2-IODO-4-METHYLANILINE

Product Name: 2-IODO-4-METHYLANILINE
CAS No.: 29289-13-2
Chemical Name: 2-IODO-4-METHYLANILINE
Synonyms: BUTTPARK 34\09-13;2-Iodo-4-Methylanline;4-Amino-3-iodotoluene;2-IODO-4-METHYLANILINE;2-Iodo-4-MethylphenylaMine;2-Iodo-4-methylbenzenamine;2-Iodo-4-methylaniline 97%;BenzenaMine, 2-iodo-4-Methyl-;4-Amino-2-iodotoluene~3-Iodo-p-toluidine;4-Amino-3-iodotoluene, 2-Iodo-p-toluidine
CBNumber: CB5236231
Molecular Formula: C7H8IN
Formula Weight: 233.05
MOL File: 29289-13-2.mol

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2-IODO-4-METHYLANILINE Property

Melting point:: 34-37°C
Boiling point:: 273°C (rough estimate)
Density: 1.7004 (estimate)
Flash point:: >110°C
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
pka: 2.97±0.10(Predicted)
form: crystalline powder
color: cream
InChIKey: AJTUKWIQLKKRHE-UHFFFAOYSA-N
CAS DataBase Reference: 29289-13-2(CAS DataBase Reference)

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Safety

Hazard Codes: T,Xi
Risk Statements: 36/37/38-41-37/38-25
Safety Statements: 26-37/39-36/37/39-27-45
RIDADR: 2811
WGK Germany: 3
HazardClass: IRRITANT
PackingGroup: Ⅲ
HS Code: 29214300

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H301Toxic if swalloed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 794376
Product name: 2-Iodo-4-methylaniline
Purity: 97%
Packaging: 1g
Price: $82.3
Updated: 2023/06/20

Sigma-Aldrich

Product number: 794376
Product name: 2-Iodo-4-methylaniline
Purity: 97%
Packaging: 5g
Price: $376
Updated: 2023/06/20

TRC

Product number: I709253
Product name: 2-Iodo-4-methylaniline
Packaging: 1g
Price: $75
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: JK275736
Product name: 2-Iodo-4-methylaniline
Purity: 97%
Packaging: 1g
Price: $60
Updated: 2021/12/16

Matrix Scientific

Product number: 044675
Product name: 2-Iodo-4-methylaniline
Purity: 95+%
Packaging: 25g
Price: $145
Updated: 2021/12/16

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2-IODO-4-METHYLANILINE Chemical Properties,Usage,Production

Chemical Properties

Milky white solid

Synthesis Reference(s)

Tetrahedron Letters, 30, p. 899, 1989 DOI: 10.1016/S0040-4039(00)95273-0

Synthesis

106-49-0

29289-13-2

Step 1: Preparation of 2-iodo-4-methylaniline To a solution of 4-methylaniline (53.5 g, 500 mmol) in dichloromethane (DCM, 200 mL) was added a solution of sodium bicarbonate (NaHCO3, 50.4 g) in water (500 mL) at room temperature, followed by iodine (I2, 127 g). The reaction mixture was stirred at room temperature overnight. After completion of the reaction, the mixture was treated with aqueous sodium bisulfite (NaHSO3) and extracted with dichloromethane (DCM). The organic layers were combined, washed with brine, dried over anhydrous sodium sulfate (Na2SO4) and concentrated under reduced pressure to give the brown oily product 2-iodo-4-methylaniline (110 g, 95% yield). The product was characterized by 1H NMR (300 MHz, CDCl3): δ 7.48 (dd, J = 1.8 and 0.6 Hz, 1H), 6.96 (dd, J = 8.1 and 1.8 Hz, 1H), 6.67 (d, J = 8.1 Hz, 1H), 3.98 (broad peak, 2H), 2.22 (s, 3H) ppm.

References

[1] Journal of Organic Chemistry, 1996, vol. 61, # 17, p. 5804 - 5812
[2] Advanced Synthesis and Catalysis, 2017, vol. 359, # 15, p. 2640 - 2652
[3] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1999, vol. 38, # 8, p. 897 - 904
[4] Bioorganic and Medicinal Chemistry Letters, 1999, vol. 9, # 19, p. 2805 - 2810
[5] Journal of Heterocyclic Chemistry, 2013, vol. 50, # 5, p. 1031 - 1038

2-IODO-4-METHYLANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-IODO-4-METHYLANILINE Suppliers

China 112 Germany 3 India 6 Spain 1 United Kingdom 10 United States 15 Global 147

J & K SCIENTIFIC LTD.

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View Lastest Price from 2-IODO-4-METHYLANILINE manufacturers

Zhuozhou Wenxi import and Export Co., Ltd

Product: 2-IODO-4-METHYLANILINE 29289-13-2
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-10

Zhuozhou Wenxi import and Export Co., Ltd

Product: 2-IODO-4-METHYLANILINE 29289-13-2
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-09

Career Henan Chemical Co

Product: 2-IODO-4-METHYLANILINE 29289-13-2
Price: US $1.00/KG
Min. Order: 1KG
Purity: 95%
Supply Ability: 500KG
Release date: 2018-08-19

29289-13-2, 2-IODO-4-METHYLANILINERelated Search:

4-AMINO-3-IODOBENZOIC ACID Methyl 4-amino-3-iodobenzoate 4-Amino-3,5-diiodobenzoic acid 4-IODO-2-METHYLANILINE, 98+%,4-IODO-2-METHYLANILINE 4-IODO-3-METHYLANILINE,4-IODO-3-METHYLANILINE 98% 5-IODO-2-METHYLANILINE 3-IODO-4-METHYLANILINE 3-Iodotoluene ALPHA-BROMO-3-IODO-4-NITROTOLUENE 4-AMINO-3,5-DIIODOBENZOIC ACID METHYL ESTER S-[2-(IODO-4-AZIDOSALICYLAMIDO)ETHYLTHIO]-2-THIOPYRIDINE ETHYL 4-AMINO-3,5-DIIODOBENZOATE BOC-PHE(3,5-DII,4-NH2)-OH 2-BROMO-6-IODO-4-METHYLANILINE 3-IODO-4-NITROTOLUENE 2-iodo-3-methylaniline 4-IODO-N-METHYLANILINE 2-iodo-N-methylaniline

2-IODO-4-METHYLANILINE

BUTTPARK 34\09-13

4-Amino-2-iodotoluene~3-Iodo-p-toluidine

4-Amino-3-iodotoluene

2-Iodo-4-methylbenzenamine

2-Iodo-4-Methylanline

2-Iodo-4-MethylphenylaMine

4-Amino-3-iodotoluene, 2-Iodo-p-toluidine

BenzenaMine, 2-iodo-4-Methyl-

2-Iodo-4-methylaniline 97%

2-IODO-4-METHYLANILINE ISO 9001：2015 REACH

29289-13-2

Anilines, Amides & Amines

Iodine Compounds

Anilines, Aromatic Amines and Nitro Compounds