ChemicalBook > CAS DataBase List > 5-NITRO-3-BROMOINDAZOLE

5-NITRO-3-BROMOINDAZOLE

Product Name: 5-NITRO-3-BROMOINDAZOLE
CAS No.: 67400-25-3
Chemical Name: 5-NITRO-3-BROMOINDAZOLE
Synonyms: 3-BROMO-5-NITROINDAZOLE;5-NITRO-3-BROMOINDAZOLE;3-bromo-5-nitro-2H-indazole;3-BROMO-5-NITRO (1H)INDAZOLE;1H-Indazole, 3-bromo-5-nitro-;3-Bro3-Bromo-5-nitroindazolemo-5-nitroindazole
CBNumber: CB4302968
Molecular Formula: C7H4BrN3O2
Formula Weight: 242.03
MOL File: 67400-25-3.mol

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5-NITRO-3-BROMOINDAZOLE Property

Melting point:: 227-229
Boiling point:: 437.3±25.0 °C(Predicted)
Density: 1.965±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
form: Powder
pka: 9.53±0.40(Predicted)
color: Pale brown

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Safety

Hazard Codes: Xi,T
Risk Statements: 25
Safety Statements: 45
RIDADR: UN2811
HazardClass: IRRITANT
HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: B695255
Product name: 3-Bromo-5-nitro-1H-indazole
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Matrix Scientific

Product number: 046878
Product name: 3-Bromo-5-nitro-1H-indazole
Purity: 95+%
Packaging: 25g
Price: $55
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140705
Product name: 3-Bromo-5-nitro-1H-indazole
Packaging: 25g
Price: $176
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140705
Product name: 3-Bromo-5-nitro-1H-indazole
Packaging: 100g
Price: $508
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140705
Product name: 3-Bromo-5-nitro-1H-indazole
Packaging: 250g
Price: $1015
Updated: 2021/12/16

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5-NITRO-3-BROMOINDAZOLE Chemical Properties,Usage,Production

Synthesis

5401-94-5

67400-25-3

Example 22 Synthesis of 3-bromo-5-nitroindazole: 5-nitroindazole (10 g, 61.3 mmol) was dissolved in acetic acid (170 mL) and heated to 80 °C. Bromine (3.1 mL, 60.7 mmol) was added slowly and dropwise. The reaction mixture was heated to reflux. After 2 hours of reaction, it was cooled to room temperature and the precipitate precipitated was collected by filtration. The filtrate was concentrated under reduced pressure to separate the additional product and the concentrated residue was partitioned between chloroform and saturated sodium bicarbonate solution, the organic phase was separated and dried over anhydrous sodium sulfate. Decompression concentration of the organic phase afforded a solid, which was combined with the aforementioned precipitate to afford the target compound 3-bromo-5-nitroindazole as a yellow solid (11.4 g, 77% yield).1H NMR (DMSO-d6) δ: 7.74 (1H, d, J=8.0 Hz), 8.21 (1H, dd, J=8.0, 1.5 Hz), 8.40 (1H, d, J=1.5 Hz), 14.5 Hz). 1.5 Hz), 14.06 (1H, brs); MS (ES-) m/z: 240 [M-H]-.

References

[1] ACS Medicinal Chemistry Letters, 2017, vol. 8, # 12, p. 1258 - 1263
[2] Patent: CN103570624, 2016, B. Location in patent: Paragraph 0019-0029
[3] Patent: US2002/103229, 2002, A1
[4] Patent: US2004/127536, 2004, A1
[5] Patent: US2005/9876, 2005, A1

5-NITRO-3-BROMOINDAZOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-NITRO-3-BROMOINDAZOLE Suppliers

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View Lastest Price from 5-NITRO-3-BROMOINDAZOLE manufacturers

Career Henan Chemical Co

Product: 5-NITRO-3-BROMOINDAZOLE 67400-25-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 150KG
Release date: 2019-07-09

67400-25-3, 5-NITRO-3-BROMOINDAZOLERelated Search:

2-FLUORO-5-NITROPHENOL Butyl 2-methylbutyrate FEMA 2200 2,8-DICHLORO-QUINOLINE-3-CARBALDEHYDE 2-Chloro-5-fluorobenzonitrile N-PHENYLETHYLENEDIAMINE Isoquinoline, 6-chloro- (6CI,9CI) Norethindrone 1-BROMO-2-CHLORO-3-NITROBENZENE 5-Nitroindazole 3-BROMO-6-NITROINDAZOLE 3-BROMO-7-NITROINDAZOLE 5-NITRO-3-BROMOINDAZOLE 3-Bromoindazole 5-AMINO-3-BROMO (1H)INDAZOLE 3-BROMO-5-NITRO-6-METHYL (1H)INDAZOLE 3-BROMO-6-CHLORO-5-NITRO (1H)INDAZOLE 3-Bromo-1-methyl-5-nitro-1H-indazole

3-BROMO-5-NITRO (1H)INDAZOLE

5-NITRO-3-BROMOINDAZOLE

3-BROMO-5-NITROINDAZOLE

3-bromo-5-nitro-2H-indazole

1H-Indazole, 3-bromo-5-nitro-

3-Bro3-Bromo-5-nitroindazolemo-5-nitroindazole

67400-25-3