ChemicalBook > CAS DataBase List > Ethyl 2-chloronicotinate
Ethyl 2-chloronicotinate
- Product Name
- Ethyl 2-chloronicotinate
- CAS No.
- 1452-94-4
- Chemical Name
- Ethyl 2-chloronicotinate
- Synonyms
- AVAC-001;oronicotinate;Ethyl 2-chloronicoti;Flunixin EP Impurity C;ETHYL 2-CHLORONICOTINATE;Ehtyl 2-chloronicotinate;ethy-2-chloroisonicoitate;Ethyl2-Chloronicotinate>Flunixin Related CoMpound C;Ethyl2-chloronicotinate,98%
- CBNumber
- CB4312224
- Molecular Formula
- C8H8ClNO2
- Formula Weight
- 185.61
- MOL File
- 1452-94-4.mol
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Ethyl 2-chloronicotinate Property
- Melting point:
- 68 C
- Boiling point:
- 78°C (0.1 mmHg)
- Density
- 1.2445 g/cm3(Temp: 25 °C)
- refractive index
- 1.5210-1.5250
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- pka
- -1.32±0.10(Predicted)
- form
- Liquid
- color
- Colorless to Light yellow to Light orange
- InChI
- InChI=1S/C8H8ClNO2/c1-2-12-8(11)6-4-3-5-10-7(6)9/h3-5H,2H2,1H3
- InChIKey
- PMIMPBYTPPRBGD-UHFFFAOYSA-N
- SMILES
- C1(Cl)=NC=CC=C1C(OCC)=O
- CAS DataBase Reference
- 1452-94-4(CAS DataBase Reference)
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Safety
- Hazard Codes
- Xi
- Risk Statements
- 36/37/38
- Safety Statements
- 26-37/39-60-37
- HazardClass
- IRRITANT
- HS Code
- 29333990
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N-Bromosuccinimide Price
Sigma-Aldrich
- Product number
- Y0000445
- Product name
- Flunixin impurity C
- Purity
- European Pharmacopoeia (EP) Reference Standard
- Packaging
- y0000445
- Price
- $153
- Updated
- 2024/03/01
Sigma-Aldrich
- Product number
- PHR2413
- Product name
- Flunixin Related Compound C
- Purity
- Pharmaceutical Secondary Standard; Certified Reference Material
- Packaging
- 50MG
- Price
- $534
- Updated
- 2024/03/01
Sigma-Aldrich
- Product number
- 1274631
- Product name
- Flunixin impurity C
- Packaging
- 50mg
- Price
- $1720
- Updated
- 2024/03/01
TCI Chemical
- Product number
- E0844
- Product name
- Ethyl 2-Chloronicotinate
- Purity
- >98.0%(GC)
- Packaging
- 25g
- Price
- $44
- Updated
- 2024/03/01
TCI Chemical
- Product number
- E0844
- Product name
- Ethyl 2-Chloronicotinate
- Purity
- >98.0%(GC)
- Packaging
- 100g
- Price
- $130
- Updated
- 2024/03/01
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Ethyl 2-chloronicotinate Chemical Properties,Usage,Production
Chemical Properties
Light yellow liquid
Uses
Ethyl 2-chloronicotinate,is used as a pharmaceutical intermediate.
Synthesis Reference(s)
Tetrahedron, 51, p. 13177, 1995 DOI: 10.1016/0040-4020(95)00788-A
Synthesis
2-Chloropyridine-3-carboxylic acid (7.9 g) and thionyl chloride (45 ml) were heated for 3 hours in benzene (65 ml) under reflux. The reaction mixture was concentrated to leave an oil, which was added dropwise to ethanol (40 ml). The mixture was heated for a further one hour under reflux. The solvent was distilled, and the residue was dissolved in toluene. The solution was dried over anhydrous magnesium sulfate. The solvent was distilled to leave Ethyl 2-chloronicotinate (8.4 g, 90%) as a pale yellow oil.
Ethyl 2-chloronicotinate Preparation Products And Raw materials
Raw materials
Preparation Products
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Ethyl 2-chloronicotinate Suppliers
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View Lastest Price from Ethyl 2-chloronicotinate manufacturers
Hebei Zhuanglai Chemical Trading Co.,Ltd
- Product
- Ethyl 2-chloronicotinate 1452-94-4
- Price
- US $10.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20ton
- Release date
- 2024-06-05
WUHAN FORTUNA CHEMICAL CO., LTD
- Product
- Ethyl 2-chloronicotinate 1452-94-4
- Price
- US $0.00/KG
- Min. Order
- 200KG
- Purity
- 98%min
- Supply Ability
- 30tons/month
- Release date
- 2023-01-11
Shaanxi Dideu Medichem Co. Ltd
- Product
- Ethyl 2-chloronicotinate 1452-94-4
- Price
- US $4656.00/KG
- Min. Order
- 1KG
- Purity
- 99.0%
- Supply Ability
- 1000 tons
- Release date
- 2024-07-25
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