ChemicalBook > CAS DataBase List > 6-CHLORO-1H-INDOLE-2-CARBALDEHYDE

6-CHLORO-1H-INDOLE-2-CARBALDEHYDE

Product Name
6-CHLORO-1H-INDOLE-2-CARBALDEHYDE
CAS No.
53590-59-3
Chemical Name
6-CHLORO-1H-INDOLE-2-CARBALDEHYDE
Synonyms
6-CHLORO-1H-INDOLE-2-CARBALDEHYDE;1H-Indole-2-carboxaldehyde, 6-chloro-
CBNumber
CB42455352
Molecular Formula
C9H6ClNO
Formula Weight
179.6
MOL File
53590-59-3.mol
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6-CHLORO-1H-INDOLE-2-CARBALDEHYDE Property

Boiling point:
373.4±22.0 °C(Predicted)
Density 
1.431±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
14.15±0.30(Predicted)
Appearance
Light yellow to brown Solid
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Safety

HS Code 
29339900
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Biosynth Carbosynth
Product number
FC141350
Product name
6-Chloro-1H-indole-2-carbaldehyde
Packaging
100mg
Price
$84
Updated
2021/12/16
Frontier Specialty Chemicals
Product number
JK271535
Product name
6-Chloro-1H-indole-2-carbaldehyde
Purity
98%
Packaging
1g
Price
$138
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC141350
Product name
6-Chloro-1H-indole-2-carbaldehyde
Packaging
250mg
Price
$167.5
Updated
2021/12/16
Apolloscientific
Product number
OR927744
Product name
6-Chloro-1H-indole-2-carbaldehyde
Purity
95%
Packaging
1g
Price
$205
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC141350
Product name
6-Chloro-1H-indole-2-carbaldehyde
Packaging
500mg
Price
$290
Updated
2021/12/16
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6-CHLORO-1H-INDOLE-2-CARBALDEHYDE Chemical Properties,Usage,Production

Chemical Properties

Brown solid

Synthesis

53590-58-2

53590-59-3

GENERAL STEPS: A suspension of 2-hydroxymethyl-6-chloroindole (1 mmol) with activated MnO2 (10 mmol) in DMF (30 mL) was stirred at room temperature for 12 hours. After completion of the reaction, the mixture was filtered through a diatomaceous earth pad. The filtrate was concentrated under vacuum and the residue was purified by column chromatography to afford 6-chloro-1H-indole-2-carbaldehyde using EtOAc-hexane mixed solvent as eluent.

References

[1] European Journal of Medicinal Chemistry, 2016, vol. 121, p. 561 - 577
[2] Patent: US2003/144282, 2003, A1
[3] Journal of Medicinal Chemistry, 2007, vol. 50, # 6, p. 1380 - 1400
[4] Patent: US2008/9485, 2008, A1. Location in patent: Page/Page column 31
[5] Journal of Medicinal Chemistry, 2014, vol. 57, # 2, p. 364 - 377

6-CHLORO-1H-INDOLE-2-CARBALDEHYDE Preparation Products And Raw materials

Raw materials

Ethanol Manganese dioxide Diethyl oxalate Tetrahydrofuran Diethyl ether Lithium Aluminum Hydride Hydrochloric acid Acetic acid Potassium 4-Chloro-2-nitrotoluene

Preparation Products

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53590-59-3, 6-CHLORO-1H-INDOLE-2-CARBALDEHYDERelated Search:

4,6-DICHLORO-1H-INDOLE-2-CARBONYL CHLORIDE 6-Chloroindole-2-carboxylic acid ethyl ester 6-Chloroindole-2-carboxylic acid Ethyl 4,6-dichloroindole-2-carboxylate 6-CHLORO-1H-INDOLE-2-CARBOXYLIC ACID METHYL ESTER 4,6-Dichloro-1H-indole-2-carboxylic acid 4,6-DICHLORO-3-[(1E)-3-OXO-3-(PHENYLAMINO)-1-PROPENYL]-1H-INDOLE-2-CARBOXYLIC ACID SODIUM SALT ETHYL 4,6-DICHLORO-3-FORMYL-1H-INDOLE-2-CARBOXYLATE 6,7-DICHLORO-1H-INDOLE-2-CARBOXYLIC ACID ETHYL ESTER 6,7-DICHLORO-1H-INDOLE-2-CARBOXYLIC ACID (Z)-2-CARBOXY-4,6-DICHLOROINDOLE-3-(2'-PHENYL-2'-CARBOXY)-ENE ETHYL 3-(2-CARBOXY-VINYL)-4,6-DICHLORO-1H-INDOLE-2-CARBOXYLATE 6-CHLORO-4-FLUORO-1H-INDOLE-2-CARBOXYLIC ACID 6-CHLORO-7-METHYL-1H-INDOLE-2-CARBOXYLIC ACID ALPHA-PHENYL-1-(2-PHENYLETHYL)-4-PIPERIDINEMETHANOL 1H-INDOLE-2-CARBOXYLIC ACID,6-CHLORO-4-FLUORO-3-FORMYL-,ETHYL ESTER 1-(beta-Dimethylaminoaethyl)-2-ethoxycarbonyl-3-ethoxy-6-chlor-indol-t oluol-4-sulfonat 4,6-DICHLORO-3-HYDROXYMETHYL-1H-INDOLE-2-CARBOXYLIC ACID ETHYL ESTER

  • 6-CHLORO-1H-INDOLE-2-CARBALDEHYDE
  • 1H-Indole-2-carboxaldehyde, 6-chloro-
  • 53590-59-3