ChemicalBook > CAS DataBase List > 2-IODO-4-METHYLANILINE

2-IODO-4-METHYLANILINE

Product Name
2-IODO-4-METHYLANILINE
CAS No.
29289-13-2
Chemical Name
2-IODO-4-METHYLANILINE
Synonyms
BUTTPARK 34\09-13;2-Iodo-4-Methylanline;4-Amino-3-iodotoluene;2-IODO-4-METHYLANILINE;2-Iodo-4-MethylphenylaMine;2-Iodo-4-methylbenzenamine;2-Iodo-4-methylaniline 97%;BenzenaMine, 2-iodo-4-Methyl-;4-Amino-2-iodotoluene~3-Iodo-p-toluidine;4-Amino-3-iodotoluene, 2-Iodo-p-toluidine
CBNumber
CB5236231
Molecular Formula
C7H8IN
Formula Weight
233.05
MOL File
29289-13-2.mol
More
Less

2-IODO-4-METHYLANILINE Property

Melting point:
34-37°C
Boiling point:
273°C (rough estimate)
Density 
1.7004 (estimate)
Flash point:
>110°C
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
pka
2.97±0.10(Predicted)
form 
crystalline powder
color 
cream
InChIKey
AJTUKWIQLKKRHE-UHFFFAOYSA-N
CAS DataBase Reference
29289-13-2(CAS DataBase Reference)
More
Less

Safety

Hazard Codes 
T,Xi
Risk Statements 
36/37/38-41-37/38-25
Safety Statements 
26-37/39-36/37/39-27-45
RIDADR 
2811
WGK Germany 
3
HazardClass 
IRRITANT
PackingGroup 
Ⅲ
HS Code 
29214300
More
Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H301Toxic if swalloed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More
Less

N-Bromosuccinimide Price

Sigma-Aldrich
Product number
794376
Product name
2-Iodo-4-methylaniline
Purity
97%
Packaging
1g
Price
$82.3
Updated
2023/06/20
Sigma-Aldrich
Product number
794376
Product name
2-Iodo-4-methylaniline
Purity
97%
Packaging
5g
Price
$376
Updated
2023/06/20
TRC
Product number
I709253
Product name
2-Iodo-4-methylaniline
Packaging
1g
Price
$75
Updated
2021/12/16
Frontier Specialty Chemicals
Product number
JK275736
Product name
2-Iodo-4-methylaniline
Purity
97%
Packaging
1g
Price
$60
Updated
2021/12/16
Matrix Scientific
Product number
044675
Product name
2-Iodo-4-methylaniline
Purity
95+%
Packaging
25g
Price
$145
Updated
2021/12/16
More
Less

2-IODO-4-METHYLANILINE Chemical Properties,Usage,Production

Chemical Properties

Milky white solid

Synthesis Reference(s)

Tetrahedron Letters, 30, p. 899, 1989 DOI: 10.1016/S0040-4039(00)95273-0

Synthesis

106-49-0

29289-13-2

Step 1: Preparation of 2-iodo-4-methylaniline To a solution of 4-methylaniline (53.5 g, 500 mmol) in dichloromethane (DCM, 200 mL) was added a solution of sodium bicarbonate (NaHCO3, 50.4 g) in water (500 mL) at room temperature, followed by iodine (I2, 127 g). The reaction mixture was stirred at room temperature overnight. After completion of the reaction, the mixture was treated with aqueous sodium bisulfite (NaHSO3) and extracted with dichloromethane (DCM). The organic layers were combined, washed with brine, dried over anhydrous sodium sulfate (Na2SO4) and concentrated under reduced pressure to give the brown oily product 2-iodo-4-methylaniline (110 g, 95% yield). The product was characterized by 1H NMR (300 MHz, CDCl3): δ 7.48 (dd, J = 1.8 and 0.6 Hz, 1H), 6.96 (dd, J = 8.1 and 1.8 Hz, 1H), 6.67 (d, J = 8.1 Hz, 1H), 3.98 (broad peak, 2H), 2.22 (s, 3H) ppm.

