7H-Pyrazolo[4,3-d]pyrimidin-7-one, 1,4-dihydro-1-methyl- (9CI)
- Product Name
- 7H-Pyrazolo[4,3-d]pyrimidin-7-one, 1,4-dihydro-1-methyl- (9CI)
- CAS No.
- 314021-93-7
- Chemical Name
- 7H-Pyrazolo[4,3-d]pyrimidin-7-one, 1,4-dihydro-1-methyl- (9CI)
- Synonyms
- 1-Methyl-1H-pyrazolo[4,3-d]pyriMidin-7-ol;1,6-dihydro-1-methyl-7H-Pyrazolo[4,3-d]pyrimidin-7-one;1-Methyl-1,6-dihydro-7H-pyrazolo[4,3-d]pyrimidin-7-one;7H-Pyrazolo[4,3-d]pyrimidin-7-one, 1,6-dihydro-1-methyl-;7H-Pyrazolo[4,3-d]pyrimidin-7-one, 1,4-dihydro-1-methyl- (9CI)
- CBNumber
- CB41082384
- Molecular Formula
- C6H6N4O
- Formula Weight
- 150.14
- MOL File
- 314021-93-7.mol
7H-Pyrazolo[4,3-d]pyrimidin-7-one, 1,4-dihydro-1-methyl- (9CI) Property
- storage temp.
- 2-8°C
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- CHM1027255
- Product name
- 1,6-DIHYDRO-1-METHYL-7H-PYRAZOLO[4,3-D]PYRIMIDIN-7-ONE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $502.02
- Updated
- 2021/12/16
- Product number
- 1082EM
- Product name
- 1-Methyl-1H-pyrazolo[4,3-D]pyrimidin-7-OL
- Packaging
- 100mg
- Price
- $796
- Updated
- 2021/12/16
- Product number
- 1082EM
- Product name
- 1-Methyl-1H-pyrazolo[4,3-D]pyrimidin-7-OL
- Packaging
- 250mg
- Price
- $895
- Updated
- 2021/12/16
- Product number
- 1082EM
- Product name
- 1-Methyl-1H-pyrazolo[4,3-D]pyrimidin-7-OL
- Packaging
- 5g
- Price
- $4224
- Updated
- 2021/12/16
- Product number
- P7122
- Product name
- 1,6-dihydro-1-methyl-7H-Pyrazolo[4,3-d]pyrimidin-7-one
- Purity
- 97.00%
- Packaging
- 25G
- Price
- $6710
- Updated
- 2021/12/16
7H-Pyrazolo[4,3-d]pyrimidin-7-one, 1,4-dihydro-1-methyl- (9CI) Chemical Properties,Usage,Production
Synthesis
923283-54-9
3473-63-0
314021-93-7
GENERAL STEPS: To a mixture of 4-amino-1-methyl-1H-pyrazole-5-carboxylic acid methyl ester (0.92 g, 5.9 mmol) dissolved in 5 mL of a mixture of N,N-diisopropylethylamine (Hunig base) and 5 mL of n-butanol was added formamidine acetate (0.68 g, 6.5 mmol). The reaction mixture was heated to 110 °C and stirred for 1 hour. After completion of the reaction, it was cooled to room temperature, the white precipitate was collected by filtration and washed with ether. The resulting white solid was dried under reduced pressure to afford 1-methyl-1H-pyrazolo[4,3-d]pyrimidin-7-ol (0.83 g, 94% yield). The product was characterized by 1H NMR (d6-DMSO): δ 4.33 (s, 3H), 8.50 (s, 1H), 8.80 (s, 1H); electrospray mass spectrometry (ES-MS) showed m/e = 151 ([M + H]+).
References
[1] Patent: US2007/27166, 2007, A1. Location in patent: Page/Page column 80
7H-Pyrazolo[4,3-d]pyrimidin-7-one, 1,4-dihydro-1-methyl- (9CI) Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 7H-Pyrazolo[4,3-d]pyrimidin-7-one, 1,4-dihydro-1-methyl- (9CI) manufacturers
- Product
- 1-Methyl-1H-pyrazolo[4,3-d]pyrimidin-7-ol 314021-93-7
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- Min98% HPLC
- Supply Ability
- G/KG/TON
- Release date
- 2020-01-31