Trifluoromethanesulfonyl chloride

Product Name: Trifluoromethanesulfonyl chloride
CAS No.: 421-83-0
Chemical Name: Trifluoromethanesulfonyl chloride
Synonyms: TRIFLYL CHLORIDE;PFC-MSC;Trifluoromethane chloride;TRIFLUOROMETHANESULFONYLCLORIDE;trifluoromethylsulfonyl chloride;Trifluoromethanesufonyl chloride;RIFLUOROMETHANESULFONYL CHLORIDE;Trifluoromathanesulfonyl chloride;TRIFLUOROMETHANESULFONYL CHLORIDE;Trifluoromethylsulphonyl chloride
CBNumber: CB4253800
Molecular Formula: CClF3O2S
Formula Weight: 168.52
MOL File: 421-83-0.mol

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Trifluoromethanesulfonyl chloride Property

Melting point:: -26 °C
Boiling point:: 29-32 °C (lit.)
Density: 1.583 g/mL at 25 °C (lit.)
vapor pressure: 10.36 psi ( 20 °C)
refractive index: n20/D 1.334(lit.)
Flash point:: 32°C
storage temp.: 2-8°C
solubility: Chloroform
form: Liquid
color: Clear colorless to faintly colored
Specific Gravity: 1.583
Water Solubility: Hydrolyzes with water.
Sensitive: Lachrymatory
BRN: 1812016
InChIKey: GRGCWBWNLSTIEN-UHFFFAOYSA-N
CAS DataBase Reference: 421-83-0(CAS DataBase Reference)

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Safety

Hazard Codes: C
Risk Statements: 14-34
Safety Statements: 26-36/37/39-45
RIDADR: UN 3265 8/PG 2
WGK Germany: 3
F: 10-21
Hazard Note: Corrosive/Lachrymatory
HazardClass: 8
PackingGroup: II
HS Code: 29049090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H314Causes severe skin burns and eye damage

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P363Wash contaminated clothing before reuse.

P405Store locked up.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 164798
Product name: Trifluoromethanesulfonyl chloride
Purity: ≥99%
Packaging: 5g
Price: $79.3
Updated: 2024/03/01

Sigma-Aldrich

Product number: 164798
Product name: Trifluoromethanesulfonyl chloride
Purity: ≥99%
Packaging: 25g
Price: $263
Updated: 2024/03/01

TCI Chemical

Product number: T1027
Product name: Trifluoromethanesulfonyl Chloride
Purity: >98.0%(GC)
Packaging: 5g
Price: $65
Updated: 2024/03/01

TCI Chemical

Product number: T1027
Product name: Trifluoromethanesulfonyl Chloride
Purity: >98.0%(GC)
Packaging: 25g
Price: $204
Updated: 2024/03/01

Alfa Aesar

Product number: B21774
Product name: Trifluoromethanesulfonyl chloride
Purity: 98%
Packaging: 5g
Price: $72.9
Updated: 2024/03/01

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Trifluoromethanesulfonyl chloride Chemical Properties,Usage,Production

Chemical Properties

Clear colorless to faintly colored liquid

Uses

Ru(II) complex-catalyzed trifluoromethylating agent for aromatics and alkenes.

Application

Trifluoromethanesulfonyl chloride can be used as:
A trifluoromethylating agent for the fluoroalkylation of heterocycles, arenes, and heteroarenes.
A sulfonating agent for alcohols.
A chlorinating agent for carbanions.

Synthesis

Add 150g (1mol) of trifluoromethanesulfonic acid to the reactor equipped with thermometer, distillation device and mechanical stirrer, slowly add 435mL (6mol) of thionyl chloride under ice bath, and then add the catalyst N,N-dimethyl Formamide 7.36 (0.1 mol), slowly raise the temperature to room temperature, stir for half an hour, continue to heat up to 40°C, continue to stir, react for 12 hours, and then drop to room temperature after the reaction is complete.Subsequently, vacuum distillation was carried out at 110° C. and -0.1 to -0.08 MPa, and at the same time, the temperature was slowly raised to 50° C. to obtain 147 g of trifluoromethanesulfonyl chloride, with a yield of 87.5%.

Trifluoromethanesulfonyl chloride Preparation Products And Raw materials

Raw materials

Preparation Products

N-Phenyl-bis(trifluoromethanesulfonimide)

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Trifluoromethanesulfonyl chloride Suppliers

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View Lastest Price from Trifluoromethanesulfonyl chloride manufacturers

Shandong Deshang Chemical Co., Ltd.

Product: Trifluoromethanesulfonyl chloride 421-83-0
Price: US $10.00-7.00/kg
Min. Order: 1kg
Purity: 99.99%
Supply Ability: 10 tons
Release date: 2024-06-14

Hebei Weibang Biotechnology Co., Ltd

Product: TRIFLUOROMETHANESULFONYL CHLORIDE 421-83-0
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20 mt
Release date: 2024-11-06

airuikechemical co., ltd.

Product: trifluoromethanesulfonyl chloride 421-83-0
Price: US $0.00-0.00/Kg
Min. Order: 1Kg
Purity: 99.9%
Supply Ability: 200tons
Release date: 2024-04-09

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421-83-0

421-86-0

CClF3O2S

CF3SO2Cl

C3F4l2

CF3ClO2S

CClF3SO2

Protection and Derivatization

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organofluorine compounds

Others

Protecting and Derivatizing Reagents

Protection and Derivatization