References

[1] Journal of Organic Chemistry, 1996, vol. 61, # 17, p. 5804 - 5812
[2] Advanced Synthesis and Catalysis, 2017, vol. 359, # 15, p. 2640 - 2652
[3] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1999, vol. 38, # 8, p. 897 - 904
[4] Bioorganic and Medicinal Chemistry Letters, 1999, vol. 9, # 19, p. 2805 - 2810
[5] Journal of Heterocyclic Chemistry, 2013, vol. 50, # 5, p. 1031 - 1038

2-IODO-4-METHYLANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

More
Less

2-IODO-4-METHYLANILINE Suppliers

China 112 Germany 3 India 6 Spain 1 United Kingdom 10 United States 15 Global 147
J & K SCIENTIFIC LTD.
Tel
18210857532; 18210857532
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
Advantage
76
Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
4006356688 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
ProdList
40228
Advantage
62
ZHIWE CHEMTECH CO LTD
Tel
021-20221225 13917446399
Fax
QQ:115820162
Email
zwchem@163.com
Country
China
ProdList
616
Advantage
61
ShangHai DEMO Chemical Co.,Ltd
Tel
400-021-7337 2355568890
Fax
0086-21-50182339
Email
sales@demochem.com
Country
China
ProdList
2572
Advantage
57
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44801
Advantage
61
Wuhan Chemwish Technology Co., Ltd
Tel
86-027-67849912
Fax
86-027-87531808
Email
sales@chemwish.com
Country
China
ProdList
35896
Advantage
56
Capot Chemical Co., Ltd
Tel
+86 (0) 571 85 58 67 18
Fax
0086-571-85864795
Country
China
ProdList
18207
Advantage
66
JinYan Chemicals(ShangHai) Co.,Ltd.
Tel
13817811078
Fax
86-021-50426522,50426273
Email
sales@jingyan-chemical.com
Country
China
ProdList
9976
Advantage
60
Jia Xing Isenchem Co.,Ltd
Tel
0573-85285100 18627885956
Fax
0573-85285100
Email
isenchem@163.com
Country
China
ProdList
9310
Advantage
66
Accela ChemBio Co.,Ltd.
Tel
021-50795510 4000665055
Fax
021-50795055
Email
sales@accelachem.com
Country
China
ProdList
11035
Advantage
64
Shanghai Longsheng chemical Co.,Ltd.
Tel
021-58099652-8005 13585536065
Fax
021-58099609
Email
bin.wu@shlschem.com
Country
China
ProdList
9883
Advantage
59
Shanghai Hanhong Scientific Co.,Ltd.
Tel
021-54306202 13764082696
Email
info@hanhongsci.com
Country
China
ProdList
42934
Advantage
64
Beijing Eternalchem Co,. Ltd.
Tel
010-59484199 18611897322
Email
sales@eternalchem.com
Country
China
ProdList
4383
Advantage
60
Wuhan Arike Technology Co., Ltd.
Tel
027- 51832457 94518350
Fax
E-Mail Inquiry
Country
China
ProdList
746
Advantage
62
Shanghai Sphchem Co., Ltd.
Tel
021-56491756 13512199871
Fax
021-5649-1756
Email
2819742715@qq.com
Country
China
ProdList
4000
Advantage
55
Nanjing Norris-Pharm Technology Co., Ltd
Tel
18652989687
Fax
+86-25-52131256
Email
sales@norris-pharm.com
Country
China
ProdList
8878
Advantage
55
9ding chemical ( Shanghai) Limited
Tel
4009209199
Fax
86-021-52271987
Email
sales@9dingchem.com
Country
China
ProdList
18209
Advantage
56
Nanjing ShengSai Chemical Co., Ltd.
Tel
025-85205967 13951876367
Fax
025-85205967
Email
shengsaichem@163.com
Country
China
ProdList
818
Advantage
58
Bide Pharmatech Ltd.
Tel
400-164-7117 13681763483
Fax
+86-21-61629029
Email
product02@bidepharm.com
Country
China
ProdList
39966
Advantage
60
Suzhou yacoo science co.,Ltd
Tel
0512-87182056 18013166090
Fax
0512-87182056
Email
lingling.qi@yacoo.com.cn
Country
China
ProdList
6295
Advantage
60
Shanghai ACT chemical Limited
Tel
021-59904146 18001826933
Fax
+86-21-59904146
Email
sales@actchemical.com
Country
China
ProdList
476
Advantage
56
Mashilabs (Shanghai) Co.,Ltd.
Tel
19916721580
Fax
QQ：3154870176
Email
mafarm@126.com
Country
China
ProdList
4542
Advantage
58
Tianjin Anhao Biological Technology Co., Ltd.
Tel
Email
sales@ahpharmatech.com
Country
China
ProdList
5734
Advantage
55
Nanjing Duolong Bio-tech Co.,Ltd.
Tel
