5-IODO-2-METHYLANILINE

Product Name: 5-IODO-2-METHYLANILINE
CAS No.: 83863-33-6
Chemical Name: 5-IODO-2-METHYLANILINE
Synonyms: 5-iodo-o-toluidine;TIMTEC-BB SBB007547;5-IODO-2-METHYLANILI;2-AMINO-4-IODOTOLUENE;2-Methyl-5-iodoaniline;5-IODO-2-METHYLANILINE;5-Iodo-2-methyl-phenylamine;Benzenamine, 5-iodo-2-methyl-;2-Amino-4-iodotoluene~5-Iodo-o-toluidine;5-IODO-2-METHYLANILINE ISO 9001：2015 REACH
CBNumber: CB5169595
Molecular Formula: C7H8IN
Formula Weight: 233.05
MOL File: 83863-33-6.mol

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5-IODO-2-METHYLANILINE Property

Melting point:: 48-52 °C (lit.)
Boiling point:: 273 °C/760 mmHg (lit.)
Density: 1.7004 (estimate)
Flash point:: 110 °C
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
solubility: soluble in Methanol
form: powder to crystal
pka: 3.49±0.10(Predicted)
color: Light yellow to Brown to Dark green
Sensitive: Light Sensitive
BRN: 2078769
CAS DataBase Reference: 83863-33-6(CAS DataBase Reference)

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Safety

Hazard Codes: T
Risk Statements: 25-37/38-41-43
Safety Statements: 26-36/37-45
RIDADR: UN 2811 6.1/PG 3
WGK Germany: 3
Hazard Note: Toxic
HazardClass: 6.1
PackingGroup: III
HS Code: 2921420090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H301Toxic if swalloed

H315Causes skin irritation

H317May cause an allergic skin reaction

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 648647
Product name: 5-Iodo-2-methylaniline
Purity: 97%
Packaging: 1g
Price: $67
Updated: 2023/06/20

Sigma-Aldrich

Product number: 648647
Product name: 5-Iodo-2-methylaniline
Purity: 97%
Packaging: 5g
Price: $255
Updated: 2023/06/20

TCI Chemical

Product number: I1021
Product name: 5-Iodo-2-methylaniline
Purity: >98.0%(GC)(T)
Packaging: 5g
Price: $97
Updated: 2025/07/31

TCI Chemical

Product number: I1021
Product name: 5-Iodo-2-methylaniline
Purity: >98.0%(GC)(T)
Packaging: 25g
Price: $344
Updated: 2025/07/31

TRC

Product number: I737298
Product name: 5-Iodo-2-methylaniline
Packaging: 250mg
Price: $45
Updated: 2021/12/16

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5-IODO-2-METHYLANILINE Chemical Properties,Usage,Production

Synthesis

41252-97-5

83863-33-6

The general procedure for the synthesis of 5-iodo-2-methylaniline from 4-iodo-2-nitrotoluene was as follows: to a 300 mL ethanol solution of 4-iodo-1-methyl-2-nitrobenzene (25.0 g, 107 mmol) was added platinum sulfide (3.00 g) and ammonium formate (20.3 g, 321 mmol). The reaction mixture was heated to reflux and maintained for 12 hours. Upon completion of the reaction, the mixture was cooled to 22 °C and filtered through a Celite pad to remove solid impurities. The filtrate was concentrated under reduced pressure to give the crude product. The crude product was diluted with 300 mL of water and subsequently extracted with dichloromethane (3 x 200 mL). The organic phases were combined, washed with saturated brine and dried over anhydrous sodium sulfate. Finally, the organic phase was concentrated under reduced pressure to afford the target product 5-iodo-2-methylaniline (21.1 g, 95% yield). Mass spectrometry analysis showed MS m/z = 234 (M + H).

References

[1] Patent: WO2006/41773, 2006, A2. Location in patent: Page/Page column 302-303
[2] Patent: WO2010/127855, 2010, A1. Location in patent: Page/Page column 121; 122
[3] Justus Liebigs Annalen der Chemie, 1871, vol. 158, p. 337

5-IODO-2-METHYLANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-IODO-2-METHYLANILINE Suppliers

Americas 1 Australia 2 Belgium 2 Canada 3 China 137 Europe 3 France 1 Germany 7 India 11 Japan 3 Poland 1 Slovakia 1 Switzerland 3 The Netherlands 1 Ukraine 1 United Kingdom 19 United States 46 Global 242

Meryer (Shanghai) Chemical Technology Co., Ltd.

