ChemicalBook > CAS DataBase List > 2,4-DICHLORO-7-BROMOQUINAZOLINE

2,4-DICHLORO-7-BROMOQUINAZOLINE

Product Name
2,4-DICHLORO-7-BROMOQUINAZOLINE
CAS No.
959237-68-4
Chemical Name
2,4-DICHLORO-7-BROMOQUINAZOLINE
Synonyms
7-Bromo-2,4-dichloroquinazoline;2,4-DICHLORO-7-BROMOQUINAZOLINE;Quinazoline, 7-bromo-2,4-dichloro-
CBNumber
CB52461006
Molecular Formula
C8H3BrCl2N2
Formula Weight
277.93
MOL File
959237-68-4.mol
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2,4-DICHLORO-7-BROMOQUINAZOLINE Property

Boiling point:
330.2±24.0 °C(Predicted)
Density 
1.851±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
-1.17±0.30(Predicted)
Appearance
White to yellow Solid
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Safety

HS Code 
2933599590
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H317May cause an allergic skin reaction

H373May cause damage to organs through prolonged or repeated exposure

Precautionary statements

P201Obtain special instructions before use.

P202Do not handle until all safety precautions have been read and understood.

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P272Contaminated work clothing should not be allowed out of the workplace.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P308+P313IF exposed or concerned: Get medical advice/attention.

P363Wash contaminated clothing before reuse.

P403Store in a well-ventilated place.

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N-Bromosuccinimide Price

TRC
Product number
B691210
Product name
7-Bromo-2,4-dichloroquinazoline
Packaging
250mg
Price
$90
Updated
2021/12/16
SynQuest Laboratories
Product number
3H32-D-3S
Product name
7-Bromo-2,4-dichloroquinazoline
Purity
98%
Packaging
1g
Price
$125
Updated
2021/12/16
AK Scientific
Product number
W9790
Product name
7-Bromo-2,4-dichloroquinazoline
Packaging
5g
Price
$491
Updated
2021/12/16
Matrix Scientific
Product number
122841
Product name
7-Bromo-2,4-dichloroquinazoline
Purity
95+%
Packaging
1g
Price
$858
Updated
2021/12/16
Crysdot
Product number
CD11002827
Product name
7-Bromo-2,4-dichloroquinazoline
Purity
97%
Packaging
25g
Price
$891
Updated
2021/12/16
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2,4-DICHLORO-7-BROMOQUINAZOLINE Chemical Properties,Usage,Production

Synthesis

114703-12-7

959237-68-4

The general procedure for the synthesis of 2,4-dichloro-7-bromoquinazoline from 7-bromoquinazoline-2,4(1H,3H)-dione was as follows: 205.0 g (0.84 mol) of 7-bromo-1H-benzo[d]-1,3-oxazine-2,4-dione was suspended in 1.26 L (12.59 mol) of phosphorochloride at room temperature, followed by the addition of 71.34 mL (0.42 mol) N-ethyl diisopropylamine. The reaction mixture was heated to reflux and kept for 36 hours. Upon completion of the reaction, 193.6 g of the target product 7-bromo-2,4-dichloroquinazoline was obtained by a conventional post-processing step. The product was analyzed by HPLC/MS and showed that the (M+H)+ peak was located at 277/279, confirming the solid form.

References

[1] Patent: US2013/12489, 2013, A1. Location in patent: Paragraph 0174
[2] Bioorganic and Medicinal Chemistry Letters, 2017, vol. 27, # 21, p. 4904 - 4907
[3] Patent: WO2012/58671, 2012, A1. Location in patent: Page/Page column 92-93
[4] Patent: US2014/38952, 2014, A1. Location in patent: Page/Page column 0160-0161
[5] Antimicrobial Agents and Chemotherapy, 2017, vol. 61, # 6,

2,4-DICHLORO-7-BROMOQUINAZOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2,4-DICHLORO-7-BROMOQUINAZOLINE Suppliers

China 130 India 1 United Kingdom 1 United States 7 Global 139
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View Lastest Price from 2,4-DICHLORO-7-BROMOQUINAZOLINE manufacturers

Career Henan Chemical Co
Product
2,4-DICHLORO-7-BROMOQUINAZOLINE 959237-68-4
Price
US $1.00/g
Min. Order
1g
Purity
99%
Supply Ability
10000KGS
Release date
2020-01-10

959237-68-4, 2,4-DICHLORO-7-BROMOQUINAZOLINERelated Search:

2,4-dichloro-8-(trifluoromethoxy)quinazoline 8-METHYL-2,4-DICHLOROQUINAZOLINE 2,4-DICHLORO-1,2,3,4-TETRAHYDRO-7-METHYLQUINAZOLINE 7-Bromoquinazoline 7-BROMO-4-CHLOROQUINAZOLINE 2,4-DICHLORO-7-BROMOQUINAZOLINE 7-bromo-2-chloroquinazoline

  • 2,4-DICHLORO-7-BROMOQUINAZOLINE
  • 7-Bromo-2,4-dichloroquinazoline
  • Quinazoline, 7-bromo-2,4-dichloro-
  • 959237-68-4