ChemicalBook > CAS DataBase List > N-(2,4-DIMETHOXYBENZYL)-N-METHYLAMINE

N-(2,4-DIMETHOXYBENZYL)-N-METHYLAMINE

Product Name
N-(2,4-DIMETHOXYBENZYL)-N-METHYLAMINE
CAS No.
102503-23-1
Chemical Name
N-(2,4-DIMETHOXYBENZYL)-N-METHYLAMINE
Synonyms
1-(2,4-DiMethoxyphenyl)-N-MethylMethanaMine;2,4-Dimethoxy-N-methylbenzylamine;AKOS BC-0898;1-(2,4-Dimethoxyphenyl);(2,4-DiMethoxybenzyl)MethylaMine;N-Methyl-2,4-Dimethoxybenzylamine;-(2,4-DIMETHOXYBENZYL)-N-METHYLAMINE;N-(2,4-DIMETHOXYBENZYL)-N-METHYLAMINE;Benzenemethanamine, 2,4-dimethoxy-N-methyl-;(2,4-diMethoxyphenyl)-N-MethylMethanaMiniuM
CBNumber
CB3372588
Molecular Formula
C10H15NO2
Formula Weight
181.23
MOL File
102503-23-1.mol
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N-(2,4-DIMETHOXYBENZYL)-N-METHYLAMINE Property

Boiling point:
262.1±25.0 °C(Predicted)
Density 
1.012±0.06 g/cm3(Predicted)
storage temp. 
2-8°C(protect from light)
pka
9.32±0.10(Predicted)
Appearance
Colorless to light yellow Liquid
InChI
InChI=1S/C10H15NO2/c1-11-7-8-4-5-9(12-2)6-10(8)13-3/h4-6,11H,7H2,1-3H3
InChIKey
ULVUWTHGZHDWMW-UHFFFAOYSA-N
SMILES
C1(CNC)=CC=C(OC)C=C1OC
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Safety

Risk Statements 
36/37/38
Safety Statements 
26-36/37/39
HS Code 
2922190090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
D481025
Product name
1-(2,4-Dimethoxyphenyl)-N-methylmethanamine
Packaging
100mg
Price
$75
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD142242
Product name
1-(2,4-Dimethoxyphenyl)-N-methylmethanamine
Packaging
250mg
Price
$72.5
Updated
2021/12/16
Apolloscientific
Product number
OR945146
Product name
(2,4-Dimethoxybenzyl)methylamine
Purity
97%
Packaging
1g
Price
$182
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD142242
Product name
1-(2,4-Dimethoxyphenyl)-N-methylmethanamine
Packaging
1g
Price
$218.75
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD142242
Product name
1-(2,4-Dimethoxyphenyl)-N-methylmethanamine
Packaging
2g
Price
$372
Updated
2021/12/16
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N-(2,4-DIMETHOXYBENZYL)-N-METHYLAMINE Chemical Properties,Usage,Production

Synthesis

613-45-6

74-89-5

102503-23-1

To a stirred solution of 2,4-dimethoxybenzaldehyde (20.0 g, 120.48 mmol) in methanol (200 mL), a methanolic solution of methylamine (33%, 15.0 g, 481.90 mmol) was slowly added at 0°C and the reaction mixture was kept stirring at 0°C for 1 hour. Subsequently, sodium borohydride (5.5 g, 144.57 mmol) was added in batches at 0 °C and the reaction mixture was kept stirring at room temperature for 12 hours. The reaction progress was monitored by thin layer chromatography (TLC). Upon completion of the reaction, the reaction mixture was acidified with dilute hydrochloric acid (200 mL) and methanol was removed by distillation under reduced pressure. The residue was diluted with water and alkalized with dilute sodium hydroxide solution (80 mL). The aqueous layer was extracted with ethyl acetate (5 x 200 mL). The organic layers were combined, dried over anhydrous sodium sulfate and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography (50-80% ethyl acetate/hexane gradient elution) to afford 2,4-dimethoxy-N-methylbenzenemethanamine (20.0 g, 92.0% yield) as a light yellow liquid.1H NMR (400 MHz, DMSO-d6): δ 7.14 (d, J = 8.4Hz, 1H), 6.51 (brs, 1H), 6.47-6.45 (d, J = 8.4Hz, 1H), 6.47-6.45 (brs, 1H). 6.47-6.45 (m, 1H), 3.74 (s, 6H), 3.53 (s, 2H), 2.24 (s, 3H); LC-MS: m/z 181.80 [M + H]+.

References

[1] Patent: WO2018/165520, 2018, A1. Location in patent: Page/Page column 301
[2] Patent: WO2008/108380, 2008, A2. Location in patent: Page/Page column 103-104
[3] Bioorganic and Medicinal Chemistry Letters, 2009, vol. 19, # 2, p. 378 - 381

N-(2,4-DIMETHOXYBENZYL)-N-METHYLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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N-(2,4-DIMETHOXYBENZYL)-N-METHYLAMINE Suppliers

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View Lastest Price from N-(2,4-DIMETHOXYBENZYL)-N-METHYLAMINE manufacturers

Career Henan Chemical Co
Product
N-(2,4-DIMETHOXYBENZYL)-N-METHYLAMINE 102503-23-1
Price
US $1.00/g
Min. Order
1g
Purity
99%
Supply Ability
200g
Release date
2020-02-01

102503-23-1, N-(2,4-DIMETHOXYBENZYL)-N-METHYLAMINERelated Search:

BERBAMINE NOSCAPINE HYDROCHLORIDE OXYACANTHINE HYDROCHLORIDE D-TUBOCURARINE CHLORIDE Narcotine CURINE HYDROCOTARNINE HYDROBROMIDE BIS(2,4-DIMETHOXYBENZYL)AMINE L-TETRANDRINE RINK AMIDE LINKER FMOC-GLN(TMOB)-OH FMOC-ASN(TMOB)-OH N-(2,5-dimethoxybenzyl)-N-methylamine (((2,4-DIMETHOXYPHENYL)METHYL)(4-(TERT-BUTYL)PHENYL)AMINO)((2-CHLOROPHENYL)AMINO)METHANE-1-THIONE NOSCAPINE HYDROCHLORIDE HYDRATE LABOTEST-BB LT00452156 1-(4-METHOXY-6-METHYL-5,6,7,8-TETRAHYDRO-[1,3]DIOXOLO[4,5-G]ISOQUINOLIN-5-YL)-PROPAN-2-ONE TIMTEC-BB SBB006457

  • N-(2,4-DIMETHOXYBENZYL)-N-METHYLAMINE
  • AKOS BC-0898
  • -(2,4-DIMETHOXYBENZYL)-N-METHYLAMINE
  • (2,4-diMethoxyphenyl)-N-MethylMethanaMiniuM
  • (2,4-DiMethoxybenzyl)MethylaMine
  • 1-(2,4-DiMethoxyphenyl)-N-MethylMethanaMine
  • N-Methyl-2,4-Dimethoxybenzylamine
  • 1-(2,4-Dimethoxyphenyl)
  • 2,4-Dimethoxy-N-methylbenzylamine
  • Benzenemethanamine, 2,4-dimethoxy-N-methyl-
  • 102503-23-1