Uses
ChemicalBook > CAS DataBase List >  4,4'-Diaminodicyclohexyl methane

4,4'-Diaminodicyclohexyl methane

Uses
Product Name
4,4'-Diaminodicyclohexyl methane
CAS No.
1761-71-3
Chemical Name
4,4'-Diaminodicyclohexyl methane
Synonyms
POLYLINK PACM;PACM20;DICYKAN;Wandamin hm;DIAMINODICYCLOHEXYLMETHANE;BIS(4-AMINOCYCLOHEXYL)METHANE;hlr4219;hlr4448;HLR 4219;HLR 4448
CBNumber
CB5109865
Molecular Formula
C13H26N2
Formula Weight
210.36
MOL File
1761-71-3.mol
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4,4'-Diaminodicyclohexyl methane Property

Melting point:
60-65°C
Boiling point:
330-331°C
Density 
0.95 g/mL at 25 °C(lit.)
vapor pressure 
<0.1 mm Hg ( 38 °C)
refractive index 
1.5032 (estimate)
Flash point:
>230 °F
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
solubility 
Chloroform (Slightly), Methanol (Slightly)
form 
powder to lump to clear liquid
pka
10.87±0.70(Predicted)
color 
White or Colorless to Almost white or Almost colorless
Odor
Ammonia odor
Water Solubility 
Insoluble (<0.1 g/100 mL)
BRN 
2079179
InChI
1S/C13H26N2/c14-12-5-1-10(2-6-12)9-11-3-7-13(15)8-4-11/h10-13H,1-9,14-15H2
InChIKey
DZIHTWJGPDVSGE-UHFFFAOYSA-N
SMILES
NC1CCC(CC1)CC2CCC(N)CC2
LogP
2.03 at 25℃
CAS DataBase Reference
1761-71-3(CAS DataBase Reference)
NIST Chemistry Reference
Cyclohexanamine, 4,4'-methylenebis-(1761-71-3)
EPA Substance Registry System
4,4'-Methylenebis(cyclohexylamine) (1761-71-3)
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Safety

Hazard Codes 
T+,N,C
Risk Statements 
26-34-51/53-48/22-43-35-22
Safety Statements 
26-28-36/37/39-45-61-50-14
RIDADR 
UN 2928 6.1/PG 2
WGK Germany 
2
RTECS 
GX1530000
10-34
TSCA 
TSCA listed
HazardClass 
8
PackingGroup 
III
HS Code 
29213000
Storage Class
8A - Combustible corrosive hazardous materials
Hazard Classifications
Acute Tox. 4 Oral
Aquatic Chronic 2
Skin Corr. 1B
Skin Sens. 1
STOT RE 2 Oral
Toxicity
LC50 inhalation in mouse: 400mg/m3/4H
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H302Harmful if swallowed

H314Causes severe skin burns and eye damage

H317May cause an allergic skin reaction

H373May cause damage to organs through prolonged or repeated exposure

H411Toxic to aquatic life with long lasting effects

Precautionary statements

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
368849
Product name
4,4′-Methylenebis(cyclohexylamine)
Purity
technical grade, 95%
Packaging
250g
Price
$132
Updated
2025/07/31
TCI Chemical
Product number
M0699
Product name
4,4'-Methylenebis(cyclohexylamine) (mixture of isomers)
Purity
>97.0%(GC)(T)
Packaging
25g
Price
$31
Updated
2025/07/31
TCI Chemical
Product number
M0699
Product name
4,4'-Methylenebis(cyclohexylamine) (mixture of isomers)
Purity
>97.0%(GC)(T)
Packaging
500g
Price
$121
Updated
2025/07/31
TRC
Product number
M227340
Product name
4,4''-Methylenebis(cyclohexylamine)
Packaging
100g
Price
$155
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD46724
Product name
4,4'-Diaminodicyclohexyl methane
Packaging
500g
Price
$200
Updated
2021/12/16
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4,4'-Diaminodicyclohexyl methane Chemical Properties,Usage,Production

Uses

4,4'-Methylenebis(cyclohexylamine) is a potential high inhibitive and high temperature resistant shale inhibitor.

Description

4,4'-Diaminodicyclohexyl methane is a sodium salt of a cyclic anhydride that is used as a specific treatment for removing dodecanedioic acid from fatty acids. The reaction solution is stable at pH 4-5 and has a viscosity of less than 1000 cps. It has good stability in the presence of amines and can be used in chromatographic science, including chromatography and gas-liquid chromatography. The UV absorption maxima for the acid complex are 195 nm and 240 nm.

Chemical Properties

Beige solidified mass or fragments

Uses

4,4'-Diaminodicyclohexyl methane be used as organic intermediates and epoxy curing agents.

Uses

4,4'-Diaminodicyclohexylmethane is used as epoxy curing agents. It is a versatile intermediate to produce leather, rubber products, plastics, dyes, and photo sensitive polymers. It is used in manufacturing diisocyanates and polyamides. It is also used as lubricant additive as and corrosion inhibitor.

Synthesis Reference(s)

Journal of the American Chemical Society, 75, p. 1156, 1953 DOI: 10.1021/ja01101a044

General Description

Yellowish white liquid or brown solid paste.

Air & Water Reactions

Sensitive to decomposition in air and light . Insoluble in water.

Reactivity Profile

4,4'-Diaminodicyclohexyl methane neutralizes acids in weakly exothermic reactions to form salts plus water. May be incompatible with isocyanates, halogenated organics, peroxides, phenols (acidic), epoxides, anhydrides, and acid halides. May generate hydrogen, a flammable gas, in combination with strong reducing agents such as hydrides.

