ChemicalBook > CAS DataBase List > methyl 3-bromo-4-chlorobenzoate
methyl 3-bromo-4-chlorobenzoate
- Product Name
- methyl 3-bromo-4-chlorobenzoate
- CAS No.
- 107947-17-1
- Chemical Name
- methyl 3-bromo-4-chlorobenzoate
- Synonyms
- methyl 3-bromo-4-chlorobenzoate;3-Bromo-4-chlorobenzoic acid methyl ester;Benzoic acid, 3-broMo-4-chloro-, Methyl ester
- CBNumber
- CB41561290
- Molecular Formula
- C8H6BrClO2
- Formula Weight
- 249.49
- MOL File
- 107947-17-1.mol
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methyl 3-bromo-4-chlorobenzoate Property
- Boiling point:
- 280℃
- Density
- 1.604
- Flash point:
- 123℃
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Off-white to light brown Solid
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
TRC
- Product number
- M295490
- Product name
- Methyl3-bromo-4-chlorobenzoate
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
Oakwood
- Product number
- 236051
- Product name
- Methyl3-bromo-4-chlorobenzoate
- Purity
- 99%
- Packaging
- 5g
- Price
- $115
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 149516
- Product name
- Methyl 3-bromo-4-chlorobenzoate
- Purity
- 95%
- Packaging
- 5g
- Price
- $119
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FB157423
- Product name
- 3-Bromo-4-chloro-benzoic acid methyl ester
- Packaging
- 1g
- Price
- $156.2
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FB157423
- Product name
- 3-Bromo-4-chloro-benzoic acid methyl ester
- Packaging
- 2g
- Price
- $240
- Updated
- 2021/12/16
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methyl 3-bromo-4-chlorobenzoate Chemical Properties,Usage,Production
Synthesis
67-56-1
42860-10-6
107947-17-1
Example 13 13.1 Synthesis of methyl 3-bromo-4-chlorobenzoate (13.1). A round bottom flask was charged with 3-bromo-4-chlorobenzoic acid (5.0 g, 21.2 mmol, CAS No. 42860-10-6, available from Aldrich), methanol (60 mL), and a cooled sulfuric acid solution (1.4 mL). The reaction mixture was heated to 80 °C and the progress of the reaction was monitored by thin layer chromatography (TLC). After 17 hours of reaction, it was cooled to room temperature and diluted with water. The aqueous phase was extracted with ether (3 x 50 mL), the organic layers were combined and dried with anhydrous magnesium sulfate. After filtration, the organic solvent was removed by distillation under reduced pressure to give a white solid product 13.1 (5.0 g, 96% yield). The 1H NMR (400 MHz, CDCl3) data of the product were as follows: δ 8.28 (1H, d, J = 2.0 Hz), 7.93 (1H, m), 7.52 (1H, d, J = 8.2 Hz), 3.93 (3H, s).
References
[1] Patent: WO2008/130514, 2008, A1. Location in patent: Page/Page column 84-85
[2] Journal of Medicinal Chemistry, 2013, vol. 56, # 23, p. 9496 - 9508
[3] Patent: WO2013/25805, 2013, A1. Location in patent: Page/Page column 89
[4] Patent: WO2008/124610, 2008, A1. Location in patent: Page/Page column 85
methyl 3-bromo-4-chlorobenzoate Preparation Products And Raw materials
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Preparation Products
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View Lastest Price from methyl 3-bromo-4-chlorobenzoate manufacturers
Career Henan Chemical Co
- Product
- methyl 3-bromo-4-chlorobenzoate 107947-17-1
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 1000KGS
- Release date
- 2019-12-20
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