula
C4H3BrS
Formula Weight
163.04
MOL File
1003-09-4.mol
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2-Bromothiophene Property

Melting point:
-10 °C
Boiling point:
149-151 °C (lit.)
Density 
1.684 g/mL at 25 °C (lit.)
refractive index 
n20/D 1.586(lit.)
Flash point:
140 °F
storage temp. 
2-8°C
form 
Liquid
color 
Clear colorless to slightly brownish
Specific Gravity
1.684
Water Solubility 
IMMISCIBLE
Sensitive 
Light Sensitive
BRN 
104663
InChIKey
TUCRZHGAIRVWTI-UHFFFAOYSA-N
CAS DataBase Reference
1003-09-4(CAS DataBase Reference)
NIST Chemistry Reference
Thiophene, 2-bromo-(1003-09-4)
EPA Substance Registry System
Thiophene, 2-bromo- (1003-09-4)
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Safety

Hazard Codes 
T,N,Xn
Risk Statements 
10-25-41-51/53-36/37/38-23/24-22-20/21/22
Safety Statements 
26-36/37/39-45-61-16-36
RIDADR 
UN 2929 6.1/PG 2
WGK Germany 
3
8
Hazard Note 
Irritant
TSCA 
T
HazardClass 
6.1
PackingGroup 
II
HS Code 
29349990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H226Flammable liquid and vapour

H300Fatal if swallowed

H318Causes serious eye damage

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P233Keep container tightly closed.

P240Ground/bond container and receiving equipment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
124168
Product name
2-Bromothiophene
Purity
98%
Packaging
10g
Price
$41.6
Updated
2024/03/01
Sigma-Aldrich
Product number
124168
Product name
2-Bromothiophene
Purity
98%
Packaging
50g
Price
$72.5
Updated
2024/03/01
TCI Chemical
Product number
B0941
Product name
2-Bromothiophene
Purity
>98.0%(GC)
Packaging
25g
Price
$21
Updated
2024/03/01
TCI Chemical
Product number
B0941
Product name
2-Bromothiophene
Purity
>98.0%(GC)
Packaging
250g
Price
$111
Updated
2024/03/01
Alfa Aesar
Product number
A11959
Product name
2-Bromothiophene, 98+%
Packaging
50g
Price
$51.8
Updated
2024/03/01
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2-Bromothiophene Chemical Properties,Usage,Production

General description

2-Bromothiophene undergoes metallation-alkylation reaction with various electrophiles to generate various 5-alkylated 2-bromo products. It is coupled with 4-bromoallyl phenyl ether to produce allyl thiophene ether, which is a new type of organic thin film transistor dielectric material.

Application

In dimethylformamide containing tetramethylammonium perchlorate, 2-bromothiophene is electrochemically reduced many mono- and dihalothiophenes on a carbon cathode by cyclic voltammetry and controlled potential electrolysis.

Product Introduction

The 2-Bromothiophene(casno:1003-09-4) is an organic compound with the formula C4H3BrS. The IUPAC name of this chemical is 2-bromothiophene. With the CAS registry number 1003-09-4, it is also named as Bromothiophene. The product's categories are Thiophenes; Halides; Thiophenes & Benzothiophenes; Thiophene & Benzothiophene; Thiophenes & Benzothiophenes. Besides, 2-Bromothiophene(casno:1003-09-4) is a colorless to light yellow transparent liquid, which should be stored in a closed dark and cool place. 2-Bromothiophene(casno:1003-09-4) can be used for organic synthesis and pharmaceutical intermediates.

Chemical Properties

colorless to light yellow liquid. Soluble in ether and acetone, insoluble in water.

Uses

2-Bromothiophene has been used in electrochemical reduction of a number of mono- and dihalothiophenes at carbon cathodes in dimethylformamide containing tetramethylammonium per chlorate by cyclic voltammetry and controlled-potential electrolysis.

Preparation

2-Bromothiophene is synthesized by bromination of thiophene, which is achieved through the following steps: dissolve thiophene in acetic acid, and add bromine in glacial acetic acid solution below 10°C. Water was added to the reaction mixture to precipitate an oily liquid. Extract with ether. Add potassium carbonate to the extract to remove acetic acid, dry it, distill off the ether, and then conduct vacuum distillation to collect fractions at 42-46°C (1.73kPa) to obtain 2-bromothiophene with a yield of 55%.

Synthesis Reference(s)

Journal of the American Chemical Society, 79, p. 5474, 1957 DOI: 10.1021/ja01577a039
Synthesis, p. 890, 1988 DOI: 10.1055/s-1988-27740

General Description

2-Bromothiophene undergoes metalation-alkylation reaction with various electrophiles to form various 5-alkylated 2-bromo products. It undergoes coupling with 4-bromo allyl phenyl ether to form allyl phenyl thiophene ether, which is a novel potential dielectric material for organic thin film transistors.

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2-Bromothiophene Suppliers

Sichuan Kulinan Technology Co., Ltd
Tel
400-1166-196 18981987031
Fax
028-84555506 800101999
Email
cdhxsj@163.com
Country
China
ProdList
11707
Advantage
57
Zhejiang Shouerfu Chemical Trade Co. Ltd.
Tel
0571-88902508
Fax
0571-88902500
Email
xiaowan@shoufuchem.com
Country
China
ProdList
491
Advantage
58
Shandong Vantage Specialty Chemicals Biotechnology Co., Ltd.
Tel
133-96369453 18678026865
Fax
0536-2101172
Email
sdfantai@163.com
Country
China
ProdList
862
Advantage
58
Weifang Siyuan Chemical Co., Ltd.
Tel
0536-8888106 17663601818
Fax
0536-8888106
Email
2354379876@qq.com
Country
China
ProdList
245
Advantage
58
Zhangjiagang Free Trade Zone Kailite Chemical Co., Ltd.
Tel
18606289633 15862625988
Fax
0512-58813106
Email
sales@clentchem.com
Country
China
ProdList
181
Advantage
60
J & K SCIENTIFIC LTD.
Tel
010-82848833 400-666-7788
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
94657
Advantage
76
Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
021-61259108 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
ProdList
40228
Advantage
62
3B Pharmachem (Wuhan) International Co.,Ltd.
Tel
821-50328103-801 18930552037
Fax
86-21-50328109
Email
3bsc@sina.com
Country
China
ProdList
15839
Advantage
69
Alfa Aesar
Tel
400-6106006
Fax
021-67582001/03/05
Email
saleschina@alfa-asia.com
Country
China
ProdList
30123
Advantage
84
TCI (Shanghai) Development Co., Ltd.
Tel
021-67121386
Fax
021-67121385
Email
Sales-CN@TCIchemicals.com
Country
China
ProdList
24529
Advantage
81
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View Lastest Price from 2-Bromothiophene manufacturers

airuikechemical co., ltd.
Product
2-bromothiophene 1003-09-4
Price
US $0.00-0.00/Kg
Min. Order
1Kg
Purity
99.9%
Supply Ability
200tons
Release date
2024-04-09
Hebei Chuanghai Biotechnology Co,.LTD
Product
2-Bromothiophene 1003-09-4
Price
US $5.00-2.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10000kg
Release date
2024-08-19
Hebei Kingfiner Technology Development Co.Ltd
Product
2-Bromothiophene 1003-09-4
Price
US $0.00-0.00/kg
Min. Order
1kg
Purity
0.99
Supply Ability
50000kg
Release date
2024-06-14

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