ChemicalBook > CAS DataBase List > 3-(2-METHOXYPHENYL)PROPIONIC ACID

3-(2-METHOXYPHENYL)PROPIONIC ACID

Product Name: 3-(2-METHOXYPHENYL)PROPIONIC ACID
CAS No.: 6342-77-4
Chemical Name: 3-(2-METHOXYPHENYL)PROPIONIC ACID
Synonyms: AKOS BC-2706;3-(2-Methoxyphenyl;TIMTEC-BB SBB003749;guaiacylpropionic acid;O-METHOXYHYDROCINNAMIC ACID;2-METHOXYHYDROCINNAMIC ACID;3-(2-methoxyphenyl)propanoate;2-Methoxybenzenepropionic acid;2-Methoxybenzenepropanoic acid;Benzenpropionic acid, 2-methoxy
CBNumber: CB4771988
Molecular Formula: C10H12O3
Formula Weight: 180.2
MOL File: 6342-77-4.mol

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3-(2-METHOXYPHENYL)PROPIONIC ACID Property

Melting point:: 85-87 °C (lit.)
Boiling point:: 273.02°C (rough estimate)
Density: 1.1272 (rough estimate)
refractive index: 1.5160 (estimate)
storage temp.: Sealed in dry,Room Temperature
pka: pK1:4.804 (25°C)
Appearance: White to off-white Solid
BRN: 2097012
InChI: InChI=1S/C10H12O3/c1-13-9-5-3-2-4-8(9)6-7-10(11)12/h2-5H,6-7H2,1H3,(H,11,12)
InChIKey: XSZSNLOPIWWFHS-UHFFFAOYSA-N
SMILES: C1(CCC(O)=O)=CC=CC=C1OC
CAS DataBase Reference: 6342-77-4(CAS DataBase Reference)

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Safety

Safety Statements: 22-24/25
WGK Germany: 3
HazardClass: IRRITANT
HS Code: 29189990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

SynQuest Laboratories

Product number: 2721-1-38
Product name: 3-(2-Methoxyphenyl)propionic acid
Packaging: 1g
Price: $21
Updated: 2021/12/16

Matrix Scientific

Product number: 037484
Product name: 3-(2-Methoxyphenyl)propanoic acid
Packaging: 5g
Price: $31
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2721-1-38
Product name: 3-(2-Methoxyphenyl)propionic acid
Packaging: 5G
Price: $42
Updated: 2021/12/16

Matrix Scientific

Product number: 037484
Product name: 3-(2-Methoxyphenyl)propanoic acid
Packaging: 25g
Price: $110
Updated: 2021/12/16

Apolloscientific

Product number: OR909100
Product name: 3-(2-Methoxyphenyl)propionic acid
Purity: 98%
Packaging: 25g
Price: $145
Updated: 2021/12/16

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3-(2-METHOXYPHENYL)PROPIONIC ACID Chemical Properties,Usage,Production

Chemical Properties

WHITE FINE CRYSTALLINE POWDER

Definition

ChEBI: 3-(2-Methoxyphenyl)propanoic acid is a monocarboxylic acid and a member of benzenes.

Synthesis

1011-54-7

6342-77-4

GENERAL METHOD: (E)-3-(2-methoxyphenyl)acrylic acid (1.0 mmol, 0.148 g), catalyst BPPd(0)Si (5 mol%, 0.0836 g), and KOH (1.0 eq., 5 mL of 0.2 M solution) were added to the reaction mixture and reacted under hydrogen (1 atm) atmosphere. After the reaction mixture was stirred at room temperature for 30 min, the catalyst was removed by filtration and the filtrate was washed with 10 mL of water and ethyl acetate. The pH of the filtrate was adjusted to 2-3 with 1 N HCl. Subsequently, the organic phase was collected by solvent extraction with ethyl acetate and dried with MgSO4. The dried organic phase was concentrated under reduced pressure and the resulting crude product was purified by silica gel column chromatography and the final product was structurally confirmed by 1H NMR spectroscopy.

References

[1] Journal of Organometallic Chemistry, 2017, vol. 846, p. 296 - 304
[2] Tetrahedron, 1989, vol. 45, # 5, p. 1441 - 1446
[3] Journal of Medicinal Chemistry, 1993, vol. 36, # 20, p. 2891 - 2898
[4] Bioorganic Chemistry, 2018, vol. 80, p. 408 - 421
[5] Bioorganic and Medicinal Chemistry Letters, 2000, vol. 10, # 14, p. 1519 - 1522

3-(2-METHOXYPHENYL)PROPIONIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

3-(2-METHOXY-PHENYL)-PROPIONYL CHLORIDE

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View Lastest Price from 3-(2-METHOXYPHENYL)PROPIONIC ACID manufacturers

Career Henan Chemical Co

Product: 3-(2-METHOXYPHENYL)PROPIONIC ACID 6342-77-4
Price: US $8.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 100KG
Release date: 2018-12-15

6342-77-4, 3-(2-METHOXYPHENYL)PROPIONIC ACIDRelated Search:

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3-(2-Methoxyphenyl

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TIMTEC-BB SBB003749

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3-(O-METHOXYPHENYL)PROPIONIC ACID

AKOS BC-2706

2-METHOXYHYDROCINNAMIC ACID

3-(2-METHOXYPHENYL)PROPANOIC ACID

3-(2-METHOXYPHENYL)PROPIONIC ACID

Benzenepropanoic acid, 2-methoxy-

Benzenpropionic acid, 2-methoxy

3-(2-Methoxyphenyl)propionic acid, 98+%

guaiacylpropionic acid

3-(2-METHOXYPHENYL)-PROPIONIC ACID 98%

2-Methoxybenzenepropanoic acid

3-(2-methoxyphenyl)propanoate

6342-77-4

Organic Building Blocks

Building Blocks

C10

Carboxylic Acids

Carbonyl Compounds

Aromatic Propionic Acids