2-Bromo-4-methoxybenzenol

Product Name: 2-Bromo-4-methoxybenzenol
CAS No.: 17332-11-5
Chemical Name: 2-Bromo-4-methoxybenzenol
Synonyms: 2-BROMO-4-METHOXYPHENOL;4-Methoxy-2-bromophenol;3-Bromo-4-hydroxyanisole;2-bromo-4-methoxylphenol;2-BROMO-4-METHOXYBENZENOL;Phenol, 2-bromo-4-methoxy-;2-Bromo-4-methoxyphenol >2-Bromo-4-methoxyphenol ,98%
CBNumber: CB3717617
Molecular Formula: C7H7BrO2
Formula Weight: 203.03
MOL File: 17332-11-5.mol

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2-Bromo-4-methoxybenzenol Property

Melting point:: 47
Boiling point:: 115 °C
Density: 1.585±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
form: powder to crystal
pka: 8.92±0.18(Predicted)
color: White to Light yellow to Light orange
CAS DataBase Reference: 17332-11-5(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 20/21/22-36/37/38
Safety Statements: 26-36/37/39
Hazard Note: Irritant
HS Code: 29071990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TCI Chemical

Product number: B3135
Product name: 2-Bromo-4-methoxyphenol
Purity: >98.0%(T)
Packaging: 5g
Price: $81
Updated: 2025/07/31

TCI Chemical

Product number: B3135
Product name: 2-Bromo-4-methoxyphenol
Purity: >98.0%(T)
Packaging: 25g
Price: $274
Updated: 2025/07/31

TRC

Product number: B696770
Product name: 2-Bromo-4-methoxyphenol
Packaging: 100mg
Price: $45
Updated: 2021/12/16

TRC

Product number: B696770
Product name: 2-Bromo-4-methoxyphenol
Packaging: 500mg
Price: $65
Updated: 2021/12/16

AK Scientific

Product number: J91568
Product name: 2-Bromo-4-methoxyphenol
Packaging: 1g
Price: $10
Updated: 2021/12/16

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2-Bromo-4-methoxybenzenol Chemical Properties,Usage,Production

Chemical Properties

Off-white solid

Synthesis

150-76-5

17332-11-5

General procedure for the synthesis of 2-bromo-4-methoxyphenol from p-hydroxyanisole: 2.6 mL (100 mMol) of bromine dissolved in 10 mL of carbon disulfide was slowly added dropwise to 12.4 g (100 mMol) of 4-methoxyphenol dissolved in 20 mL of carbon disulfide at 0 °C. The reaction temperature was maintained at 30 °C. After 30 min, 1 mL of bromine dissolved in 10 mL of carbon disulfide was added dropwise. The reaction temperature was maintained at 30 °C. After 30 min, 1 mL of the solution of bromine dissolved in 10 mL of carbon disulfide was added dropwise. After completion of the reaction, the mixture was concentrated under reduced pressure. The residue was dissolved in ether and washed sequentially with 100 mL of water and 100 mL of saturated aqueous sodium chloride. The organic phase was dried with magnesium sulfate and concentrated under reduced pressure. The residue was purified by silica gel column chromatography using a gradient elution with hexane containing 0 to 20% ethyl acetate. The fractions containing the target product were combined and concentrated under reduced pressure to give 11.6 g (57% yield) of 2-bromo-4-methoxyphenol as a crystalline solid.1H-NMR (CDCl3): δ 7.0 (d, 1H), 6.95 (d, 1H), 6.8 (dd, 1H), 5.15 (s, 1H), 3.75 (s, 3H).

References

[1] Organic Letters, 2004, vol. 6, # 4, p. 457 - 460
[2] Synthetic Communications, 2007, vol. 37, # 2, p. 323 - 328
[3] Chemistry - A European Journal, 2012, vol. 18, # 11, p. 3286 - 3291
[4] Chemical Communications, 2012, vol. 48, # 52, p. 6577 - 6579
[5] Patent: WO2013/97224, 2013, A1. Location in patent: Page/Page column 72

2-Bromo-4-methoxybenzenol Preparation Products And Raw materials

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Preparation Products

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2-Bromo-4-methoxybenzenol Suppliers

Americas 1 China 146 Europe 1 France 1 Germany 1 India 5 Japan 2 United Kingdom 10 United States 27 Global 194

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View Lastest Price from 2-Bromo-4-methoxybenzenol manufacturers

Shaanxi Dideu New Materials Co. Ltd

Product: 2-BroMo-4-Methoxyphenol 17332-11-5
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98.0%
Supply Ability: 10000KGS
Release date: 2024-11-19

Career Henan Chemical Co

Product: 2-Bromo-4-methoxybenzenol 17332-11-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 25kg
Release date: 2019-07-12

17332-11-5, 2-Bromo-4-methoxybenzenolRelated Search:

4-Methoxybenzyl cyanide 3-Bromophenol Guaiacol POLY(ETHYLENE GLYCOL) METHYL ETHER ACRYLATE Anisole (Trifluoromethoxy)benzene 2-Bromophenol p-Anisaldehyde 4-Methoxyphenol Bromine 1,4-Dibromo-2,5-dimethoxybenzene 4-BROMO-2,5-DIMETHOXYTOLUENE 4-Bromo-2,5-dimethoxybenzaldehyde 1-Bromo-2,5-dimethoxybenzene 4-BROMO-2,5-DIMETHOXYPHENETHYLAMINE HCL TETRADECABROMO-1,4-DIPHENOXYBENZENE 5- BROMO-2-METHOXYPHENOL 4-BROMO-2-METHOXYPHENOL

2-BROMO-4-METHOXYBENZENOL

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2-Bromo-4-methoxyphenol ,98%

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17332-11-5

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