3-METHOXY-5-NITROBENZALDEHYDE
- Product Name
- 3-METHOXY-5-NITROBENZALDEHYDE
- CAS No.
- 354512-22-4
- Chemical Name
- 3-METHOXY-5-NITROBENZALDEHYDE
- Synonyms
- 3-METHOXY-5-NITROBENZALDEHYDE;Benzaldehyde, 3-methoxy-5-nitro-
- CBNumber
- CB4787943
- Molecular Formula
- C8H7NO4
- Formula Weight
- 181.15
- MOL File
- 354512-22-4.mol
3-METHOXY-5-NITROBENZALDEHYDE Property
- Melting point:
- 96 °C
- Boiling point:
- 326.5±27.0 °C(Predicted)
- Density
- 1.322±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M493005
- Product name
- 3-Methoxy-5-nitrobenzaldehyde
- Packaging
- 10mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- 4421AB
- Product name
- 3-Methoxy-5-nitrobenzaldehyde
- Packaging
- 250mg
- Price
- $367
- Updated
- 2021/12/16
- Product number
- CHM0372504
- Product name
- 3-METHOXY-5-NITROBENZALDEHYDE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $502.5
- Updated
- 2021/12/16
- Product number
- A238638
- Product name
- 3-Methoxy-5-nitrobenzaldehyde
- Purity
- 95%
- Packaging
- 100mg
- Price
- $15
- Updated
- 2021/12/16
- Product number
- A238638
- Product name
- 3-Methoxy-5-nitrobenzaldehyde
- Purity
- 95%
- Packaging
- 250mg
- Price
- $25
- Updated
- 2021/12/16
3-METHOXY-5-NITROBENZALDEHYDE Chemical Properties,Usage,Production
Synthesis
354525-36-3
354512-22-4
Step 3. (3-methoxy-5-nitrophenyl)methanol (75 g, 0.41 mol) was dissolved in dichloromethane (1.5 L) and cooled below 10°C. Under stirring, pyridinium dichromate (382 g, 1.02 mol) and silica gel (382 g) were added in batches. After addition, the reaction mixture was brought to room temperature and stirring was continued for 3 hours. The progress of the reaction was monitored by thin layer chromatography (TLC) (Expanding agent: petroleum ether/ethyl acetate = 3:1, Rf = 0.6) to confirm the complete conversion of the raw material. Upon completion of the reaction, the crude product was purified by fast column chromatography (eluent: dichloromethane) to afford 3-methoxy-5-nitrobenzaldehyde as a yellow solid (170 g, 76% yield in 3 batches).
References
[1] Patent: WO2013/148365, 2013, A1. Location in patent: Paragraph 0095
[2] Journal of Medicinal Chemistry, 2004, vol. 47, # 11, p. 2897 - 2905
[3] MedChemComm, 2018, vol. 9, # 8, p. 1293 - 1304
3-METHOXY-5-NITROBENZALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
3-METHOXY-5-NITROBENZALDEHYDE Suppliers
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