ChemicalBook > CAS DataBase List > 10-Bromodecanoic acid

10-Bromodecanoic acid

Product Name: 10-Bromodecanoic acid
CAS No.: 50530-12-6
Chemical Name: 10-Bromodecanoic acid
Synonyms: Bromocapricacid;10-Bromodecanoic;W-BROMODECANOIC ACID;1-Bromodecanoic acid;10-BROMO-DECYLIC ACID;10-BROMODECANOIC ACID;OMEGA-BROMOCAPRIC ACID;OMEGA-BROMODECANOIC ACID;Decanoic acid, 10-bromo-;10-Bromodecanoic acid 98%
CBNumber: CB5189571
Molecular Formula: C10H19BrO2
Formula Weight: 251.16
MOL File: 50530-12-6.mol

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10-Bromodecanoic acid Property

Melting point:: 38-41 °C (lit.)
Boiling point:: 160 °C(Press: 1 Torr)
Density: 1.3099 (rough estimate)
refractive index: 1.5845 (estimate)
Flash point:: >231 °F
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
form: powder to crystal
pka: 4.78±0.10(Predicted)
color: White to Light yellow to Light orange
Water Solubility: Partly miscible in water.
CAS DataBase Reference: 50530-12-6(CAS DataBase Reference)
NIST Chemistry Reference: 10-Bromodecanoic acid(50530-12-6)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-37
WGK Germany: 3
HazardClass: IRRITANT
HS Code: 29159000

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 541397
Product name: 10-Bromodecanoic acid
Purity: 95%
Packaging: 5g
Price: $26.5
Updated: 2025/07/31

Sigma-Aldrich

Product number: 541397
Product name: 10-Bromodecanoic acid
Purity: 95%
Packaging: 25g
Price: $54.05
Updated: 2025/07/31

TCI Chemical

Product number: B2264
Product name: 10-Bromodecanoic Acid
Purity: >97.0%(GC)
Packaging: 5g
Price: $41
Updated: 2025/07/31

TCI Chemical

Product number: B2264
Product name: 10-Bromodecanoic Acid
Purity: >97.0%(GC)
Packaging: 25g
Price: $129
Updated: 2025/07/31

TRC

Product number: B685323
Product name: 10-Bromodecanoic Acid
Packaging: 5g
Price: $55
Updated: 2021/12/16

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10-Bromodecanoic acid Chemical Properties,Usage,Production

Chemical Properties

Flaky crystals. Melting point 42°C, boiling point 163-165°C (0.27 kPa).

Uses

10-Bromodecanoic acid may be employed as an alkylcarboxylate chain source in the preparation of alkylcarboxylate-grafted polyethylenimine. It may also be used in the synthesis of :

10-(methylsulfinyl)decanoic acid
10-cyanodecanoic acid
(10-oxo-10-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)-decyl)triphenylphosphonium bromide
11-thiastearic acid

General Description

10-Bromodecanoic acid can be prepared from 10-bromodecanol via oxidation.

reaction suitability

reagent type: linker

Synthesis

53463-68-6

50530-12-6

The general procedure for the synthesis of 10-bromodecanoic acid from 10-bromo-1-decanol is as follows: 1. 48% hydrobromic acid (22.6 mL, 0.2 mol, 1 eq.) was slowly added dropwise to a toluene solution (400 mL) of 1,10-decanediol (34.8 g, 0.2 mol, 1 eq.) with stirring and refluxed for 24 hr. at 180° C. using a Dean-Stark manifold. 2. After completion of the reaction, the mixture was cooled to room temperature and washed sequentially with 6N NaOH (150 mL), 10% HCl (150 mL), water (2 x 250 mL) and brine (200 mL). 3. The organic layer was dried over anhydrous sodium sulfate and concentrated, separated by silica gel column chromatography using cyclohexane/ethyl acetate (4:1) as eluent to afford 43.5 g (92%) of 10-bromo-1-decanol as a colorless liquid. 4. To an acetone solution (130 mL) of 10-bromo-1-decanol (41 g, 0.17 mol, 1 eq.) was slowly added a chromic acid solution prepared from chromium trioxide (25.7 g, 0.26 mol, 1.5 eq.), water (25 mL), and concentrated sulfuric acid (22.5 mL, 0.34 mol, 2 eq.) at -5°C. 5. The reaction mixture was stirred at 0°C for 2 hours and then left at room temperature overnight. 6. After completion of the reaction, the mixture was extracted with ether (3 x 250 mL), washed sequentially with water (250 mL) and brine (250 mL), dried over anhydrous sodium sulfate and concentrated. 7. The residue was separated by silica gel column chromatography using dichloromethane as eluent and recrystallized from petroleum ether to give 31.0 g (73%) of 10-bromodecanoic acid as a white solid with a melting point of 36-37 °C. The residue was separated by 1H2O2 column chromatography using dichloromethane as eluent. 8. The structure of the product was confirmed by 1H NMR and 13C NMR: 1H NMR δ 11.23 (bs, 1H, -OH), 3.41 (t, J = 7.0 Hz, 2H, H-10), 2.36 (t, J = 7.6 Hz, 2H, H-2), 1.87 (m, 2H, H-9), 1.64 (m, 2H, H-3), 1.22- 1.44 (m, 10H, H-3), 1.22- 2H, H-3). 1.44 (m, 10H, H-4-8); 13C NMR δ 180.2 (C1), 34.1 (C2), 34.0 (C10), 32.9, 29.1, 28.9, 28.6, 28.4, 28.2, 24.7.

References

[1] Bioorganic and Medicinal Chemistry, 2011, vol. 19, # 1, p. 567 - 579
[2] Patent: DE867243, 1943,
[3] Journal of the American Chemical Society, 1956, vol. 78, p. 2255,2256
[4] Journal of Organic Chemistry, 1956, vol. 21, p. 883,885
[5] Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 2000, vol. 350, p. 93 - 101

10-Bromodecanoic acid Preparation Products And Raw materials

Raw materials

10-Hydroxydecanoic acid Hydrogen bromide Three-necked flask

Preparation Products

ETHYL 10(METHYLSULFONYL)DECANOATE

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View Lastest Price from 10-Bromodecanoic acid manufacturers

Hebei Chuanghai Biotechnology Co,.LTD

Product: 10-Bromodecanoic Acid 50530-12-6
Price: US $1.70/kg
Min. Order: 10kg
Purity: 99%
Supply Ability: 10000kg
Release date: 2024-08-22

Henan Fengda Chemical Co., Ltd

Product: 10-Bromodecanoic acid 50530-12-6
Price: US $30.00-1.00/KG
Min. Order: 1KG
Purity: 99%，95%
Supply Ability: g-kg-tons, free sample is available
Release date: 2024-01-03

Zhuozhou Wenxi import and Export Co., Ltd

Product: 10-Bromodecanoic acid 50530-12-6
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-06-27

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50530-12-6

BrCH29CO2H

Organic Building Blocks

Carbonyl Compounds

Carboxylic Acids

C10

Building Blocks

Organic acids

omega-Bromocarboxylic Acids

omega-Functional Alkanols, Carboxylic Acids, Amines & Halides

C10

Carbonyl Compounds

Carboxylic Acids