Health Hazard

ACUTE/CHRONIC HAZARDS: 4,4'-Diaminodicyclohexyl methane is corrosive.

Fire Hazard

4,4'-Diaminodicyclohexyl methane is probably combustible.

Flammability and Explosibility

Non flammable

Toxicology

On resorption, predominant clinical signs of intoxication were hyperexcitability, excessive salivation, and convulsions in animals; repeated oral dosing (50 – 100 mg kg -1 d -1 in rats and mice for 10 and 16 d, respectively, 50 mg/kg in dogs for up to 82 weeks) resulted in gastrointestinal hemorrhagic inflammations, nephritis, and fatty changes to the liver. No changes in methemoglobin or in other hematological parameters were induced in cats on repeated doses of 50 and 100 mg kg -1 d -1, given twice per week over 2 months. Several in vitro and in vivo mutagenicity studies gave no evidence of a mutagenic or clastogenic potential.

Synthesis

1g of titanium dioxide powder was dispersed in 40mL of water and methanol mixture (water and methanol volume ratio of 9:1), stirred well, then added 60??mol/ml of RuCl3-xH2O dark brown aqueous solution, control the amount of addition so that the ruthenium in the titanium dioxide loading of 5wt%. After sealing and stirring for 3 hours at room temperature, 1M sodium hydroxide solution was added dropwise to pH10.5 and continued to seal and stir for 20 hours, centrifuged and washed with a mixture of water and ethanol for 3-5 times, and then vacuum-dried at 60??C overnight to obtain a light-green powder, and the catalyst was obtained.

The freshly prepared catalyst was placed in a reaction kettle, a certain volume of solvent was added, and an appropriate amount of 4,4'-diaminodiphenylmethane (MDA) was added, and the molar ratio of ruthenium in the MDA and the catalyst 4 was controlled to be 10,000, and the reaction kettle was closed and rinsed with hydrogen for 10 times, then the reaction kettle was heated up to 150 ?? to start the reaction, and the molar ratio of hydrogen and MDA was controlled to not be less than 80, and the hydrogen and MDA were controlled to be not less than 80. The molar ratio of hydrogen to MDA was controlled to be not less than 80, and the pressure of hydrogen was 1-5 MPa, and real-time samples were taken to check the reaction products and conversion rates.The benzene ring in MDA could be rapidly hydrogenated to produce a single benzene ring hydrogenation product (+6H) and a bis-benzene ring hydrogenation product, 4,4'-diaminodicyclohexylmethane (+12H) without deaminated products, which is worth mentioning that the 4,4'-diaminodicyclohexylmethane (+12H) is not deaminated. '-diaminodicyclohexylmethane is a feedstock compound for specialty nylons.

Toxics Screening Level

The initial threshold screening level (ITSL) for 4,4'-diaminodicyclohexylmethane is 6 μg/m3 based on an annual averaging time.

4,4'-Diaminodicyclohexyl methane Preparation Products And Raw materials

Raw materials

Preparation Products

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4,4'-Diaminodicyclohexyl methane Suppliers

Shanghai LanRun Chemical Co., Ltd.
Tel
021-69515658 ; 69515628 13701998368
Fax
021-69515998
Email
longrunchem@163.com
Country
China
ProdList
3786
Advantage
50
Hubei Xinjiecheng Chemical Technology Co., Ltd
Tel
13554075426
Email
1014723310@qq.com
Country
China
ProdList
3001
Advantage
58
Jingzhou Yinjie Chemical Co., Ltd
Tel
18008658728
Email
2718637152@qq.com
Country
China
ProdList
2820
Advantage
58
J & K SCIENTIFIC LTD.
Tel
18210857532; 18210857532
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
Advantage
76
Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
4006356688 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
ProdList
40228
Advantage
62
Alfa Aesar
Tel
400-6106006
Fax
021-67582001/03/05
Email
saleschina@alfa-asia.com
Country
China
ProdList
30123
Advantage
84
TCI (Shanghai) Development Co., Ltd.
Tel
021-67121386
Fax
021-67121385
Email
Sales-CN@TCIchemicals.com
Country
China
ProdList
24529
Advantage
81
Beijing HwrkChemical Technology Co., Ltd
Tel
010-89508211 18501085097
Fax
010-89508210
Email
sales.bj@hwrkchemical.com
Country
China
ProdList
9411
Advantage
55
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44802
Advantage
61
Capot Chemical Co., Ltd
Tel
+86 (0) 571 85 58 67 18
Fax
0086-571-85864795
Country
China
ProdList
18207
Advantage
66
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View Lastest Price from 4,4'-Diaminodicyclohexyl methane manufacturers

Hebei Chuanghai Biotechnology Co., Ltd
Product
4,4'-Diaminodicyclohexyl methane 1761-71-3
Price
US $25.00/ASSAYS
Min. Order
100ASSAYS
Purity
99.5%
Supply Ability
100 mt
Release date
2024-11-19
HebeiShuoshengImportandExportco.,Ltd
Product
4,4'-Diaminodicyclohexyl methane 1761-71-3
Price
US $6.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
2000KG/Month
Release date
2024-08-09
Hebei Chuanghai Biotechnology Co., Ltd
Product
Bis(4-aminocyclohexyl)methane 1761-71-3
Price
US $0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
500000kg
Release date
2024-10-31

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