ChemicalBook > CAS DataBase List > Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl-

Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl-

Product Name: Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl-
CAS No.: 1333316-35-0
Chemical Name: Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl-
Synonyms: 2,7-dibromo-9,9-dimethylacridan;2,7-Dibromo-9,9-dimethylacridine;2,7-dibromo-9,9-dimethyl-9,10-dihydroacridine;2,7-dibroMo-9,10-dihydro-9,9-diMethyl-Acridine;Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl-
CBNumber: CB42728876
Molecular Formula: C15H13Br2N
Formula Weight: 367.08
MOL File: 1333316-35-0.mol

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Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl- Property

Boiling point:: 416.7±45.0 °C(Predicted)
Density: 1.576±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
solubility: Chloroform; Dichloromethane; DMSO
pka: 0.46±0.40(Predicted)
form: Solid
color: Light Green

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: D426570
Product name: 2,7-Dibromo-9,10-dihydro-9,9-dimethylacridine
Packaging: 100mg
Price: $60
Updated: 2021/12/16

TRC

Product number: D426570
Product name: 2,7-Dibromo-9,10-dihydro-9,9-dimethylacridine
Packaging: 500mg
Price: $195
Updated: 2021/12/16

TRC

Product number: D426570
Product name: 2,7-Dibromo-9,10-dihydro-9,9-dimethylacridine
Packaging: 1g
Price: $330
Updated: 2021/12/16

AK Scientific

Product number: 4472DT
Product name: 2,7-Dibromo-9,9-dimethyl-9,10-dihydroacridine
Packaging: 1g
Price: $186
Updated: 2021/12/16

Alichem

Product number: 1333316350
Product name: 2,7-Dibromo-9,9-dimethyl-9,10-dihydroacridine
Packaging: 5g
Price: $765
Updated: 2021/12/16

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Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl- Chemical Properties,Usage,Production

Uses

2,7-Dibromo-9,10-dihydro-9,9-dimethylacridine is an intermediate in the synthesis of 2,7-Diisopropyl-9,9-dimethyl-4a,9,9a,10-tetrahydroacridine (D455760). 2,7-Diisopropyl-9,9-dimethyl-4a,9,9a,10-tetrahydroacridine is a useful chemical reagent. Also, it is derived from 9,9-Dimethyl-9,10-dihydroacridine (D474300), which are currently being used in the development of thermally activated delayed fluorescence (TADF) molecules which are being researched for their possible efficient deep-?blue TADF emitting potential.

Synthesis

6267-02-3

1333316-35-0

9,9-Dimethyl-9,10-dihydroacridine (2.7 g, 12.93 mmol) was dissolved in chloroform (200 ml) under the protection of nitrogen (by N2 purge) with continuous stirring. Subsequently, 3 equivalents of bromine were added slowly and dropwise. After 8 hours of reaction, the reaction was quenched by addition of aqueous sodium thiosulfate. The reaction mixture was then subjected to an extraction process. Purification by column chromatography using a solvent mixture of methylene chloride (MC) and hexane (1:5) as the unfolding agent resulted in 2,7-dibromo-9,9-dimethyl-9,10-dihydroacridine as a white solid (4.24 g, 90% yield).

References

[1] Patent: US2018/166636, 2018, A1. Location in patent: Paragraph 0115; 0116
[2] Patent: WO2014/165307, 2014, A2. Location in patent: Paragraph 0321

Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl- Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl- manufacturers

Hefei Lbao Physical & Chemical Science Co.,Ltd

Product: 2,7-Dibromo-9,9-dimethyl-9,10-dihydroacridine 1333316-35-0
Price: US $0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: Customise
Release date: 2025-09-16

1333316-35-0, Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl-Related Search:

DIMETHYLMERCURY Acridine 9-Phenylacridine 9-(BROMOMETHYL)ACRIDINE 9-Chloroacridine 9-AMINOACRIDINE 2-Bromo-9,10-dihydro-9,9-dimethyl-10-phenylacridine 9-ACRIDINECARBOXYLIC ACID 9-ACRIDINECARBOXYLIC ACID HYDRATE 9(10H)-ACRIDONE 9-METHYLACRIDINE 2-(9-oxoacridin-10-yl)acetic acid 9-Acridanone, 10-ethyl- NSC27927 9-Oxo-10(9H)-acridineacetic acid

Acridine, 2,7-dibroMo-9,10-dihydro-9,9-diMethyl-

2,7-dibroMo-9,10-dihydro-9,9-diMethyl-Acridine

2,7-dibromo-9,9-dimethyl-9,10-dihydroacridine

2,7-dibromo-9,9-dimethylacridan

2,7-Dibromo-9,9-dimethylacridine

1333316-35-0