1-AMINO-CYCLOBUTANECARBOXYLIC ACID METHYL ESTER
- Product Name
- 1-AMINO-CYCLOBUTANECARBOXYLIC ACID METHYL ESTER
- CAS No.
- 215597-35-6
- Chemical Name
- 1-AMINO-CYCLOBUTANECARBOXYLIC ACID METHYL ESTER
- Synonyms
- 1, 1-ACCB(OME);Methyl 1-aMinocyclobutanecarboxylate;methyl 1-aminocyclobutane-1-carboxylate;1-AMINO-CYCLOBUTANECARBOXYLIC ACID METHYL ESTER;Cyclobutanecarboxylic acid, 1-aMino-, Methyl ester;Cyclobutanecarboxylic acid, 1-amino-, methyl ester (9CI);1-AMINO-CYCLOBUTANECARBOXYLIC ACID METHYL ESTER USP/EP/BP;Cyclobutanecarboxylicacid, 1-amino-, methyl ester, hydrochlo...
- CBNumber
- CB4710963
- Molecular Formula
- C6H11NO2
- Formula Weight
- 129.16
- MOL File
- 215597-35-6.mol
1-AMINO-CYCLOBUTANECARBOXYLIC ACID METHYL ESTER Property
- Boiling point:
- 162.3±23.0 °C(Predicted)
- Density
- 1.127±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
- pka
- 7.71±0.20(Predicted)
- form
- Solid
- Appearance
- Colorless to light yellow Liquid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- A596345
- Product name
- 1-Amino-cyclobutanecarboxylicacidmethylester
- Packaging
- 250mg
- Price
- $240
- Updated
- 2021/12/16
- Product number
- FA148096
- Product name
- 1-Amino-cyclobutanecarboxylic acid methylester
- Packaging
- 500mg
- Price
- $590
- Updated
- 2021/12/16
- Product number
- 074125
- Product name
- 1-Amino-cyclobutanecarboxylic acid methyl ester
- Purity
- 95+%
- Packaging
- 5g
- Price
- $825
- Updated
- 2021/12/16
- Product number
- CHM0017688
- Product name
- 1-AMINO-CYCLOBUTANECARBOXYLIC ACID METHYL ESTER
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $1136.52
- Updated
- 2021/12/16
- Product number
- W4473
- Product name
- 1-Amino-cyclobutanecarboxylicacidmethylester
- Packaging
- 5g
- Price
- $1163
- Updated
- 2021/12/16
1-AMINO-CYCLOBUTANECARBOXYLIC ACID METHYL ESTER Chemical Properties,Usage,Production
Synthesis
67-56-1
120728-10-1
215597-35-6
Stage 1: Synthesis of methyl 1-aminocyclobutanecarboxylate Concentrated H2SO4 (10 ml) was slowly added to a methanol solution (30 ml) containing 1-(tert-butoxycarbonylamino)-cyclobutane-1-carboxylic acid (9.29 mmol, 1 eq.) at 0°C. The reaction mixture was refluxed at 0°C for 2 hours. After completion of the reaction, the solvent was removed by distillation under reduced pressure. The residue was dissolved in distilled water and the pH was adjusted to 8-9 with saturated sodium bicarbonate solution, followed by extraction with ethyl acetate (2 x 200 ml). The combined organic phases were washed sequentially with distilled water (2 x 150 ml) and saturated NaCl solution (2 x 50 ml) and dried with anhydrous sodium sulfate. Finally, the solvent was removed by concentration under reduced pressure to afford methyl 1-aminocyclobutanecarboxylate as a white solid in 75% yield.
References
[1] Patent: US2010/173889, 2010, A1. Location in patent: Page/Page column 34
1-AMINO-CYCLOBUTANECARBOXYLIC ACID METHYL ESTER Preparation Products And Raw materials
Raw materials
Preparation Products
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