3-(Aminomethyl)-1-methylpiperidine

Product Name: 3-(Aminomethyl)-1-methylpiperidine
CAS No.: 14613-37-7
Chemical Name: 3-(Aminomethyl)-1-methylpiperidine
Synonyms: (1-METHYLPIPERIDIN-3-YL)METHANAMINE;CHEMBRDG-BB 4103006;1-Methyl-3-(aminomethyl)p...;3-AMINOMETHYL-1-METHYLPIPERIDINE;1-Methyl-3-piperidinemethanamine;(1-METHYLPIPERID-3-YL)METHYLAMINE;(1-methyl-3-piperidyl)methanamine;3-PIPERIDINEMETHANAMINE, 1-METHYL-;N-Methyl-3-(aMinoMethyl)piperidine;N-Methyl-3-(aMinoMethyl)-piperidin
CBNumber: CB3687503
Molecular Formula: C7H16N2
Formula Weight: 128.22
MOL File: 14613-37-7.mol

More

Less

3-(Aminomethyl)-1-methylpiperidine Property

Boiling point:: 58°C/6mm
Density: 0.9096 g/cm3
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 10.12±0.29(Predicted)
form: liquid
color: Colourless to pale yellow

More

Less

Safety

Hazard Codes: Xi,Xn
Risk Statements: 22
HazardClass: IRRITANT
HS Code: 2933399990

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H318Causes serious eye damage

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P308+P313IF exposed or concerned: Get medical advice/attention.

More

Less

N-Bromosuccinimide Price

TRC

Product number: A613905
Product name: 3-(Aminomethyl)-1-methylpiperidine
Packaging: 25mg
Price: $45
Updated: 2021/12/16

TRC

Product number: A613905
Product name: 3-(Aminomethyl)-1-methylpiperidine
Packaging: 250mg
Price: $145
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-1-M3
Product name: 3-(Aminomethyl)-1-methylpiperidine
Packaging: 1g
Price: $225
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA51097
Product name: 3-(Aminomethyl)-1-methyl-piperidine
Packaging: 500mg
Price: $360
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA51097
Product name: 3-(Aminomethyl)-1-methyl-piperidine
Packaging: 1g
Price: $435
Updated: 2021/12/16

More

Less

3-(Aminomethyl)-1-methylpiperidine Chemical Properties,Usage,Production

Synthesis

672324-98-0

14613-37-7

3-(Di-tert-butoxymethylamino)-1-methylpiperidine (500 mg, 1.52 mmol) was used as raw material and dissolved in a 1,4-dioxane solution (19.75 mL) of methanol (7.5 mL) and 10% (v/v) concentrated sulfuric acid. The reaction mixture was stirred at 25°C for 0.5 hours. Methanol (300 mL) was then added and BioRad AG1-X8 resin (OH type) was added until the pH reached 10. The resin was removed by filtration and the resin was washed with methanol (2 x 200 mL). The eluates were combined and evaporated to dryness, and the residue was purified by silica gel column chromatography (30 × 2.5 cm) to afford 3-(aminomethyl)-1-methylpiperidine (69.2 mg, 35%) using 10% concentrated ammonium hydroxide in methanol solution-dichloromethane as eluent. The product characterization data were as follows: FABMS: m/z 129.1 (MH+); HRFABMS: m/z 129.1392 (MH+), calculated value C7H17N2: m/z 129.1392; 1H NMR (CDCl3) δ 0.90 (2H, m, CH2), 1.65 (2H, m, CH2), 1.72 (1H, m. CH), 1.79 (1H, m, CH2), 1.91 (1H, m, CH2), 2.30 (3H, s, NCH3), 2.64 (2H, m, CH2), 2.82 (1H, m, CH2NH2), 2.92 (1H, m, CH2NH2); 13C NMR (CDCl3) δ CH3: 46.7; CH2: 25.2, 28.0, 46.0, 36.4, 60.3; CH: 39.9.

References

[1] Patent: WO2004/22561, 2004, A1. Location in patent: Page 109

3-(Aminomethyl)-1-methylpiperidine Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

3-(Aminomethyl)-1-methylpiperidine Suppliers

Belgium 1 China 72 Germany 1 India 2 Switzerland 1 Ukraine 1 United Kingdom 2 United States 22 Global 102

J & K SCIENTIFIC LTD.

