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2-Bromo-9-phenyl-9H-carbazole

Product Name
2-Bromo-9-phenyl-9H-carbazole
CAS No.
94994-62-4
Chemical Name
2-Bromo-9-phenyl-9H-carbazole
Synonyms
2-Bromo-9-phenylcarbazole;2-Brom-xanthen-9-on;2-bromo-N-phenylcoumarin;2-BroMo-N-phenylcarbazole;N-Phenyl-2-bromocarbazole;2-Bromo-9-phenyl-9H-carba;Phenyl-2-bromo-N- carbazole;2-Bromo-9-phenyl-9H-carbazol;Carbazole, 2-bromo-9-phenyl-;2-Bromo-9-phenyl-9H-carbazole
CBNumber
CB42614371
Molecular Formula
C18H12BrN
Formula Weight
322.2
MOL File
94994-62-4.mol
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2-Bromo-9-phenyl-9H-carbazole Property

Melting point:
88.0 to 92.0 °C
Boiling point:
461.7±27.0 °C(Predicted)
Density 
1.39
storage temp. 
Sealed in dry,Room Temperature
form 
powder to crystal
color 
White to Almost white
InChI
InChI=1S/C18H12BrN/c19-13-10-11-16-15-8-4-5-9-17(15)20(18(16)12-13)14-6-2-1-3-7-14/h1-12H
InChIKey
SOODLDGRGXOSTA-UHFFFAOYSA-N
SMILES
N1(C2=CC=CC=C2)C2=C(C=CC=C2)C2=C1C=C(Br)C=C2
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Safety

HS Code 
2933.99.8290
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TCI Chemical
Product number
B4439
Product name
2-Bromo-9-phenylcarbazole
Purity
>98.0%(GC)(N)
Packaging
1g
Price
$37
Updated
2025/07/31
TCI Chemical
Product number
B4439
Product name
2-Bromo-9-phenylcarbazole
Purity
>98.0%(GC)(N)
Packaging
5g
Price
$110
Updated
2025/07/31
TRC
Product number
B678358
Product name
2-Bromo-9-phenyl-9H-carbazole
Packaging
500mg
Price
$175
Updated
2021/12/16
AK Scientific
Product number
J57244
Product name
2-Bromo-9-phenyl-9H-carbazole
Packaging
25g
Price
$189
Updated
2021/12/16
Chem-Impex
Product number
30932
Product name
2-Bromo-9-phenylcarbazole,≥98%(GC)
Purity
≥98%(GC)
Packaging
1G
Price
$50.17
Updated
2021/12/16
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2-Bromo-9-phenyl-9H-carbazole Chemical Properties,Usage,Production

Chemical Properties

off-white powder

Uses

2-Bromo-9-phenyl-9H-carbazole is used as a reactant for the preparation of OLED screens and electronic devices.

Synthesis

3652-90-2

591-50-4

94994-62-4

2-Bromocarbazole (10 mmol), iodobenzene (20 mmol), potassium carbonate (20 mmol), L-proline (2 mmol), copper(I) iodide (1 mmol), and dimethyl sulfoxide (25 mL) were added to the pressure vessel. After evacuation and replacement with nitrogen three times, the vessel was sealed and the reaction was stirred at 90°C for 72 hours. After completion of the reaction, it was cooled to room temperature, the reaction mixture was diluted with dichloromethane (200 mL), washed four times sequentially with water (200 mL) and the organic phase was dried with anhydrous magnesium sulfate. After concentration under reduced pressure to remove the solvent, the crude product was purified by silica gel column chromatography using hexane as eluent to give 2-bromo-9-phenyl-9H-carbazole in 85% yield.

References

[1] Patent: WO2013/122402, 2013, A1. Location in patent: Paragraph 196; 201; 202
[2] Patent: WO2013/162284, 2013, A1. Location in patent: Paragraph 164; 165
[3] Journal of Materials Chemistry, 2012, vol. 22, # 1, p. 215 - 224
[4] Patent: WO2015/99484, 2015, A1. Location in patent: Paragraph 181-182
[5] Patent: WO2014/3440, 2014, A1. Location in patent: Paragraph 172; 173; 178; 179

2-Bromo-9-phenyl-9H-carbazole Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Bromo-9-phenyl-9H-carbazole Suppliers

Americas 1 China 180 Europe 1 India 2 Japan 1 United States 4 Global 189
TCI AMERICA
Tel
800-4238616
Fax
+1-888-520-1075 / +1-503-283-1987
Email
sales@tciamerica.com
Country
Americas
ProdList
23653
Advantage
75
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View Lastest Price from 2-Bromo-9-phenyl-9H-carbazole manufacturers

Hebei Chuanghai Biotechnology Co., Ltd
Product
2-Bromo-9-phenyl-9H-carbazole 94994-62-4
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
5tons
Release date
2024-12-04
Shanghai Daken Advanced Materials Co.,Ltd
Product
9H-Carbazole, 2-bromo-9-phenyl- 94994-62-4
Price
US $0.00/KG
Min. Order
1KG
Purity
98.00%
Supply Ability
150KG /month
Release date
2021-11-17
Henan Fengda Chemical Co., Ltd
Product
2-Bromo-9-phenyl-9H-carbazole 94994-62-4
Price
US $200.00-1.00/KG
Min. Order
1KG
Purity
99%, 99.5% Sublimated
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-31

94994-62-4, 2-Bromo-9-phenyl-9H-carbazoleRelated Search:

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