ChemicalBook > CAS DataBase List > 3-Methoxy-5-nitrobenzotrifluoride

3-Methoxy-5-nitrobenzotrifluoride

Product Name: 3-Methoxy-5-nitrobenzotrifluoride
CAS No.: 328-79-0
Chemical Name: 3-Methoxy-5-nitrobenzotrifluoride
Synonyms: TIMTEC-BB SBB010016;3-METHOXY-5-NITROBENZOTRIFLUORIDE;5-methoxy-3-nitrobenzotrifluoride;3-Nitro-5-(trifluoroMethyl)anisole;3-Methoxy-5-nitrobenzotrifluoride99%;3-Methoxy-5-nitrobenzotrifluoride 99%;1-Methoxy-3-nitro-5-(trifluoromethyl)benzene;Benzene, 1-methoxy-3-nitro-5-(trifluoromethyl)-
CBNumber: CB4270562
Molecular Formula: C8H6F3NO3
Formula Weight: 221.13
MOL File: 328-79-0.mol

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3-Methoxy-5-nitrobenzotrifluoride Property

Melting point:: 36-38 °C (lit.)
Boiling point:: 246.9±40.0 °C(Predicted)
Density: 1.392±0.06 g/cm3(Predicted)
Flash point:: >230 °F
storage temp.: 2-8°C
form: solid
color: Low-mwlting
CAS DataBase Reference: 328-79-0(CAS DataBase Reference)
NIST Chemistry Reference: 3-Methoxy-5-nitrobenzotrifluoride(328-79-0)

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Safety

Hazard Codes: C,Xi
Risk Statements: 34-36/38-21/22
Safety Statements: 26-27-28-36/37/39-45
RIDADR: UN 1759 8/PG 2
WGK Germany: 3
Hazard Note: Irritant
HazardClass: 8
PackingGroup: III
HS Code: 2909309090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H314Causes severe skin burns and eye damage

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P363Wash contaminated clothing before reuse.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 303674
Product name: 3-Methoxy-5-nitrobenzotrifluoride
Purity: 99%
Packaging: 5g
Price: $51.5
Updated: 2023/06/20

TRC

Product number: M327028
Product name: 3-Methoxy-5-nitrobenzotrifluoride
Packaging: 500mg
Price: $65
Updated: 2021/12/16

TRC

Product number: M327028
Product name: 3-Methoxy-5-nitrobenzotrifluoride
Packaging: 100mg
Price: $45
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0023699
Product name: 3-METHOXY-5-NITROBENZOTRIFLUORIDE
Purity: 95.00%
Packaging: 1G
Price: $597.87
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0023699
Product name: 3-METHOXY-5-NITROBENZOTRIFLUORIDE
Purity: 95.00%
Packaging: 5G
Price: $803.15
Updated: 2021/12/16

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3-Methoxy-5-nitrobenzotrifluoride Chemical Properties,Usage,Production

Uses

3-Methoxy-5-nitrobenzotrifluoride may be used in chemical synthesis.

Synthesis

401-99-0

124-41-4

328-79-0

To a solution of 3,5-dinitrobenzotrifluoride (10 g, 42.4 mmol) in anhydrous methanol (100 mL) was slowly added a solution of sodium methanolate (3.43 g, 63.5 mmol) in anhydrous methanol (20 mL). The reaction mixture was heated to reflux for 1 hour and subsequently concentrated by rotary evaporation to remove the methanol solvent. The concentrated residue was diluted with ethyl acetate (80 mL) and water (30 mL) to separate the organic phase. The organic phase was dried over anhydrous sodium sulfate (Na2SO4), filtered and concentrated to give 3-nitro-5-(trifluoromethyl)anisole (8.5 g) as a red solid. The product was analyzed by LC-MS (ESI): no [M + H]+ peak was observed; retention time was 1.85 min.

References

[1] Journal of the Chemical Society, 1951, p. 2013,2016
[2] Journal of the American Chemical Society, 1955, vol. 77, p. 2284,2285
[3] Patent: WO2013/13503, 2013, A1. Location in patent: Page/Page column 43

3-Methoxy-5-nitrobenzotrifluoride Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-Methoxy-5-nitrobenzotrifluoride manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 3-Methoxy-5-nitrobenzotrifluoride 328-79-0
Price: US $0.00-0.00/KG
Min. Order: 10mg
Purity: 99%HPLC
Supply Ability: 2000tons
Release date: 2020-01-10

Honest Joy Holdings Limited

Product: 3-Methoxy-5-nitrobenzotrifluoride 328-79-0
Price: US $0.00/KG
Min. Order: 1KG
Purity: 97.8%
Supply Ability: 100 tons
Release date: 2022-02-18

Career Henan Chemical Co

Product: 3-Methoxy-5-nitrobenzotrifluoride 328-79-0
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 1000KGS
Release date: 2019-12-24

328-79-0, 3-Methoxy-5-nitrobenzotrifluorideRelated Search:

Benzotrifluoride 3-Fluorobenzotrifluoride 4-Nitrotoluene 2-Chloro-5-nitrobenzotrifluoride 2-Nitrotoluene (Trifluoromethoxy)benzene 2-Methylbenzotrifluoride 4-(Trifluoromethoxy)aniline TRITON 3-METHYL-5-NITRO PHENOL 3-Nitrobenzotrifluoride 3-Nitro-5-(trifluoromethyl)phenol 3-AMINO-5-METHYL PHENOL 3-(Trifluoromethyl)anisole 3-Nitroanisole 3-Methoxy-5-(trifluoromethyl)aniline 4-Methoxy-3-nitrobenzotrifluoride98%,4-METHOXY-3-NITROBENZOTRIFLUORIDE,4-METHOXY-3-NITROBENZOTRIFLUORIDE 99% alpha,alpha,alpha-Trifluoro-o-cresol

TIMTEC-BB SBB010016

1-Methoxy-3-nitro-5-(trifluoromethyl)benzene

3-Methoxy-5-nitrobenzotrifluoride 99%

3-Methoxy-5-nitrobenzotrifluoride99%

5-methoxy-3-nitrobenzotrifluoride

3-METHOXY-5-NITROBENZOTRIFLUORIDE

3-Nitro-5-(trifluoroMethyl)anisole

Benzene, 1-methoxy-3-nitro-5-(trifluoromethyl)-

328-79-0

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Nitrogen Compounds

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Nitro Compounds

Nitrogen Compounds

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