ChemicalBook > CAS DataBase List > 3,5-DICHLORO-4-FORMYL PYRIDINE

3,5-DICHLORO-4-FORMYL PYRIDINE

Product Name
3,5-DICHLORO-4-FORMYL PYRIDINE
CAS No.
136590-83-5
Chemical Name
3,5-DICHLORO-4-FORMYL PYRIDINE
Synonyms
3,5-DICHLOROISONICOTINALDEHYDE;3,5-dichloropyridine-4-carbaldehyde;3,5-DICHLORO-4-PYRIDINECARBOXALDEHYDE;TIMTEC-BB SBB003785;3,5-DICHLORO-4-FORMYL PYRIDINE;,5-Dichloropyridine-4-carboxaldehyde;3,5-Dichloropyridine-4-carboxaldehyde;3,5-DICHLOROPYRIDINE-4-CARBOXYALDEHYDE;4-PYRIDINECARBOXALDEHYDE, 3,5-DICHLORO-;3,5-Dichloro-4-pyridinecarboxaldehyde 97%
CBNumber
CB3725131
Molecular Formula
C6H3Cl2NO
Formula Weight
176
MOL File
136590-83-5.mol
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3,5-DICHLORO-4-FORMYL PYRIDINE Property

Melting point:
75-79 °C (lit.)
Boiling point:
242.4±35.0 °C(Predicted)
Density 
1.488±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
solubility 
soluble in Methanol
form 
powder to crystal
pka
-0.42±0.10(Predicted)
color 
White to Brown
InChIKey
RBFNWOINNIOZKR-UHFFFAOYSA-N
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36
WGK Germany 
3
HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
572470
Product name
3,5-Dichloro-4-pyridinecarboxaldehyde
Purity
97%
Packaging
5g
Price
$111
Updated
2025/07/31
TCI Chemical
Product number
D5790
Product name
3,5-Dichloro-4-pyridinecarboxaldehyde
Packaging
1G
Price
$26
Updated
2025/07/31
TCI Chemical
Product number
D5790
Product name
3,5-Dichloro-4-pyridinecarboxaldehyde
Packaging
5G
Price
$77
Updated
2025/07/31
Apolloscientific
Product number
OR46033
Product name
3,5-Dichloroisonicotinaldehyde
Packaging
25g
Price
$151
Updated
2021/12/16
SynQuest Laboratories
Product number
4H15-5-Z5
Product name
3,5-Dichloroisonicotinaldehyde
Packaging
25g
Price
$176
Updated
2021/12/16
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3,5-DICHLORO-4-FORMYL PYRIDINE Chemical Properties,Usage,Production

Uses

3,5-Dichloroisonicotinaldehyde is an aldehyde compound that can be synthesized with heteroarylsulfonamides to form heteroarylsulfonylcarboxamides[1].

Synthesis

2457-47-8

136590-83-5

Diisopropylamine (33.6 mL, 0.24 mol) was dissolved in tetrahydrofuran (400 mL) under argon protection and cooled to -65 °C. The solution of 1.6 M n-butyllithium in hexane (156 mL) was added slowly. A hexane solution (156 mL) of 1.6 M n-butyllithium was slowly added. after 20 min, a solution of 3,5-dichloropyridine (29.6 g, 0.20 mol) in tetrahydrofuran (150 mL) was added dropwise, and stirring was continued for 30 min. Subsequently, a tetrahydrofuran (50 mL) solution of dimethylformamide (23.2 mL, 0.30 mol) was added, kept at a constant temperature and stirred for 1 hour. The reaction mixture was poured into 5% aqueous ammonium chloride solution (1,000 mL) and extracted with ethyl acetate. The organic layer was washed sequentially with water and saturated brine, dried over anhydrous sodium sulfate and concentrated under reduced pressure. The residue was purified by silica gel column chromatography to afford 3,5-dichloropyridine-4-carbaldehyde (27.2 g, 77% yield).1H-NMR (CDCl3) δ: 8.63 (2H, s), 10.44 (1H, s).

References

[1] Patent: US5935977, 1999, A
[2] Patent: EP1270577, 2003, A1

3,5-DICHLORO-4-FORMYL PYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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3,5-DICHLORO-4-FORMYL PYRIDINE Suppliers

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View Lastest Price from 3,5-DICHLORO-4-FORMYL PYRIDINE manufacturers

Henan Aochuang Chemical Co.,Ltd.
Product
3,5-DICHLORO-4-FORMYL PYRIDINE 136590-83-5
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1Ton
Release date
2022-10-14
R&D Scientific Inc.
Product
3,5-Dichloropyridine-4-carboxaldehyde 136590-83-5
Price
US $1290.00/g
Min. Order
1g
Purity
98
Supply Ability
500 Kg
Release date
2024-03-19
Honest Joy Holdings Limited
Product
3,5-Dichloro-4-pyridinecarboxaldehyde 136590-83-5
Price
US $0.00/KG
Min. Order
1KG
Purity
97.2%
Supply Ability
100 tons
Release date
2022-01-26

136590-83-5, 3,5-DICHLORO-4-FORMYL PYRIDINERelated Search:


  • 3,5-Dichloropyridine-4-carboxaldehyde, 3,5-Dichloro-4-formylpyridine
  • 3,5-Dichloro-4-pyridinecarboxaldehyde 97%
  • TIMTEC-BB SBB003785
  • 3,5-DICHLORO-4-FORMYL PYRIDINE
  • 3,5-DICHLOROISONICOTINALDEHYDE
  • 3,5-DICHLORO-4-PYRIDINECARBOXALDEHYDE
  • 3,5-DICHLOROPYRIDINE-4-CARBOXYALDEHYDE
  • 3,5-Dichloropyridine-4-carboxaldehyde
  • 4-PYRIDINECARBOXALDEHYDE, 3,5-DICHLORO-
  • ,5-Dichloropyridine-4-carboxaldehyde
  • 4-PYRIDINECARBOXALDEHYDE, 3,5-DICHLORO- (9CI)
  • 3,5-dichloropyridine-4-carbaldehyde
  • 3,5-DICHLORO-4-FORMYL PYRIDINE ISO 9001:2015 REACH
  • 136590-83-5
  • Halogenated Heterocycles
  • Heterocyclic Building Blocks
  • Pyridines
  • Building Blocks
  • Aldehydes
  • Building Blocks
  • C1 to C6
  • C6Heterocyclic Building Blocks
  • Halogenated Heterocycles
  • Heterocyclic Building Blocks
  • Pyridines
  • pharmacetical
  • Pyridine
  • Aldehyde
  • Organohalides
  • C5 to C6
  • C6 to C7
  • Carbonyl Compounds
  • Chemical Synthesis
  • Halogenated Heterocycles
  • Heterocyclic Building Blocks
  • Organic Building Blocks