ChemicalBook > CAS DataBase List > 3-FLUORO-5-IODOANILINE

3-FLUORO-5-IODOANILINE

Product Name: 3-FLUORO-5-IODOANILINE
CAS No.: 660-49-1
Chemical Name: 3-FLUORO-5-IODOANILINE
Synonyms: 3-FLUORO-5-IODOANILINE;5-FLUORO-3-IODOANILINE;3-Fluoro-5-iodoaniline,96%;3-FLUORO-5-IODO-PHENYLAMINE;Benzenamine, 3-fluoro-5-iodo-
CBNumber: CB3398647
Molecular Formula: C6H5FIN
Formula Weight: 237.01
MOL File: 660-49-1.mol

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3-FLUORO-5-IODOANILINE Property

Boiling point:: 279.5±25.0 °C(Predicted)
Density: 2.008±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 2.62±0.10(Predicted)
Appearance: Brown to reddish brown Liquid
Sensitive: Light Sensitive
CAS DataBase Reference: 660-49-1(CAS DataBase Reference)

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Safety

Risk Statements: 36/37/38
Safety Statements: 26-36/37/39
HS Code: 2921420090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H301Toxic if swalloed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: F592160
Product name: 3-Fluoro-5-iodoaniline
Packaging: 250mg
Price: $55
Updated: 2021/12/16

TRC

Product number: F592160
Product name: 3-Fluoro-5-iodoaniline
Packaging: 500mg
Price: $65
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3630-K-35
Product name: 3-Fluoro-5-iodoaniline
Purity: 97%
Packaging: 1g
Price: $45
Updated: 2021/12/16

Apolloscientific

Product number: PC5888
Product name: 3-Fluoro-5-iodoaniline
Packaging: 1g
Price: $100
Updated: 2021/12/16

Matrix Scientific

Product number: 119140
Product name: 3-Fluoro-5-iodoaniline
Purity: 96%
Packaging: 1g
Price: $180
Updated: 2021/12/16

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3-FLUORO-5-IODOANILINE Chemical Properties,Usage,Production

Synthesis

3819-88-3

660-49-1

1. A suspension of 1-fluoro-3-iodo-5-nitrobenzene (0.5 g, 1.87 mmol) with SnCl2-2H2O (1.5 g, 6.64 mmol) in ethanol (10 mL) was heated to reflux for 1.5 hours. After completion of the reaction, the solvent was removed under reduced pressure and the crude product was diluted with ether and washed sequentially with 4N NaOH solution and saturated saline. The ether layer was separated, dried with anhydrous Na2SO4, filtered and concentrated to give the amine compound as a solid (0.4 g, 91% yield). The crude product can be used directly in the next step of the reaction. 2. A mixture of amine (0.4 g, 1.69 mmol), iodomethane (0.719 g, 5 mmol) and potassium carbonate (0.46 g, 3.38 mmol) obtained above in N,N-dimethylformamide (DMF; 10 mL) was stirred at room temperature for 48 hours. After completion of the reaction, water (10 mL) was added and extracted three times with ether. The organic extracts were combined, washed sequentially with water and saturated saline, dried over anhydrous Na2SO4, filtered and concentrated. The crude product was purified by column chromatography to afford 3-fluoro-5-iodo-N,N-dimethylaniline (VMY-2-119) as liquid (0.23 g, 52% yield). 1H NMR (399 MHz, CDCl3) δ: 6.69-6.63 (m, 2H), 6.22 (dt, J = 12.5, 2.3 Hz, 1H), 2.83 (s, 6H). 13C NMR (100 MHz, CDCl3) δ: 163.33 (d, JF-C = 245 Hz), 152.49 (d, J = 11 Hz), 116.91 (d, J = 2.4 Hz), 112.12 (d, J = 24 Hz), 98.73 (d, J = 26 Hz), 94.24 (d, J = 11 Hz), 40.21 (s, 3H). 40.21 (s, 3H).

References

[1] Patent: WO2013/71067, 2013, A1. Location in patent: Page/Page column 42-43
[2] Chemical and Pharmaceutical Bulletin, 2005, vol. 53, # 2, p. 153 - 163
[3] Journal of Organic Chemistry, 1960, vol. 25, p. 1342 - 1348
[4] Patent: EP1382603, 2004, A1. Location in patent: Page 170
[5] Patent: US6821980, 2004, B1. Location in patent: Page column 40-41

3-FLUORO-5-IODOANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-FLUORO-5-IODOANILINE manufacturers

Hebei Chuanghai Biotechnology Co., Ltd

Product: 3-FLUORO-5-IODOANILINE 660-49-1
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20 mt
Release date: 2024-11-13

Career Henan Chemical Co

Product: 3-FLUORO-5-IODOANILINE 660-49-1
Price: US $3.00/KG
Min. Order: 1KG
Purity: 99%min
Supply Ability: 200kg
Release date: 2020-03-06

660-49-1, 3-FLUORO-5-IODOANILINERelated Search:

3-FLUORO-4-IODOANILINE 4-FLUORO-2-IODOANILINE 3-FLUORO-2-IODOANILINE 5-FLUORO-2-IODOANILINE 2-Fluoro-4-iodoaniline 98%,2-FLUORO-4-IODOANILINE,2-Fluoro-4-iodoaniline98% 4-Chloro-2-fluoro-6-iodoaniline 96%,4-Chloro-2-fluoro-6-iodoaniline96%,4-CHLORO-2-FLUORO-6-IODOANILINE 2-Fluoro-5-Iodoaniline 2-FLUORO-6-IODOANILINE 2-FLUORO-4-IODO-6-NITROANILINE 1-Fluoro-3-iodobenzene 1,2-DIAMINO-3-FLUORO-5-IODOBENZENE 3-FLUORO-5-IODOANILINE 1-FLUORO-3-IODO-5-NITROBENZENE

3-FLUORO-5-IODOANILINE

3-FLUORO-5-IODO-PHENYLAMINE

5-FLUORO-3-IODOANILINE

Benzenamine, 3-fluoro-5-iodo-

3-Fluoro-5-iodoaniline,96%

660-49-1