18905173768
Fax
025-83263139
Email
52513593@qq.com
Country
China
ProdList
2331
Advantage
50
Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.
Tel
025-66028182 18626450290
Email
yftan@aikonchem.com
Country
China
ProdList
16679
Advantage
50
Sigma-Aldrich
Tel
021-61415566 800-8193336
Email
orderCN@merckgroup.com
Country
China
ProdList
51395
Advantage
80
Changzhou Anxuan Chemical, Co., Ltd.
Tel
13912302692 13912302692;
Fax
0519-88064678
Email
sales@anxuanchem.com
Country
China
ProdList
4828
Advantage
58
Nanjing Endesa Bio-tech Co., Ltd.
Tel
025-58862853 18915922038
Fax
+86-025-58862853
Email
sales@endesachem.com
Country
China
ProdList
591
Advantage
58
Zhengzhou Alfachem Co., Ltd.
Tel
0371-53765687 18937137882
Fax
QQ:2885373884
Email
2853979813@qq.com
Country
China
ProdList
7991
Advantage
55
Shangdong Youbang Biochemical Technology Co.,LTD.
Tel
15098208899
Fax
0530-7159266
Email
3368029756@qq.com
Country
China
ProdList
292
Advantage
58
Hubei Chuangliankangcheng Pharmaceutical Co., Ltd.
Tel
027-65388397 18164111589
Fax
027-65388397
Email
3321478047@qq.com
Country
China
ProdList
2007
Advantage
55
Henan CoreyChem Co., Ltd
Tel
0371-86658258
Fax
0371-60996044
Email
info@coreychem.com
Country
China
ProdList
10453
Advantage
58
Shanghai YuanYe Biotechnology Co., Ltd.
Tel
021-61312847; 18021002903
Fax
QQ:3008007432
Email
3008007409@qq.com
Country
China
ProdList
71826
Advantage
60
parabiochem
Tel
025-83453382-8005
Fax
025-83453382
Email
sale@parabiochem.com
Country
China
ProdList
9595
Advantage
55
Chengdu Xiaojia Technology Co., Ltd.
Tel
15902830537
Email
zhanghao@happysyn.com
Country
China
ProdList
3180
Advantage
55
Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
Email
sales@amadischem.com
Country
China
ProdList
131957
Advantage
58
Dalian lichuang Chemical Co., Ltd
Tel
0411-0411-00000000 13644282108
Fax
-
Email
3500508746@qq.com
Country
China
ProdList
2896
Advantage
55
Hangzhou Molcore Biopharmatech Co.,Ltd
Tel
400-711-5280 86-571-81025280
Fax
86-571-85806285
Email
sales@molcore.com
Country
China
ProdList
9967
Advantage
58
Capot Chemical Co.,Ltd.
Tel
+86-（0）57185586718; +8613336195806
Fax
+86-571-85864795
Email
sales@capot.com
Country
China
ProdList
29735
Advantage
60
Shanghai QiQiao Biological Technology Co., Ltd.
Tel
021-37653318; 15221675714
Email
515366396@qq.com
Country
China
ProdList
2089
Advantage
58
Rhawn Reagent
Tel
400-400-1332688 18019345275
Fax
400-133-2688
Email
amy@rhawn.cn
Country
China
ProdList
14948
Advantage
58
Shanghai Haohong Pharmaceutical Co., Ltd.
Tel
400-8210725 400821072
Fax
021-58955996
Email
malulu@leyan.com
Country
China
ProdList
25000
Advantage
58
Tianjin heowns Biochemical Technology Co., Ltd.
Tel
400-6387771-6039 18920764717
Email
sales@heowns.com
Country
China
ProdList
23771
Advantage
60
3A Chemicals
Tel
400-668-9898
Fax
010-51582189
Email
service@3achem.com
Country
China
ProdList
20557
Advantage
58
Zhengzhou Acme Chemical Co., Ltd.
Tel
0371-037163312495,13303845143 13303845143
Fax
QQ3001379618
Email
3001379618@qq.com
Country
China
ProdList
10267
Advantage
58
Cool Pharm, Ltd
Tel
021-58581007 18019463053
Fax
021-50966098
Email
sales@coolpharm.com
Country
China
ProdList
12878
Advantage
58
Xinyi Kaiwu Chemical Technology Co., Ltd.
Tel
0516-0516-88997009 18651776937
Email
4164357@qq.com
Country
China
ProdList
3204
Advantage
58
Allfluoro pharmaceutical co. ltd.
Tel
+86-400-0216110 +86-15958047586
Fax
0086-21-33275002
Email
sales@allfluoro.com
Country
China
ProdList
11385
Advantage
58
Henan Alfa Chemical Co., Ltd
Tel
+8615838112936
Email
alfa10@alfachem.cn
Country
China
ProdList
12921
Advantage
58
Nanjing Hengbei Chemicals Co., Ltd.
Tel
+86-25-58393656
Fax
+86-25-58393656
Email
sales@hengbeichem.cn
Country
China
ProdList
6854
Advantage
58
More
Less

