ChemicalBook > CAS DataBase List > Cyclofenil

Cyclofenil

Product Name
Cyclofenil
CAS No.
2624-43-3
Chemical Name
Cyclofenil
Synonyms
f6066;h3452;oginex;ondonid;sexovar;ici48213;fertodur;ondogyne;sexadieno;cyclofenyl
CBNumber
CB5212631
Molecular Formula
C23H24O4
Formula Weight
364.44
MOL File
2624-43-3.mol
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Cyclofenil Property

Melting point:
135-136°
Boiling point:
415.62°C (rough estimate)
Density 
1.0986 (rough estimate)
refractive index 
1.4433 (estimate)
storage temp. 
2-8°C
solubility 
DMSO: 10 mg/mL at 60 °C, soluble
form 
solid
color 
White to Off-White
CAS DataBase Reference
2624-43-3(CAS DataBase Reference)
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Safety

WGK Germany 
2
RTECS 
GO7550000
Toxicity
LD50 oral in rat: > 12gm/kg
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

Cayman Chemical
Product number
18676
Product name
Cyclofenil
Purity
≥98%
Packaging
5mg
Price
$32
Updated
2024/03/01
Cayman Chemical
Product number
18676
Product name
Cyclofenil
Purity
≥98%
Packaging
10mg
Price
$61
Updated
2024/03/01
Cayman Chemical
Product number
18676
Product name
Cyclofenil
Purity
≥98%
Packaging
50mg
Price
$93
Updated
2024/03/01
TRC
Product number
C987835
Product name
Cyclofenil
Packaging
500mg
Price
$95
Updated
2021/12/16
TRC
Product number
C987835
Product name
Cyclofenil
Packaging
10g
Price
$575
Updated
2021/12/16
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Cyclofenil Chemical Properties,Usage,Production

Chemical Properties

White Solid

Originator

Ondogyne,Roussel,France,1970

Uses

Cyclofenil is a weak nonsteroidal estrogen with ovulation induction properties. Mammalian hormone.

Definition

ChEBI: Cyclofenil is an organic molecular entity.

Manufacturing Process

(A) Preparation of p-Hydroxy-p'-Methoxybenzhydrylidenecyclohexane: To a Grignard solution prepared from 110 g of magnesium (4.5 mols) and 840 g of p-bromoanisole (4.5 mols) in one liter of anhydrous ether, there was added dropwise with vigorous agitation 307 g of p-hydroxyphenyl cyclohexyl ketone (1.5 mols) dissolved in one liter of anhydrous ether. Upon completion of the addition the reaction mixture was refluxed for 2.5 hours with agitation, and was then cooled. Thereupon 15 mols of ammonium chloride dissolved in 3 liters of water were added. The ethereal layer was separated, washed with water, dried over anhydrous sodium sulfate and distilled. Yield: 370 g. BP 180° to 190°C at 0.1 mm. The substance was recrystallized from a mixture of carbon tetrachloride and petroleum ether. MP 145° to 146°C.
(B)Preparation of p,p'-Dihydroxybenzhydrylidenecyclohexane: A mixture of 118 g of p-hydroxy-p'-methoxybenzhydrylidenecyclohexane (0.4 mol), 120 g of potassium hydroxide pellets and 500 ml of triethylene glycol was stirred 4 hours at 220°C. When the reaction mixture was poured into water the substance crystallized, and the crystals were filtered off and washed with water. The substance was then recrystallized from a mixture of ethanol and petroleum ether. Yield: 104 g. MP 235° to 236°C.
(C) Preparation of p,p'-Diacetoxybenzhydrylidenecyclohexane: 56 g of p,p'- dihydroxybenzhydrylidenecyclohexane (0.2 mol) was mixed with 250 ml of acetic anhydride and 500 ml of pyridine. The mixture was refluxed for 2 hours and was then poured into water, the substance crystallizing out. The crystals were filtered off and washed with water. Finally the substance was recrystallized from ethanol. Yield: 62 g. MP 135° to 136°C.

Therapeutic Function

Ovulation stimulant

Cyclofenil Preparation Products And Raw materials

Raw materials

Preparation Products

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Cyclofenil Suppliers

EMMX Biotechnology LLC
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View Lastest Price from Cyclofenil manufacturers

Career Henan Chemical Co
Product
Cyclofenil 2624-43-3
Price
US $8.00/kg
Min. Order
1kg
Purity
98%
Supply Ability
100KG
Release date
2018-12-15

2624-43-3, CyclofenilRelated Search:


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