4-IODO-N-METHYLANILINE

Product Name: 4-IODO-N-METHYLANILINE
CAS No.: 60577-34-6
Chemical Name: 4-IODO-N-METHYLANILINE
Synonyms: 4-IODO-N-METHYLANILINE;p-Iodo-N-methylaniline;N-Methyl-4-iodoaniline;4-Methylaminophenyl iodide;4-Iodo-N-methyl-benzenamine;(4-IODO-PHENYL)-METHYL-AMINE;Benzenamine, 4-iodo-N-methyl-
CBNumber: CB1815027
Molecular Formula: C7H8IN
Formula Weight: 233.05
MOL File: 60577-34-6.mol

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4-IODO-N-METHYLANILINE Property

Melting point:: 28-29 °C(Solv: hexane (110-54-3))
Boiling point:: 261.1±23.0 °C(Predicted)
Density: 1.779±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
pka: 3.82±0.12(Predicted)
Appearance: Dark purple to black <28°C Solid,>29°C Liquid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: I715703
Product name: 4-Iodo-n-methylaniline
Packaging: 500mg
Price: $140
Updated: 2021/12/16

Matrix Scientific

Product number: 074702
Product name: 4-Iodo-N-methylaniline
Purity: 95+%
Packaging: 1g
Price: $462
Updated: 2021/12/16

AK Scientific

Product number: W7309
Product name: 4-iodo-N-methylaniline
Packaging: 5g
Price: $480
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0049746
Product name: (4-IODO-PHENYL)-METHYL-AMINE
Purity: 95.00%
Packaging: 100MG
Price: $592.05
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0049746
Product name: (4-IODO-PHENYL)-METHYL-AMINE
Purity: 95.00%
Packaging: 500MG
Price: $624.07
Updated: 2021/12/16

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4-IODO-N-METHYLANILINE Chemical Properties,Usage,Production

Uses

4-Iodo-n-methylaniline is useful in general efficient method for direct N-methylation of aromatic primary amines with methanol .

Synthesis

100-61-8

60577-34-6

General procedure: The iodination of aryl amines was carried out under solvent-free conditions. The procedure was as follows: DBDABCODCI (0.5 mmol) was mixed and ground with N-methylaniline (1 mmol) in a porcelain mortar at room temperature. The reaction process was monitored by thin layer chromatography (TLC). Upon completion of the reaction, ethyl acetate was added to the mixture and subsequently filtered. The organic layer was washed with 5% aqueous sodium thiosulfate and dried with anhydrous magnesium sulfate. The solvent was evaporated under reduced pressure and the resulting crude product was purified by column chromatography, the eluent being a solvent mixture of ethyl acetate and hexane. The structure of the purified product was confirmed by melting point determination and 1H NMR spectroscopy.

References

[1] Organic Letters, 2001, vol. 3, # 7, p. 991 - 992
[2] Journal of Organic Chemistry, 2018, vol. 83, # 15, p. 7606 - 7621
[3] Bulletin of the Chemical Society of Ethiopia, 2015, vol. 29, # 1, p. 157 - 162
[4] Bulletin of the Chemical Society of Japan, 1988, vol. 61, # 2, p. 600 - 602
[5] Bulletin of the Chemical Society of Japan, 2012, vol. 85, # 11, p. 1239 - 1243

4-IODO-N-METHYLANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-IODO-N-METHYLANILINE Suppliers

China 71 India 1 Switzerland 1 Ukraine 1 United States 7 Global 81

Adamas Reagent, Ltd.

Tel: 400-6009262 16621234537
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ShangHai AmK Pharmaceutical Technology Co., Ltd.

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Shanghai Tombiopharma Chemical Co. Ltd.

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View Lastest Price from 4-IODO-N-METHYLANILINE manufacturers

Career Henan Chemical Co

Product: METHYL HENEICOSANOATE 6064-90-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 200kgs
Release date: 2020-01-10

Career Henan Chemical Co

Product: 4-IODO-N-METHYLANILINE 60577-34-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 85.0-99.8%
Supply Ability: 200kgs
Release date: 2020-01-10

60577-34-6, 4-IODO-N-METHYLANILINERelated Search:

N-(4-IODOPHENYL)MALEAMIC ACID Acetrizoic acid sodium acetrizoate 5-IODOISATIN Diatrizoate sodium N-(4-Iodophenyl)acetamide Metrizamide 1-(4-IODOPHENYL)-2-THIOUREA 3-IODO-4-METHYLANILINE 2-IODO-4-METHYLANILINE 5-IODO-2-METHYLANILINE 4-IODO-2-METHYLANILINE,4-IODO-2-METHYLANILINE, 98+% 4-IODO-3-METHYLANILINE 98%,4-IODO-3-METHYLANILINE N-(4-IODOPHENYL)SUCCINIMIDE 1-(4-IODOPHENYL)-1H-PYRROLE-2,5-DIONE 1-(5-IODOINDOLIN-1-YL)ETHANONE 2-IODO-5-METHYLANILINE,3-IODO-5-METHYLANILINE 2-BROMO-6-IODO-4-METHYLANILINE

4-IODO-N-METHYLANILINE

4-Methylaminophenyl iodide

N-Methyl-4-iodoaniline

p-Iodo-N-methylaniline

(4-IODO-PHENYL)-METHYL-AMINE

Benzenamine, 4-iodo-N-methyl-

4-Iodo-N-methyl-benzenamine

60577-34-6