Tel: 18210857532; 18210857532
Fax: 86-10-82849933
Email: jkinfo@jkchemical.com
Country: China
ProdList: 96815
Advantage: 76

Wuhan Chemwish Technology Co., Ltd

Tel: 86-027-67849912
Fax: 86-027-87531808
Email: sales@chemwish.com
Country: China
ProdList: 35896
Advantage: 56

Shanghai Boc Chemical Co.,Ltd

Tel: 021-34975603-808 18721111801
Fax: +86-21-34975602-805
Email: sales@bocpharma.com
Country: China
ProdList: 1009
Advantage: 64

ZEROSCHEM.CO.,LTD.

Tel: 10-61256048 13810278579
Fax: +86 10 61256049
Email: sales@zeroschem.com
Country: China
ProdList: 1371
Advantage: 59

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
Email: info@hanhongsci.com
Country: China
ProdList: 42934
Advantage: 64

Chemsky（shanghai）International Co.,Ltd.

Tel: 021-50135380
Email: shchemsky@sina.com
Country: China
ProdList: 32321
Advantage: 50

Beijing HengPuGao Pharmaceutical Chemistry Technology Co., Ltd.

Tel: 010-81520996 13439320863
Fax: 010-81520996
Email: hengpugao@126.com
Country: China
ProdList: 159
Advantage: 57

Amber MolTech LLC

Tel: 086-010-62176588
Fax: 086-010-62117849
Email: amber@jyamber.com
Country: China
ProdList: 10151
Advantage: 56

Beijing Yisiyan Technology Research Center

Tel: 010-56645598 13366904824
Fax: 01062230033
Email: bjkaida@163.com
Country: China
ProdList: 1618
Advantage: 59

Thermo Fisher Scientific

Tel: 800-810-5118
Fax: +86-10-84193589
Email: cnchemical@thermofisher.com
Country: China
ProdList: 17770
Advantage: 75

More

Less

View Lastest Price from 3-(Aminomethyl)-1-methylpiperidine manufacturers

Career Henan Chemical Co

Product: 3-(Aminomethyl)-1-methylpiperidine 14613-37-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: Customized
Release date: 2019-12-20

14613-37-7, 3-(Aminomethyl)-1-methylpiperidineRelated Search:

Hexamethyldisilazane N-Methylpiperidine 2-Amino-2-methyl-1-propanol Haloperidol 2,2,6,6-Tetramethyl-4-piperidinol 2,2,6,6-Tetramethylpiperidinooxy DIHYDROERGOTAMINE TARTRATE DIHYDROERGOCRISTINE MESYLATE (-)-Sparteine sulfate pentahydrate Renzapride METERGOLINE Dihydroergotoxine mesylate CYTISINE SPARTEINE SULFATE (1-Methyl-4-piperidinyl)methanamine C-(1-METHYL-PIPERIDIN-2-YL)-METHYLAMINE Dihydroergotoxine Diphenoxylate

(1-METHYLPIPERIDIN-3-YL)METHANAMINE

3-AMINOMETHYL-1-METHYLPIPERIDINE

3-PIPERIDINEMETHANAMINE, 1-METHYL-

CHEMBRDG-BB 4103006

C-(1-METHYL-PIPERIDIN-3-YL)-METHYLAMINE

C-(1-METHYL-PIPERIDIN-3-YL)-METHYLAMINE, HCL

1-Methyl-3-piperidinemethanamine

(1-METHYLPIPERID-3-YL)METHYLAMINE

1-Methyl-3-(aminomethyl)p...

N-Methyl-3-(aMinoMethyl)piperidine 2HCl

1-(1-methylpiperidin-3-yl)methanamine(SALTDATA: FREE)

(1-Methylpiperidin-3-yl)methylamine

N-Methyl-3-(aMinoMethyl)piperidine

N-Methyl-3-(aMinoMethyl)-piperidin

rac 3-(Aminomethyl)-1-methyl-piperidine, 98%

(1-methyl-3-piperidyl)methanamine

14613-37-7