View Lastest Price from 2-IODO-4-METHYLANILINE manufacturers

Zhuozhou Wenxi import and Export Co., Ltd
Product
2-IODO-4-METHYLANILINE 29289-13-2
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-10
Zhuozhou Wenxi import and Export Co., Ltd
Product
2-IODO-4-METHYLANILINE 29289-13-2
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-09
Career Henan Chemical Co
Product
2-IODO-4-METHYLANILINE 29289-13-2
Price
US $1.00/KG
Min. Order
1KG
Purity
95%
Supply Ability
500KG
Release date
2018-08-19

29289-13-2, 2-IODO-4-METHYLANILINERelated Search:

4-AMINO-3-IODOBENZOIC ACID Methyl 4-amino-3-iodobenzoate 4-Amino-3,5-diiodobenzoic acid 4-IODO-2-METHYLANILINE, 98+%,4-IODO-2-METHYLANILINE 4-IODO-3-METHYLANILINE,4-IODO-3-METHYLANILINE 98% 5-IODO-2-METHYLANILINE 3-IODO-4-METHYLANILINE 3-Iodotoluene ALPHA-BROMO-3-IODO-4-NITROTOLUENE 4-AMINO-3,5-DIIODOBENZOIC ACID METHYL ESTER S-[2-(IODO-4-AZIDOSALICYLAMIDO)ETHYLTHIO]-2-THIOPYRIDINE ETHYL 4-AMINO-3,5-DIIODOBENZOATE BOC-PHE(3,5-DII,4-NH2)-OH 2-BROMO-6-IODO-4-METHYLANILINE 3-IODO-4-NITROTOLUENE 2-iodo-3-methylaniline 4-IODO-N-METHYLANILINE 2-iodo-N-methylaniline

  • 2-IODO-4-METHYLANILINE
  • BUTTPARK 34\09-13
  • 4-Amino-2-iodotoluene~3-Iodo-p-toluidine
  • 4-Amino-3-iodotoluene
  • 2-Iodo-4-methylbenzenamine
  • 2-Iodo-4-Methylanline
  • 2-Iodo-4-MethylphenylaMine
  • 4-Amino-3-iodotoluene, 2-Iodo-p-toluidine
  • BenzenaMine, 2-iodo-4-Methyl-
  • 2-Iodo-4-methylaniline 97%
  • 2-IODO-4-METHYLANILINE ISO 9001：2015 REACH
  • 29289-13-2
  • Anilines, Amides & Amines
  • Iodine Compounds
  • Anilines, Aromatic Amines and Nitro Compounds