3-METHOXY-5-NITROBENZALDEHYDE

Product Name: 3-METHOXY-5-NITROBENZALDEHYDE
CAS No.: 354512-22-4
Chemical Name: 3-METHOXY-5-NITROBENZALDEHYDE
Synonyms: 3-METHOXY-5-NITROBENZALDEHYDE;Benzaldehyde, 3-methoxy-5-nitro-
CBNumber: CB4787943
Molecular Formula: C8H7NO4
Formula Weight: 181.15
MOL File: 354512-22-4.mol

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3-METHOXY-5-NITROBENZALDEHYDE Property

Melting point:: 96 °C
Boiling point:: 326.5±27.0 °C(Predicted)
Density: 1.322±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M493005
Product name: 3-Methoxy-5-nitrobenzaldehyde
Packaging: 10mg
Price: $65
Updated: 2021/12/16

AK Scientific

Product number: 4421AB
Product name: 3-Methoxy-5-nitrobenzaldehyde
Packaging: 250mg
Price: $367
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0372504
Product name: 3-METHOXY-5-NITROBENZALDEHYDE
Purity: 95.00%
Packaging: 5MG
Price: $502.5
Updated: 2021/12/16

Alichem

Product number: 354512224
Product name: 3-Methoxy-5-nitrobenzaldehyde
Packaging: 1g
Price: $1519.8
Updated: 2021/12/16

Chemcia Scientific

Product number: BB20-8034
Product name: 3-Methoxy-5-nitro-benzaldehyde
Purity: 95%
Packaging: 0.5g
Price: $335
Updated: 2021/12/16

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3-METHOXY-5-NITROBENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

354525-36-3

354512-22-4

Step 3. (3-methoxy-5-nitrophenyl)methanol (75 g, 0.41 mol) was dissolved in dichloromethane (1.5 L) and cooled below 10°C. Under stirring, pyridinium dichromate (382 g, 1.02 mol) and silica gel (382 g) were added in batches. After addition, the reaction mixture was brought to room temperature and stirring was continued for 3 hours. The progress of the reaction was monitored by thin layer chromatography (TLC) (Expanding agent: petroleum ether/ethyl acetate = 3:1, Rf = 0.6) to confirm the complete conversion of the raw material. Upon completion of the reaction, the crude product was purified by fast column chromatography (eluent: dichloromethane) to afford 3-methoxy-5-nitrobenzaldehyde as a yellow solid (170 g, 76% yield in 3 batches).

References

[1] Patent: WO2013/148365, 2013, A1. Location in patent: Paragraph 0095
[2] Journal of Medicinal Chemistry, 2004, vol. 47, # 11, p. 2897 - 2905
[3] MedChemComm, 2018, vol. 9, # 8, p. 1293 - 1304

3-METHOXY-5-NITROBENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-METHOXY-5-NITROBENZALDEHYDE Suppliers

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354512-22-4, 3-METHOXY-5-NITROBENZALDEHYDERelated Search:

3,4-DIMETHOXY-5-NITRO-BENZOIC ACID 2-HYDROXY-3-METHOXY-5-NITROBENZALDEHYDE 2-HYDROXY-5-METHOXY-3-NITRO-BENZALDEHYDE 3-METHOXY-5-NITROBENZOIC ACID 2,5-DIMETHOXY-3-NITROBENZOIC ACID 5-Nitrovanillin 2,3-dimethoxy-5-nitro-benzaldehyde CHEMBRDG-BB 6755049 CHEMBRDG-BB 6744545 CHEMBRDG-BB 6742514 3-ETHOXY-4-HYDROXY-5-NITROBENZALDEHYDE METHYL 3-METHOXY-5-NITROBENZOATE CHEMBRDG-BB 6766958 RARECHEM AL BE 0173 SALOR-INT L170909-1EA 3-NITRODIBENZO[B,F]OXEPINE-1-CARBOXYLIC ACID RARECHEM AL BE 0234 3-ETHOXY-2-HYDROXY-5-NITROBENZALDEHYDE

3-METHOXY-5-NITROBENZALDEHYDE

Benzaldehyde, 3-methoxy-5-nitro-

354512-22-4