ChemicalBook > CAS DataBase List > 1-(4-METHOXY-1-NAPHTHYL)ETHANONE

1-(4-METHOXY-1-NAPHTHYL)ETHANONE

Product Name
1-(4-METHOXY-1-NAPHTHYL)ETHANONE
CAS No.
24764-66-7
Chemical Name
1-(4-METHOXY-1-NAPHTHYL)ETHANONE
Synonyms
1-Acetyl-4-methoxynaphthalene;1-(4-METHOXY-1-PHTHYL)ETHANONE;1-(4-Methoxy-1-naphthyl)ethanone;4-Methoxy-1-Naphthyl Ethyl Ketone;1-(4-methoxynaphthalen-1-yl)ethanone;1-(4-Methoxy-1-naphthalenyl)-ethanone;Ethanone, 1-(4-methoxy-1-naphthalenyl)-
CBNumber
CB41490152
Molecular Formula
C13H12O2
Formula Weight
200.23
MOL File
24764-66-7.mol
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1-(4-METHOXY-1-NAPHTHYL)ETHANONE Property

storage temp. 
Sealed in dry,Room Temperature
Appearance
Off-white to light brown Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
M331373
Product name
1-(4-Methoxy-1-naphthalenyl)-ethanone
Packaging
100mg
Price
$90
Updated
2021/12/16
AK Scientific
Product number
J57174
Product name
1-Acetyl-4-methoxynaphthalene
Packaging
1g
Price
$29
Updated
2021/12/16
Matrix Scientific
Product number
157090
Product name
1-(4-Methoxy-1-naphthyl)ethanone
Packaging
0.500g
Price
$160
Updated
2021/12/16
Matrix Scientific
Product number
157090
Product name
1-(4-Methoxy-1-naphthyl)ethanone
Packaging
1g
Price
$200
Updated
2021/12/16
Matrix Scientific
Product number
157090
Product name
1-(4-Methoxy-1-naphthyl)ethanone
Packaging
5g
Price
$700
Updated
2021/12/16
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1-(4-METHOXY-1-NAPHTHYL)ETHANONE Chemical Properties,Usage,Production

Synthesis Reference(s)

The Journal of Organic Chemistry, 36, p. 540, 1971 DOI: 10.1021/jo00803a011
Tetrahedron Letters, 31, p. 3933, 1990 DOI: 10.1016/S0040-4039(00)97510-5

Synthesis

75-36-5

2216-69-5

24764-66-7

Aluminum trichloride (800 mg, 6 mmol) in anhydrous dichloromethane (12 mL) was cooled to 0 °C under nitrogen protection and acetyl chloride (236 mg, 3 mmol) was slowly added. The reaction mixture was stirred at room temperature for 10 min before 1-methoxynaphthalene (474 mg, 3 mmol) was added and stirring was continued at room temperature overnight. After completion of the reaction, the reaction was quenched with water, the organic phase was separated, dried over anhydrous sodium sulfate and concentrated under reduced pressure. The residue was purified by silica gel column chromatography (eluent: ethyl acetate/petroleum ether=1:15, v/v) to afford 4-methoxynaphthaleneacetophenone (338 mg, 56% yield) as a white solid.1H NMR (300 MHz, CDCl3) δ: 9.01-9.96 (m, 1H), 8.32-8.35 (m, 1H), 8.03 (d, 1H), 7.63-7.65 (m, 1H), 7.53-7.58 (m, 1H), 6.79 (d, 1H), 4.07 (s, 3H), 2.72 (s, 3H).LC-MS: m/z 201 [M+1]+.

References

[1] Canadian Journal of Chemistry, 1981, vol. 59, p. 2629 - 2641
[2] Patent: US2012/220629, 2012, A1. Location in patent: Page/Page column 46
[3] Patent: WO2012/113103, 2012, A1. Location in patent: Page/Page column 62-63
[4] Recueil des Travaux Chimiques des Pays-Bas, 1945, vol. 64, p. 214,216
[5] Zhurnal Obshchei Khimii, 1938, vol. 8, p. 402,407

1-(4-METHOXY-1-NAPHTHYL)ETHANONE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1-(4-METHOXY-1-NAPHTHYL)ETHANONE manufacturers

Shenzhen Nexcon Pharmatechs Ltd.
Product
1-(4-METHOXY-1-NAPHTHYL)ETHANONE 24764-66-7
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
2000
Release date
2025-04-18
Career Henan Chemica Co
Product
1-(4-METHOXY-1-NAPHTHYL)ETHANONE 24764-66-7
Price
US $1.30/g
Min. Order
1g
Purity
98%
Supply Ability
10kg
Release date
2020-10-28

24764-66-7, 1-(4-METHOXY-1-NAPHTHYL)ETHANONERelated Search:

N-CBZ-4-HYDROXYCYCLOHEXANE 3,4-Diaminobenzoic acid 4-PHENYLIMIDAZOLE Dimenhydrinate 2-Thiophenecarbonyl chloride 4-Bromobenzonitrile DL-Adrenalin Hydroxyaluminum distearate (R)-N-BOC-5-METHOXYCARBONYL-2-PYRROLIDINONE 2-AMINO-3,5-DIBROMO-6-METHYLPYRIDINE Diisopropyl succinate LanthanuM(III) chloride hydrate 4-Amino-3-fluoropyridine 3-(4-BROMOBENZOYL)PROPIONIC ACID 2,4-Difluoronitrobenzene Propyleneglycol alginate 3-CHLORO-2,5-DIMETHYLPYRAZINE 4-Bromo-3-fluoroanisole

  • Ethanone, 1-(4-methoxy-1-naphthalenyl)-
  • 1-(4-Methoxy-1-naphthalenyl)-ethanone
  • 1-(4-Methoxy-1-naphthyl)ethanone
  • 1-(4-methoxynaphthalen-1-yl)ethanone
  • 1-Acetyl-4-methoxynaphthalene
  • 1-(4-METHOXY-1-PHTHYL)ETHANONE
  • 4-Methoxy-1-Naphthyl Ethyl Ketone
  • 24764-66-7
  • PAHs series