ChemicalBook > CAS DataBase List > 2,3-Dibromo-5-chloropyridine

2,3-Dibromo-5-chloropyridine

Product Name
2,3-Dibromo-5-chloropyridine
CAS No.
137628-17-2
Chemical Name
2,3-Dibromo-5-chloropyridine
Synonyms
2,3-Dibromo-5-chL;7-Bromopicolinic acid;Atogepant Impurity 25;3-Dibromo-5-chloropyridine;5-CHLORO-2,3-DIBROMOPYRIDINE;2,3 DIBROMO-5-CHLORO PYRIDINE;2,3-DIBROMO-5-DICHLOROPYRIDINE;Pyridine, 2,3-dibromo-5-chloro-;2,3-Dibromo-5-chloropyridine>2,3-Dibromo-5-chloropyridine 98%
CBNumber
CB4843265
Molecular Formula
C5H2Br2ClN
Formula Weight
271.34
MOL File
137628-17-2.mol
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2,3-Dibromo-5-chloropyridine Property

Melting point:
41.0 to 45.0 °C
Boiling point:
259.9±35.0 °C(Predicted)
Density 
2.136±0.06 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Room Temperature
solubility 
soluble in Methanol
form 
powder to crystal
pka
-3.85±0.20(Predicted)
color 
White to Light yellow to Light orange
InChI
InChI=1S/C5H2Br2ClN/c6-4-1-3(8)2-9-5(4)7/h1-2H
InChIKey
GDUFWKJMOOVEMX-UHFFFAOYSA-N
SMILES
C1(Br)=NC=C(Cl)C=C1Br
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Safety

Hazard Codes 
Xi,T
Risk Statements 
36/37/38-25
Safety Statements 
26-37-45
RIDADR 
UN 2811 6.1 / PGIII
HazardClass 
IRRITANT
HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H301Toxic if swalloed

Precautionary statements

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TCI Chemical
Product number
D4381
Product name
2,3-Dibromo-5-chloropyridine
Purity
>98.0%(GC)
Packaging
5g
Price
$35
Updated
2024/03/01
TCI Chemical
Product number
D4381
Product name
2,3-Dibromo-5-chloropyridine
Purity
>98.0%(GC)
Packaging
25g
Price
$152
Updated
2024/03/01
TRC
Product number
D425215
Product name
2,3-Dibromo-5-chloropyridine
Packaging
25g
Price
$275
Updated
2021/12/16
TRC
Product number
D425215
Product name
2,3-Dibromo-5-chloropyridine
Packaging
5G
Price
$220
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD75498
Product name
2,3-Dibromo-5-chloropyridine
Packaging
50g
Price
$632.5
Updated
2021/12/16
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2,3-Dibromo-5-chloropyridine Chemical Properties,Usage,Production

Uses

2,3-Dibromo-5-chloropyridine has been used as a reactant for regiospecific Grignard reactions with lactones.

Synthesis

3-Bromo-5-chloropyridone (8.0 g, 38.4 mmole) was dissolved in dimethylformamide (60 ml) at ambient temperature. Phosphorus (V) tribromide oxide (16.5 g, 57.6 mmoles) was added and the reaction heated to 80° C for 72 hours. After cooling, the reaction was poured onto 800 g of ice. Vacuum filtration provided the product as a dark solid (6.85 g). Hexane (225 ml) and decolorizing carbon was added to the crude product and the contents heated to reflux and then filtered through celite. The clear colorless filtrate was stripped under vacuum to yield 2,3-Dibromo-5-chloropyridine as a white solid (5.3 g, 51%).

2,3-Dibromo-5-chloropyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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2,3-Dibromo-5-chloropyridine Suppliers

Pure Chemistry Scientific Inc.
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View Lastest Price from 2,3-Dibromo-5-chloropyridine manufacturers

Henan Fengda Chemical Co., Ltd
Product
2,3-Dibromo-5-chloropyridine 137628-17-2
Price
US $8.00-0.80/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2024-01-22
Shaanxi Dideu Medichem Co. Ltd
Product
2,3-DibroMo-5-chloropyridine 137628-17-2
Price
US $1.00/Kg
Min. Order
1KG
Purity
98%
Supply Ability
20T
Release date
2019-12-26
Shaanxi Dideu Medichem Co. Ltd
Product
5-CHLORO-2,3-DIBROMOPYRIDINE 137638-17-2
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20T
Release date
2019-12-30

137628-17-2, 2,3-Dibromo-5-chloropyridineRelated Search:


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