ChemicalBook > CAS DataBase List > 4-IODO-N-METHYLANILINE

4-IODO-N-METHYLANILINE

Product Name
4-IODO-N-METHYLANILINE
CAS No.
60577-34-6
Chemical Name
4-IODO-N-METHYLANILINE
Synonyms
4-IODO-N-METHYLANILINE;p-Iodo-N-methylaniline;N-Methyl-4-iodoaniline;4-Methylaminophenyl iodide;4-Iodo-N-methyl-benzenamine;(4-IODO-PHENYL)-METHYL-AMINE;Benzenamine, 4-iodo-N-methyl-
CBNumber
CB1815027
Molecular Formula
C7H8IN
Formula Weight
233.05
MOL File
60577-34-6.mol
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4-IODO-N-METHYLANILINE Property

Melting point:
28-29 °C(Solv: hexane (110-54-3))
Boiling point:
261.1±23.0 °C(Predicted)
Density 
1.779±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
pka
3.82±0.12(Predicted)
Appearance
Dark purple to black <28°C Solid,>29°C Liquid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
I715703
Product name
4-Iodo-n-methylaniline
Packaging
500mg
Price
$140
Updated
2021/12/16
Matrix Scientific
Product number
074702
Product name
4-Iodo-N-methylaniline
Purity
95+%
Packaging
1g
Price
$462
Updated
2021/12/16
AK Scientific
Product number
W7309
Product name
4-iodo-N-methylaniline
Packaging
5g
Price
$480
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0049746
Product name
(4-IODO-PHENYL)-METHYL-AMINE
Purity
95.00%
Packaging
100MG
Price
$592.05
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0049746
Product name
(4-IODO-PHENYL)-METHYL-AMINE
Purity
95.00%
Packaging
500MG
Price
$624.07
Updated
2021/12/16
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4-IODO-N-METHYLANILINE Chemical Properties,Usage,Production

Uses

4-Iodo-n-methylaniline is useful in general efficient method for direct N-methylation of aromatic primary amines with methanol .

Synthesis

100-61-8

60577-34-6

General procedure: The iodination of aryl amines was carried out under solvent-free conditions. The procedure was as follows: DBDABCODCI (0.5 mmol) was mixed and ground with N-methylaniline (1 mmol) in a porcelain mortar at room temperature. The reaction process was monitored by thin layer chromatography (TLC). Upon completion of the reaction, ethyl acetate was added to the mixture and subsequently filtered. The organic layer was washed with 5% aqueous sodium thiosulfate and dried with anhydrous magnesium sulfate. The solvent was evaporated under reduced pressure and the resulting crude product was purified by column chromatography, the eluent being a solvent mixture of ethyl acetate and hexane. The structure of the purified product was confirmed by melting point determination and 1H NMR spectroscopy.

References

[1] Organic Letters, 2001, vol. 3, # 7, p. 991 - 992
[2] Journal of Organic Chemistry, 2018, vol. 83, # 15, p. 7606 - 7621
[3] Bulletin of the Chemical Society of Ethiopia, 2015, vol. 29, # 1, p. 157 - 162
[4] Bulletin of the Chemical Society of Japan, 1988, vol. 61, # 2, p. 600 - 602
[5] Bulletin of the Chemical Society of Japan, 2012, vol. 85, # 11, p. 1239 - 1243

4-IODO-N-METHYLANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4-IODO-N-METHYLANILINE manufacturers

Career Henan Chemical Co
Product
METHYL HENEICOSANOATE 6064-90-0
Price
US $1.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
200kgs
Release date
2020-01-10
Career Henan Chemical Co
Product
4-IODO-N-METHYLANILINE 60577-34-6
Price
US $1.00/KG
Min. Order
1KG
Purity
85.0-99.8%
Supply Ability
200kgs
Release date
2020-01-10

60577-34-6, 4-IODO-N-METHYLANILINERelated Search:

N-(4-IODOPHENYL)MALEAMIC ACID Acetrizoic acid sodium acetrizoate 5-IODOISATIN Diatrizoate sodium N-(4-Iodophenyl)acetamide Metrizamide 1-(4-IODOPHENYL)-2-THIOUREA 3-IODO-4-METHYLANILINE 2-IODO-4-METHYLANILINE 5-IODO-2-METHYLANILINE 4-IODO-2-METHYLANILINE,4-IODO-2-METHYLANILINE, 98+% 4-IODO-3-METHYLANILINE 98%,4-IODO-3-METHYLANILINE N-(4-IODOPHENYL)SUCCINIMIDE 1-(4-IODOPHENYL)-1H-PYRROLE-2,5-DIONE 1-(5-IODOINDOLIN-1-YL)ETHANONE 2-IODO-5-METHYLANILINE,3-IODO-5-METHYLANILINE 2-BROMO-6-IODO-4-METHYLANILINE

  • 4-IODO-N-METHYLANILINE
  • 4-Methylaminophenyl iodide
  • N-Methyl-4-iodoaniline
  • p-Iodo-N-methylaniline
  • (4-IODO-PHENYL)-METHYL-AMINE
  • Benzenamine, 4-iodo-N-methyl-
  • 4-Iodo-N-methyl-benzenamine
  • 60577-34-6