Tel: 4006356688 18621169109
Fax: 86-21-61259102
Email: market03@meryer.com
Country: China
ProdList: 40228
Advantage: 62

Alfa Aesar

Tel: 400-6106006
Fax: 021-67582001/03/05
Email: saleschina@alfa-asia.com
Country: China
ProdList: 30123
Advantage: 84

Ark Pharm, Inc.

Tel: 847-367-3680
Fax: 847-367-3681
Email: sales@arkpharminc.com
Country: United States
ProdList: 1670
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Energy Chemical

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Fax: 021-58436166
Email: sales8178@energy-chemical.com
Country: China
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Advantage: 61

Beijing Ouhe Technology Co., Ltd

Tel: 010-010-82967028 13522913783
Fax: +86-10-82967029
Email: 2355560935@qq.com
Country: China
ProdList: 12000
Advantage: 60

JinYan Chemicals(ShangHai) Co.,Ltd.

Tel: 13817811078
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Jia Xing Isenchem Co.,Ltd

Tel: 0573-85285100 18627885956
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Country: China
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Pure Chemistry Scientific Inc.

Tel: 001-857-928-2050 or 1-888-588-9418
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Country: United States
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Adamas Reagent, Ltd.

Tel: 400-6009262 16621234537
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Email: chenyj@titansci.com
Country: China
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Accela ChemBio Co.,Ltd.

Tel: 021-50795510 4000665055
Fax: 021-50795055
Email: sales@accelachem.com
Country: China
ProdList: 11035
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View Lastest Price from 5-IODO-2-METHYLANILINE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 5-IODO-2-METHYLANILINE 83863-33-6
Price: US $1.00-4.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200000KG
Release date: 2025-09-05

Henan Aochuang Chemical Co.,Ltd.

Product: 5-IODO-2-METHYLANILINE 83863-33-6
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-10-13

Shaanxi Dideu New Materials Co. Ltd

Product: 5-Iodo-2-methylaniline 83863-33-6
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98.0%
Supply Ability: 10000KGS
Release date: 2024-11-09

83863-33-6, 5-IODO-2-METHYLANILINERelated Search:

5-IODO-2-METHYLANILINE 4-Iodo-2-nitrotoluene 3-IODO-4-METHYLANILINE 2-IODO-4-METHYLANILINE 4-IODO-3-METHYLANILINE 98%,4-IODO-3-METHYLANILINE 4-IODO-2-METHYLANILINE,4-IODO-2-METHYLANILINE, 98+% 7-IODO-1H-QUINAZOLIN-4-ONE 2,4-DIMETHYL-1-IODO-5-NITROBENZENE 6-IODO-2,3-DIHYDRO-1H-INDOLE HYDROCHLORIDE 2,6-DINITRO-4-IODOBENZOIC ACID 6-IODO-4-TRIFLUOROMETHYL-ISATIN 4-IODO-2-NITROBENZYL ALCOHOL 2-BROMO-4-IODO-6-NITROTOLUENE 4-IODO-2,6-DINITROTOLUENE BUTTPARK 148\07-02 2-BROMO-6-IODO-4-METHYLANILINE 4-IODO-N-METHYLANILINE 6-CHLORO-4-IODO-3-METHYLANILINE

Benzenamine, 5-iodo-2-methyl-

TIMTEC-BB SBB007547

5-IODO-2-METHYLANILINE

2-AMINO-4-IODOTOLUENE

2-Methyl-5-iodoaniline

2-Amino-4-iodotoluene~5-Iodo-o-toluidine

5-iodo-o-toluidine

5-Iodo-2-methyl-phenylamine

5-IODO-2-METHYLANILI

5-IODO-2-METHYLANILINE ISO 9001：2015 REACH

83863-33-6

13192-68-8

IC6H3CH3NH2

C7

Amines

Building Blocks

Nitrogen Compounds

Organic Building Blocks

Building Blocks

Chemical Synthesis

Nitrogen Compounds

Organic Building Blocks

Aromatic Hydrocarbons (substituted) & Derivatives

Anilines, Aromatic Amines and Nitro Compounds

Aniline

Amines

C7

Nitrogen Compounds